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5-Methylcytosine, 2TMS derivative


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spec Data Center, S.E. Stein, director

Kovats' RI, non-polar column, isothermal

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Column typeActive phaseTemperature (C)IReferenceComment
PackedOV-101160.1536.3Miller, Pacáková, et al., 1976Ar, AW-DMCS Chromosorb W HP; Column length: 2. m

Kovats' RI, non-polar column, custom temperature program

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Column typeActive phaseIReferenceComment
PackedOV-11533.Yamaji, Kimura, et al., 1978Gas Chrom Q; Column length: 1. m; Program: not specified
PackedOV-11533.Yamaji, Kimura, et al., 1978Gas Chrom Q; Column length: 1. m; Program: not specified
PackedOV-11537.Yamaji, Kimura, et al., 1978Gas Chrom Q; Column length: 1. m; Program: not specified
PackedOV-11537.Yamaji, Kimura, et al., 1978Gas Chrom Q; Column length: 1. m; Program: not specified
PackedOV-11537.Yamaji, Kimura, et al., 1978Gas Chrom Q; Column length: 1. m; Program: not specified
PackedOV-11538.Yamaji, Kimura, et al., 1978Gas Chrom Q; Column length: 1. m; Program: not specified
PackedOV-11533.Yamaji, Kimura, et al., 1978Gas Chrom Q; Column length: 1. m; Program: not specified

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column typeActive phaseIReferenceComment
PackedOV-11546.Butts, 1972He, Chromosorb W HP (80-100 mesh), 10. K/min; Column length: 2. m; Tstart: 100. C; Tend: 325. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column typeActive phaseIReferenceComment
PackedSE-301544.Butts, 1970He, Chromosorb W; Column length: 2. m; Program: not specified

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Miller, Pacáková, et al., 1976
Miller, V.; Pacáková, V.; Smolková, E., Gas-liquid chromatographic analysis of trimethylsilyl derivatives of pyrimidine and purine bases and nucleosides, J. Chromatogr., 1976, 119, 355-367. [doi:10.1016/S0021-9673(00)86799-0] [all data]

Yamaji, Kimura, et al., 1978
Yamaji, A.; Kimura, S.; Kawasaki, H.; Yuki, H., Gas chromatographic analysis of pyrimidine and purine bases by retention indices, Yakugaku Zasshi, 1978, 98, 1, 1536-1541. [all data]

Butts, 1972
Butts, W.C., Two-Column Gas Chromatography of Trimethylsilyl Derivatives of Biochemically Significant Compounds, Anal. Biochemistry, 1972, 46, 1, 187-199. [doi:10.1016/0003-2697(72)90411-3] [all data]

Butts, 1970
Butts, W.C., Gas chromatographic separation of trimethylsilyl (TMS)-nucleosides: TMS-methoxime derivatives of cytidine and deoxycytidine, J. Chromatogr. Sci., 1970, 8, 8, 474-476. [doi:10.1093/chromsci/8.8.474] [all data]


Notes

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