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Bicyclo[3.1.0]hexan-3-ol, 4-methylene-1-(1-methylethyl)-, [1S-(1«alpha»,3«beta»,5«alpha»)]-


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spec Data Center, S.E. Stein, director

Kovats' RI, non-polar column, custom temperature program

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Column typeActive phaseIReferenceComment
CapillaryDB-5MS1139.Tuberoso, Kowalczyk, et al., 200530. m/0.25 mm/0.25 «mu»m, He; Program: 60C(5min) => 2C/min => 140C= 5C/min => 250C(5min)
CapillaryBP-11130.MacLeod, MacLeod, et al., 1988Column length: 25. m; Column diameter: 0.2 mm; Program: not specified

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column typeActive phaseIReferenceComment
CapillaryHP-5MS1143.Saroglou, Arfan, et al., 200730. m/0.25 mm/0.25 «mu»m, He, 60. C @ 5. min, 4. K/min; Tend: 280. C
CapillaryMethyl Silicone1133.Sumathykutty, Rao, et al., 199950. m/0.25 mm/0.17 «mu»m, N2, 2. K/min; Tstart: 80. C; Tend: 200. C
CapillaryMethyl Silicone1134.Píry, Príbela, et al., 199525. m/0.2 mm/0.3 «mu»m, He, 2. K/min; Tstart: 40. C; Tend: 200. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column typeActive phaseIReferenceComment
CapillaryHP-5MS1143.1Andriamaharavo, 201430. m/0.25 mm/0.25 «mu»m, He; Program: 60C (1 min) => 5 C/min => 210C => 10 C/min => 280C (15 min)

Normal alkane RI, non-polar column, temperature ramp

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Column typeActive phaseIReferenceComment
CapillaryHP-5 MS1136.Sardashti, Valizadeh, et al., 201360. m/0.25 mm/0.25 «mu»m, Helium, 40. C @ 1. min, 3. K/min, 250. C @ 20. min
CapillaryDB-5 MS1143.Chalchat, Figueredo, et al., 201025. m/0.30 mm/0.25 «mu»m, Helium, 3. K/min; Tstart: 50. C; Tend: 240. C
CapillaryHP-51136.Monsef-Esfahani, Miri, et al., 201030. m/0.25 mm/0.25 «mu»m, Helium, 50. C @ 5. min, 3. K/min; Tend: 240. C
CapillaryDB-11132.Cégiéla-Carlioz, Bessière, et al., 200525. m/0.25 mm/0.25 «mu»m, He, 50. C @ 3. min, 3. K/min; Tend: 250. C
CapillaryHP-5MS1149.Melkani, Dev, et al., 200530. m/0.25 mm/0.25 «mu»m, 50. C @ 10. min, 3. K/min, 250. C @ 5. min
CapillarySE-541141.Kilic, Hafizoglu, et al., 200430. m/0.25 mm/0.25 «mu»m, He, 60. C @ 5. min, 2. K/min; Tend: 260. C
CapillaryDB-51142.Rohloff, Mordal, et al., 200430. m/0.25 mm/0.25 «mu»m, He, 2.5 K/min, 220. C @ 6. min; Tstart: 35. C
CapillaryOV-11114.Bicchi, Binello, et al., 199925. m/0.32 mm/0.30 «mu»m, Hydrogen, 50. C @ 1. min, 3. K/min, 200. C @ 10. min
CapillaryOV-11114.Bicchi, Binello, et al., 199925. m/0.32 mm/0.30 «mu»m, Hydrogen, 50. C @ 1. min, 3. K/min, 200. C @ 10. min
CapillaryOV-11114.Bicchi, Binello, et al., 199925. m/0.32 mm/0.30 «mu»m, Hydrogen, 50. C @ 1. min, 3. K/min, 200. C @ 10. min
CapillaryOV-11117.Bicchi, Binello, et al., 199925. m/0.32 mm/0.30 «mu»m, Hydrogen, 50. C @ 1. min, 3. K/min, 200. C @ 10. min
CapillaryDB-11147.Binder, Flath, et al., 19894. K/min, 250. C @ 5. min; Column length: 60. m; Column diameter: 0.32 mm; Tstart: 50. C

