Pregn-5-ene-3,17,20-triol, (3β,20S)-, 3TMS derivative


Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type Capillary
Active phase OV-1
Column length (m)  
Carrier gas He
Substrate  
Column diameter (mm)  
Phase thickness (μm)  
Tstart (C) 180.
Tend (C) 250.
Heat rate (K/min) 1.
Initial hold (min)  
Final hold (min)  
I 2944.
ReferenceBègue, Dumas, et al., 1979
Comment MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Bègue, Dumas, et al., 1979
Bègue, R.-J.; Dumas, M.; Morinière, M.; Nivois, C.; Padieu, P., Steroids and hypertension. 1-Gas-liquid chromatography and gas chromatography mass spectrometry of 3,15- and 3,16-dihydroxy-17-oxosteroids, Biomed. Mass Spectrom., 1979, 6, 11, 476-481, https://doi.org/10.1002/bms.1200061104 . [all data]


Notes

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