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Kovats' RI, polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase StabilwaxPE-WaxPE-WaxDB-WaxDB-Wax
Column length (m) 30.30.30.60.60.
Carrier gas N2N2N2HeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (mum) 1.  0.250.25
Tstart (C) 50.60.60.40.40.
Tend (C) 220.200.200.200.200.
Heat rate (K/min) 2.5.5.3.3.
Initial hold (min) 3.4.4.5.5.
Final hold (min) 15.5.5.  
I 1462.1442.1442.1456.1456.
ReferenceHazzit, Baaliouamer, et al., 2006Chandravadana, Vekateshwarlu, et al., 2005Venkateshwarlu, Chandravadana, et al., 1999Tatsuka, Suekane, et al., 1990Tatsuka, Suekane, et al., 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryPackedCapillaryCapillaryCapillary
Active phase DB-WaxCarbowax 20MCarbowax 20MCarbowax 20MCarbowax 20M
Column length (m) 60.2.150.150.150.
Carrier gas HeN2HeHe 
Substrate  Chromosorb W A/W DMCS   
Column diameter (mm) 0.25 0.640.640.64
Phase thickness (mum)      
Tstart (C) 40.60.50.50.50.
Tend (C) 200.200.170.170.170.
Heat rate (K/min) 2.3.1.1.1.
Initial hold (min) 10. 30.30.30.
Final hold (min)      
I 1445.1427.1460.1460.1460.
ReferenceUmano and Shibamoto, 1987Chen, Chen, et al., 1984Buttery, Kamm, et al., 1982Buttery, Kamm, et al., 1982Buttery, Ling, et al., 1982
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase Carbowax 20MCarbowax 20M
Column length (m) 50.50.
Carrier gas HeHe
Substrate   
Column diameter (mm) 0.280.28
Phase thickness (mum)   
Tstart (C) 70.70.
Tend (C) 190.190.
Heat rate (K/min) 2.2.
Initial hold (min)   
Final hold (min)   
I 1437.1437.
ReferenceTressl, Friese, et al., 1978Tressl, Friese, et al., 1978, 2
Comment MSDC-RI MSDC-RI

References

Go To: Top, Kovats' RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Hazzit, Baaliouamer, et al., 2006
Hazzit, M.; Baaliouamer, A.; Faleiro, M.L.; Miguel, M.G., Composition of the Essential Oils of Thymus and Origanum Species from Algeria and Their Antioxidant and Antimicrobial Activities, J. Agric. Food Chem., 2006, 54, 17, 6314-6321, https://doi.org/10.1021/jf0606104 . [all data]

Chandravadana, Vekateshwarlu, et al., 2005
Chandravadana, M.V.; Vekateshwarlu, G.; Bujji Babu, C.S.; Roy, T.K.; Shivashankara, K.S.; Pandey, M.; Tewari, R.P.; Selvaraj, Y., Volatile flavour components of dry milky mushrooms (Calocybe indica), Flavour Fragr. J., 2005, 20, 6, 715-717, https://doi.org/10.1002/ffj.1653 . [all data]

Venkateshwarlu, Chandravadana, et al., 1999
Venkateshwarlu, G.; Chandravadana, M.V.; Tewari, R.P., Volatile flavour components of some edible mushrooms (Basidiomycetes), Flavour Fragr. J., 1999, 14, 3, 191-194, https://doi.org/10.1002/(SICI)1099-1026(199905/06)14:3<191::AID-FFJ810>3.0.CO;2-7 . [all data]

Tatsuka, Suekane, et al., 1990
Tatsuka, K.; Suekane, S.; Sakai, Y.; Sumitani, H., Volatile constituents of kiwi fruit flowers: simultaneous distillation and extraction versus headspace sampling, J. Agric. Food Chem., 1990, 38, 12, 2176-2180, https://doi.org/10.1021/jf00102a015 . [all data]

Umano and Shibamoto, 1987
Umano, K.; Shibamoto, T., Analysis of headspace volatiles from overheated beef fat, J. Agric. Food Chem., 1987, 35, 1, 14-18, https://doi.org/10.1021/jf00073a004 . [all data]

Chen, Chen, et al., 1984
Chen, C.-C.; Chen, S.-D.; Chen, J.-J.; Wu, C.-M., Effects of pH value on the formation of volatiles of shiitake (Lentinus edodes), and edible mushroom, J. Agric. Food Chem., 1984, 32, 5, 999-1001, https://doi.org/10.1021/jf00125a011 . [all data]

Buttery, Kamm, et al., 1982
Buttery, R.G.; Kamm, J.A.; Ling, L.C., Volatile components of alfalfa flowers and pods, J. Agric. Food Chem., 1982, 30, 4, 739-742, https://doi.org/10.1021/jf00112a028 . [all data]

Buttery, Ling, et al., 1982
Buttery, R.G.; Ling, L.C.; Wellso, S.G., Oat leaf volatiles: possible insect attractants, J. Agric. Food Chem., 1982, 30, 4, 791-792, https://doi.org/10.1021/jf00112a045 . [all data]

Tressl, Friese, et al., 1978
Tressl, R.; Friese, L.; Fendesack, F.; Köppler, H., Gas chromatographic--mass spectrometric investigation of hop aroma constituents in beer, J. Agric. Food Chem., 1978, 26, 6, 1422-1426, https://doi.org/10.1021/jf60220a037 . [all data]

Tressl, Friese, et al., 1978, 2
Tressl, R.; Friese, L.; Fendesack, F.; Köppler, H., Studies of the volatile composition of hops during storage, J. Agric. Food Chem., 1978, 26, 6, 1426-1430, https://doi.org/10.1021/jf60220a036 . [all data]


Notes

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