Androstane-3,16-diol, (3«beta»,5«alpha»,16«beta»)-, 2TMS derivative


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type Packed
Active phase SE-30
Column length (m) 2.
Carrier gas N2
Substrate Gas Chrom Q
Column diameter (mm)  
Phase thickness (mum)  
Tstart (C) 150.
Tend (C) 300.
Heat rate (K/min) 4.
Initial hold (min)  
Final hold (min)  
I 2605.
ReferenceHarvey, 1980
Comment MSDC-RI

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Harvey, 1980
Harvey, D.J., Vinyldimethylsilyl ethers as derivative for the characterization of steroids and cannabinoids by gas chromatography mass spectrometry, Biomed. Mass Spectrom., 1980, 7, 5, 211-216, https://doi.org/10.1002/bms.1200070507 . [all data]


Notes

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