6-(Dimethylamino)purine, TMS derivative
- Formula: C10H17N5Si
- Molecular weight: 235.3610
- IUPAC Standard InChI: InChI=1S/C10H17N5Si/c1-14(2)9-8-10(12-6-11-9)15(7-13-8)16(3,4)5/h6-7H,1-5H3
- IUPAC Standard InChIKey: XILWLVGCTPVKKT-UHFFFAOYSA-N
- CAS Registry Number: 32865-76-2
- Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript. - Other names: 9H-Purin-6-amine, N,N-dimethyl-9-(trimethylsilyl)-; Adenine, N,N-dimethyl-9-(trimethylsilyl)-; Dimethylaminopurine, N-trimethylsilyl-; N,N-Dimethyl-9-(trimethylsilyl)-9H-purin-6-amine; 6-Dimethyladenine, TMS
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Van Den Dool and Kratz RI, non-polar column, custom temperature program
Go To: Top, References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
| Column type | Capillary | Packed |
|---|---|---|
| Active phase | VF-5MS | SE-30 |
| Column length (m) | 30. | 2. |
| Carrier gas | He | He |
| Substrate | Chromosorb W | |
| Column diameter (mm) | 0.25 | |
| Phase thickness (μm) | 0.25 | |
| Program | Multi-step temperature program; T(initial)=60C; T(final)=270C | not specified |
| I | 1850.4 | 1795. |
| Reference | Tret'yakov, 2007 | Butts, 1970 |
| Comment | MSDC-RI | MSDC-RI |
References
Go To: Top, Van Den Dool and Kratz RI, non-polar column, custom temperature program, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Tret'yakov, 2007
Tret'yakov, K.V.,
Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2007. [all data]
Butts, 1970
Butts, W.C.,
Gas chromatographic separation of trimethylsilyl (TMS)-nucleosides: TMS-methoxime derivatives of cytidine and deoxycytidine,
J. Chromatogr. Sci., 1970, 8, 8, 474-476, https://doi.org/10.1093/chromsci/8.8.474
. [all data]
Notes
Go To: Top, Van Den Dool and Kratz RI, non-polar column, custom temperature program, References
- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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