Normal alkane RI, non-polar column, custom temperature program

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Column typeActive phaseIReferenceComment
Capillary5 % Phenyl polydimethyl siloxane1144.Chaverri, Diaz, et al., 2011Program: not specified
CapillaryCP Sil 8 CB1142.Radudienë, Judpintienë, et al., 200550. m/0.32 mm/0.25 «mu»m, He; Program: 60C(2min) => 5C/min => 160C(1min) => 10C/min => 250C (3min)
CapillaryDB-11147.Binder, Flath, et al., 1989Column length: 60. m; Column diameter: 0.32 mm; Program: not specified
CapillaryOV-1011135.Shibamoto, 1987Program: not specified
PackedOV-1011130.Swigar and Silverstein, 1981N2, Chromosorb G 60-80mesh DMCS; Column length: 2.5 m; Program: not specified

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Tuberoso, Kowalczyk, et al., 2005
Tuberoso, C.I.G.; Kowalczyk, A.; Coroneo, V.; Russo, M.T.; Dessì, S.; Cabras, P., Chemical Composition and Antioxidant, Antimicrobial, and Antifungal Activities of the Essential Oil of Achillea ligustica All., J. Agric. Food Chem., 2005, 53, 26, 10148-10153. [doi:10.1021/jf0518913] [all data]

MacLeod, MacLeod, et al., 1988
MacLeod, A.J.; MacLeod, G.; Subramanian, G., Volatile aroma constituents of orange, Phytochemistry, 1988, 27, 7, 2185-2188. [doi:10.1016/0031-9422(88)80123-7] [all data]

Saroglou, Arfan, et al., 2007
Saroglou, V.; Arfan, M.; Shabir, A.; Hadjipavlou-Litina, D.; Skaltsa, H., Composition and antioxidant activity of the essential oil of Teucrium royleanum Wall. ex Benth growing in Pakistan, Flavour Fragr. J., 2007, 22, 2, 154-157. [doi:10.1002/ffj.1774] [all data]

Sumathykutty, Rao, et al., 1999
Sumathykutty, M.A.; Rao, J.M.; Padmakumari, K.P.; Narayanan, C.S., Essential oil constituents of some Piper species, Flavour Fragr. J., 1999, 14, 5, 279-282. [doi:10.1002/(SICI)1099-1026(199909/10)14:5<279::AID-FFJ821>3.0.CO;2-0] [all data]

Píry, Príbela, et al., 1995
Píry, J.; Príbela, A.; Durcanská, J.; Farkas, P., Fractionation of volatiles from blackcurrant (Ribes nigrum L.) by different extractive methods, Food Chem., 1995, 54, 1, 73-77. [doi:10.1016/0308-8146(95)92665-7] [all data]

Andriamaharavo, 2014
Andriamaharavo, N.R., Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2014. [all data]

Sardashti, Valizadeh, et al., 2013
Sardashti, A.R.; Valizadeh, J.; Adhami, Y., Variations in the essential oil composition of Peroskia abrotonolides of different growth stage in Baluchestan, Middle-East J. Sci. Res., 2013, 13, 6, 781-784. [all data]

Chalchat, Figueredo, et al., 2010
Chalchat, J.-C.; Figueredo, G.; Ozcan, M.M.; Unver, A., Effect of hydrodistillation and microwave distillation extraction methods on chemical composition of essential oil of pickling herb and myrtle plants, South Western J. of Agriculture, 2010, 1, 2, 133-141. [all data]

