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Mitotane

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Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
PackedSE-302130.Ramsey, Lee, et al., 1980He, Chromosorb G HP (80-100 mesh); Column length: 1.5 m; Program: not specified

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryOV-12119.de Paoli, Taccheo-Barbina, et al., 199125. m/0.32 mm/0.10 «mu»m, 160. C @ 1. min, 1. K/min; Tend: 240. C
CapillaryOV-12123.de Paoli, Taccheo-Barbina, et al., 199125. m/0.32 mm/0.10 «mu»m, 160. C @ 1. min, 1. K/min; Tend: 240. C
CapillaryOV-12116.de Paoli, Taccheo-Barbina, et al., 199125. m/0.32 mm/0.10 «mu»m, 160. C @ 1. min, 1.3 K/min; Tend: 240. C
CapillaryOV-12128.de Paoli, Taccheo-Barbina, et al., 199125. m/0.32 mm/0.10 «mu»m, 160. C @ 1. min, 1.3 K/min; Tend: 240. C
CapillaryOV-12119.de Paoli, Taccheo-Barbina, et al., 199125. m/0.32 mm/0.10 «mu»m, 160. C @ 1. min, 1.5 K/min; Tend: 240. C
CapillaryOV-12123.de Paoli, Taccheo-Barbina, et al., 199125. m/0.32 mm/0.10 «mu»m, 160. C @ 1. min, 1.5 K/min; Tend: 240. C
CapillaryOV-12116.de Paoli, Taccheo-Barbina, et al., 199125. m/0.32 mm/0.10 «mu»m, 160. C @ 1. min, 2. K/min; Tend: 240. C
CapillaryOV-12128.de Paoli, Taccheo-Barbina, et al., 199125. m/0.32 mm/0.10 «mu»m, 160. C @ 1. min, 2. K/min; Tend: 240. C
CapillaryCP Sil 5 CB2118.Wells, Gillespie, et al., 1985120. C @ 1. min, 3. K/min; Column length: 25. m; Column diameter: 0.22 mm; Tend: 250. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryUltra-12118.Tameo and Kiyos, 1991Program: not specified
CapillaryOV-12146.Waggott and Davies, 1984Hydrogen; Column length: 50. m; Column diameter: 0.32 mm; Program: not specified
CapillaryOV-1, SE-30, Methyl silicone, SP-2100, OV-101, DB-1, etc.2146.Waggott and Davies, 1984Hydrogen; Column length: 50. m; Column diameter: 0.32 mm; Program: not specified
OtherMethyl Silicone2130.Ardrey and Moffat, 1981Program: not specified

Normal alkane RI, polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryCarbowax 20M3104.Tameo and Kiyos, 1991Program: not specified
CapillarySuperox 0.6; Carbowax 20M3120.Waggott and Davies, 1984Hydrogen; Column length: 50. m; Column diameter: 0.32 mm; Program: not specified
CapillaryCarbowax 400, Carbowax 20M, Carbowax 1540, Carbowax 4000, Superox 06, PEG 20M, etc.3120.Waggott and Davies, 1984Hydrogen; Column length: 50. m; Column diameter: 0.32 mm; Program: not specified

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Ramsey, Lee, et al., 1980
Ramsey, J.D.; Lee, T.D.; Osselton, M.D.; Moffat, A.C., Gas-liquid chromatographic retention indices of 296 non-drug substances on SE-30 or OV-1 likely to be encountered in toxicological analyses, J. Chromatogr., 1980, 184, 2, 185-206, https://doi.org/10.1016/S0021-9673(00)85641-1 . [all data]

de Paoli, Taccheo-Barbina, et al., 1991
de Paoli, M.; Taccheo-Barbina, M.; Bontempelli, G., Gas chromatographic system for the identification of halogenated pesticides by retention indices using n-alkanes as standards, J. Chromatogr., 1991, 547, 355-365, https://doi.org/10.1016/S0021-9673(01)88659-3 . [all data]

Wells, Gillespie, et al., 1985
Wells, D.E.; Gillespie, M.J.; Porter, A.E.A., Dichlorobenzyl alkyl ether homologs as retention index markers and internal standards for the analysis of environmental samples using capillary gas chromatography, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1985, 8, 8, 443-449, https://doi.org/10.1002/jhrc.1240080818 . [all data]

Tameo and Kiyos, 1991
Tameo, O.; Kiyos, I., Simultaneous determination of pesticides by capillary gas chromatography, Cannot be traslated (in Japan), 1991, 14, 2, 109-122. [all data]

Waggott and Davies, 1984
Waggott, A.; Davies, I.W., Identification of organic pollutants using linear temperature programmed retention indices (LTPRIs) - Part II, 1984, retrieved from http://dwi.defra.gov.uk/research/completed-research/reports/dwi0383.pdf. [all data]

Ardrey and Moffat, 1981
Ardrey, R.E.; Moffat, A.C., Gas-liquid chromatographic retention indices of 1318 substances of toxicological interest on SE-30 or OV-1 stationary phase, J. Chromatogr., 1981, 220, 3, 195-252, https://doi.org/10.1016/S0021-9673(00)81925-1 . [all data]


Notes

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