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Clotiazepam


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spec Data Center, S.E. Stein, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillaryBP-1250.2513.Weston, Japp, et al., 199125. m/0.22 mm/0.25 «mu»m, N2
CapillaryDB-1250.2530.Weston, Japp, et al., 199130. m/0.53 mm/1.5 «mu»m, N2

Kovats' RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryCross-Linked Methylsilicone2540.Maurer and Pfleger, 198712. m/0.2 mm/0.33 «mu»m, He, 100. C @ 3. min, 30. K/min, 310. C @ 5. min

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-52485.Zamechnik, Ethier, et al., 198915. m/0.25 mm/0.25 «mu»m, He, 150. C @ 1. min, 10. K/min; Tend: 260. C

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Weston, Japp, et al., 1991
Weston, S.I.; Japp, M.; Partridge, J.; Osselton, M.D., Collection of analytical data for benzodiazepines and benzophenones. Appendix, J. Chromatogr., 1991, 538, 2, 277-284, https://doi.org/10.1016/S0021-9673(01)88848-8 . [all data]

Maurer and Pfleger, 1987
Maurer, H.; Pfleger, K., Identification and differentiation of benzodiazepines and their metabolites in urine by computerized gas chromatography-mass spectrometry, J. Chromatogr., 1987, 422, 85-101, https://doi.org/10.1016/0378-4347(87)80442-5 . [all data]

Zamechnik, Ethier, et al., 1989
Zamechnik, J.; Ethier, J.-C.; Neville, G.A., Benzodiazepines- an extensive collection of mass spectra, J. Can. Soc. Forensic Sci., 1989, 22, 3, 233-259, https://doi.org/10.1080/00085030.1989.10757437 . [all data]


Notes

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