Monsef-Esfahani, Miri, et al., 2010
Monsef-Esfahani, H.R.; Miri, A.; Amini, M.; Amanzadeh, Y.; Hadjiakhoondi, A.; Hajiaghaee, R.; Ajani, Y., Seasonal variations in the chemical composition, antioxidant activity and total phenolic content of Teucrium persicum Boiss. essential oils, Res. J. Biol. Sci., 2010, 5, 7, 492-498. [doi:10.3923/rjbsci.2010.492.498] [all data]

Cégiéla-Carlioz, Bessière, et al., 2005
Cégiéla-Carlioz, P.; Bessière, J.-M.; David, B.; Mariotte, A.-M.; Gibbons, S.; Dijoux-Franca, M.-G., Modulation of multi-drug resistance (MDR) in Staphylococcus aureus by Osha (Ligusticum porteri L., Apiaceae) essential oil compounds, Flavour Fragr. J., 2005, 20, 6, 671-675. [doi:10.1002/ffj.1584] [all data]

Melkani, Dev, et al., 2005
Melkani, A.B.; Dev, V.; Beauchamp, P.S.; Negi, A.; Mehta, S.P.S.; Melkani, K.B., Constituents of the essential oil of a new chemotype of Elsholtzia strobilifera Benth., Biochem. Syst. Ecol., 2005, 33, 4, 419-425. [doi:10.1016/j.bse.2004.10.009] [all data]

Kilic, Hafizoglu, et al., 2004
Kilic, A.; Hafizoglu, H.; Kollmannsberger, H.; Nitz, S., Volatile constituents and key odorants in leaves, buds, flowers, and fruits of Laurus nobilis L., J. Agric. Food Chem., 2004, 52, 6, 1601-1606. [doi:10.1021/jf0306237] [all data]

Rohloff, Mordal, et al., 2004
Rohloff, J.; Mordal, R.; Dragland, S., Chemotypical variation of tansy (Tanacetum vulgare L.) from 40 different locations in Norway, J. Agric. Food Chem., 2004, 52, 6, 1742-1748. [doi:10.1021/jf0352430] [all data]

Bicchi, Binello, et al., 1999
Bicchi, C.; Binello, A.; D'Amato, A.; Rubiolo, P., Reliability of Van den Dool retention indices in the analysis of essential oils, J. Chromatogr. Sci., 1999, 37, 8, 288-294. [doi:10.1093/chromsci/37.8.288] [all data]

Binder, Flath, et al., 1989
Binder, R.G.; Flath, R.A.; Mon, T.R., Volatile components of bittermelon, J. Agric. Food Chem., 1989, 37, 2, 418-420. [doi:10.1021/jf00086a032] [all data]

Chaverri, Diaz, et al., 2011
Chaverri, C.; Diaz, C.; Cicco, J.F., Chemical analysis of essential oils from Ocotea gomezii W.C. Burger and Ocotea morae Gomez-Laur. (Lauraceae) collected at Reserva biologica Alberto M. Brenes in Costa Rica and their cytotoxic activity on Tumor cell lines, J. Braz. Chem. Soc., 2011, 22, 4, s1-s4. [doi:10.1590/S0103-50532011000400018] [all data]

Radudienë, Judpintienë, et al., 2005
Radudienë, J.; Judpintienë, A.; Peèiulytë, D.; Janulis, V., Chemical composition of essential oil and antimicrobial activity of Origanum vulgare, Biologija, 2005, 4, 53-58. [all data]

Shibamoto, 1987
Shibamoto, T., Retention Indices in Essential Oil Analysis in Capillary Gas Chromatography in Essential Oil Analysis, Sandra, P.; Bicchi, C., ed(s)., Hutchig Verlag, Heidelberg, New York, 1987, 259-274. [all data]

Swigar and Silverstein, 1981
Swigar, A.A.; Silverstein, R.M., Monoterpenes, Aldrich Chemical Company, Milwaukee, WI, USA, 1981, 130. [all data]


Notes

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