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3,16-Dihydroxyandrost-5-en-17-one, (3«beta»,16«beta»)-, 2TMS derivative


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryOV-12727.Bègue, Dumas, et al., 1979He, 1. K/min; Tstart: 180. C; Tend: 250. C
CapillaryOV-12729.Bègue, Dumas, et al., 1979He, 1. K/min; Tstart: 180. C; Tend: 250. C
CapillarySE-302698.Bègue, Dumas, et al., 1979N2, 1. K/min; Column length: 25. m; Column diameter: 0.5 mm; Tstart: 210. C; Tend: 260. C
CapillarySE-302698.Bègue, Dumas, et al., 1979N2, 1. K/min; Column length: 25. m; Column diameter: 0.5 mm; Tstart: 210. C; Tend: 260. C

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Bègue, Dumas, et al., 1979
Bègue, R.-J.; Dumas, M.; Morinière, M.; Nivois, C.; Padieu, P., Steroids and hypertension. 1-Gas-liquid chromatography and gas chromatography mass spectrometry of 3,15- and 3,16-dihydroxy-17-oxosteroids, Biomed. Mass Spectrom., 1979, 6, 11, 476-481, https://doi.org/10.1002/bms.1200061104 . [all data]


Notes

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