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Cyclopentasiloxane, decamethyl-

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Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryUltra-11166.Richmond and Pombo-Villar, 199825. m/0.32 mm/0.52 «mu»m, He, 15. K/min, 320. C @ 10. min; Tstart: 35. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryVF-5MS1215.1Tret'yakov, 200730. m/0.25 mm/0.25 «mu»m, He; Program: Multi-step temperature program; T(initial)=60C; T(final)=270C

Normal alkane RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
PackedSE-30110.1164.Garzo and Alexander, 1971Chromosorb G AW DMCS (80-100 mesh); Column length: 3.5 m
PackedSE-30125.1160.Garzo and Alexander, 1971Chromosorb G AW DMCS (80-100 mesh); Column length: 3.5 m

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillarySP-21001165.Fischer and Kusch, 1993He, 40. C @ 3. min, 5. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tend: 280. C
CapillaryMethyl Silicone1184.Fujimoto, Ohtani, et al., 199025. m/0.25 mm/0.1 «mu»m, He, 5. K/min; Tstart: 40. C; Tend: 350. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryUltra-11169.Kazuyoshi, Seiichi, et al., 200030. m/0.25 mm/0.50 «mu»m; Program: 40 0C (5 min) 10 0C/min -> 200 0C 20 0C/min -> 320 0C (13 min)
CapillaryUltra-11172.Kazuyoshi, Seiichi, et al., 200030. m/0.25 mm/0.50 «mu»m; Program: 40 0C (5 min) 10 0C/min -> 200 0C 20 0C/min -> 320 0C (13 min)
CapillaryUltra-11173.Kazuyoshi, Seiichi, et al., 200030. m/0.25 mm/0.50 «mu»m; Program: 40 0C (5 min) 10 0C/min -> 200 0C 20 0C/min -> 320 0C (13 min)
CapillaryUltra-11176.Kazuyoshi, Seiichi, et al., 200030. m/0.25 mm/0.50 «mu»m; Program: 40 0C (5 min) 10 0C/min -> 200 0C 20 0C/min -> 320 0C (13 min)
CapillaryUltra-11183.Kazuyoshi, Seiichi, et al., 200030. m/0.25 mm/0.50 «mu»m; Program: 40 0C (5 min) 10 0C/min -> 200 0C 20 0C/min -> 320 0C (13 min)
CapillaryUltra-11183.Kazuyoshi, Seiichi, et al., 200030. m/0.25 mm/0.50 «mu»m; Program: 40 0C (5 min) 10 0C/min -> 200 0C 20 0C/min -> 320 0C (13 min)
CapillaryUltra-11161.Richmond and Pombo-Villar, 199825. m/0.32 mm/0.52 «mu»m, He; Program: not specified

Lee's RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-5193.3Fuentes, Font, et al., 2007Column length: 60. m; Program: not specified

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Richmond and Pombo-Villar, 1998
Richmond, R.; Pombo-Villar, E., Short communication. Use of persistent trace gas chromatography artifacts for the calculation of pseudo-Sadtler retention indices, J. Chromatogr. A, 1998, 811, 1-2, 241-245, https://doi.org/10.1016/S0021-9673(98)00285-4 . [all data]

Tret'yakov, 2007
Tret'yakov, K.V., Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2007. [all data]

Garzo and Alexander, 1971
Garzo, G.; Alexander, G., Gas chromatographic retention characteristics of low molecular weight linear, cyclic and polycyclic methylpolysiloxanes, Chromatographia, 1971, 4, 12, 554-560, https://doi.org/10.1007/BF02317591 . [all data]

Fischer and Kusch, 1993
Fischer, G.W.; Kusch, P., An Automated Curie-Point Pyrolysis-High Resolution Gas Chromatography System, LC-GC Int., 1993, 6, 12, 760-763. [all data]

Fujimoto, Ohtani, et al., 1990
Fujimoto, S.; Ohtani, H.; Yamagiwa, K.; Tsuge, S., Study on retention behavior of cyclic siloxanes by high resolution pyrolysis-gas chromatography with a fused silica capillary column, J. Hi. Res. Chromatogr., 1990, 13, 6, 397-404, https://doi.org/10.1002/jhrc.1240130603 . [all data]

Kazuyoshi, Seiichi, et al., 2000
Kazuyoshi, N.; Seiichi, Y.; Kazuo, K.; Katsumi, I.; Okihiko, S., Polymer analysis by improved pyrolysis gas chromatography hyphenated with four specific detectors, J. Soc. Cosmet. Chem. Jpn., 2000, 34, 2, 142-151, https://doi.org/10.5107/sccj.34.142 . [all data]

Fuentes, Font, et al., 2007
Fuentes, M.J.; Font, R.; Gomez-Rico, M.F.; Martin-Gullon, I., Pyrolysis and combustion of waste lubricant oil from diesel cars: Decomposition and pollutants, J. Anal. Appl. Pyrolysis, 2007, 79, 1-2, 215-226, https://doi.org/10.1016/j.jaap.2006.12.004 . [all data]


Notes

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