Bicyclo[3.1.0]hex-2-ene, 2-methyl-5-(1-methylethyl)-

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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1RTX-1RTX-1Mega-5HP-5 MS
Column length (m) 30.60.60.25.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.220.220.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.50.35.
Tend (C) 240.230.230.220.300.
Heat rate (K/min) 3.2.2.3.3.
Initial hold (min)    1.5.
Final hold (min)  5.5.5.15.
I 928.932.932.929.929.
ReferenceAlizadeh and Shaabani, 2012Bendiabdellah, El Amine Dib, et al., 2012Bendiabdellah, El Amine Dib, et al., 2012Dell'Agli, Sanna, et al., 2012Kotowska, Zalikowski, et al., 2012
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5HP-5 MSHP-1
Column length (m) 25.25.25.30.30.
Carrier gas HydrogenHydrogenHydrogenHeliumHelium
Substrate      
Column diameter (mm) 0.320.320.320.250.25
Phase thickness (μm) 0.520.520.520.250.25
Tstart (C) 40.40.40.50.60.
Tend (C) 280.280.280.250.240.
Heat rate (K/min) 4.4.4.7.3.
Initial hold (min)    1. 
Final hold (min) 10.10.10.5. 
I 922.922.922.929.928.
ReferenceVelickovic, Ristic, et al., 2012Velickovic, Ristic, et al., 2012Velickovic, Ristic, et al., 2012Zouari, Ayadi, et al., 2012Alizadeh, Khosh-Khui, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Sil 5 CBHP-5DB-5CP-Sil 5 CBDB-1
Column length (m) 25.30.30.25.30.
Carrier gas HeliumHeliumHeliumHydrogenHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.150.250.250.150.25
Tstart (C) 50.60.40.50.40.
Tend (C) 220.240.250.230.210.
Heat rate (K/min)  3.3.3.5.
Initial hold (min)   5.  
Final hold (min)   20.  
I 926.930.928.935.934.
ReferenceAmeen, Usman, et al., 2011Bertoli, Lepnardi, et al., 2011Cao, Li, et al., 2011Esseien, Aboaba, et al., 2011Fathi, Sahari, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSVF-5 MSVF-5 MSSE-30 MSCP-Sil 5 CB
Column length (m) 30.60.60.30.30.
Carrier gas HeliumHeliumHeliumHeliumNitrogen
Substrate      
Column diameter (mm) 0.250.320.320.250.25
Phase thickness (μm) 0.250.250.250.250.26
Tstart (C) 50.30.30.50.45.
Tend (C) 180.260.260.250.280.
Heat rate (K/min) 2.2.2.5.3.
Initial hold (min)    5. 
Final hold (min)  28.28.10.22.
I 919.925.929.926.926.
ReferenceHammami, Kamoun, et al., 2011Leffingwell and Alford, 2011Leffingwell and Alford, 2011Menichini, Tundis, et al., 2011Mothana, Hasson, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5DB-5 MSDB-5 MSDB-5DB-1
Column length (m) 30.25.25.30.30.
Carrier gas NitrogenHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.320.300.300.320.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.50.60.50.
Tend (C) 210.240.240.280.265.
Heat rate (K/min) 3.3.3.3.2.5
Initial hold (min)     1.
Final hold (min)     20.
I 933.926.926.925.917.
ReferencePrasad, Moulekhi, et al., 2011Chalchat, Figueredo, et al., 2010Chalchat, Figueredo, et al., 2010Georgiou, Koutsaviti, et al., 2010Hajimahdipoor, Samadi, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5 MSHP-5SPB-1HP-5 MS
Column length (m) 30.60.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.200.25
Phase thickness (μm) 0.250.250.250.200.25
Tstart (C) 50.40.50.70.60.
Tend (C) 250.250.240.220.220.
Heat rate (K/min) 2.5.3.3.5.
Initial hold (min)  15.5. 10.
Final hold (min)  15. 15. 
I 930.924.922.921.931.
ReferenceHo, Wang, et al., 2010Mesa-Arango, Betancur-Galvis, et al., 2010Monsef-Esfahani, Miri, et al., 2010Neves, Rosa, et al., 2010Ogunwande, Flamini, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5SLB-5 MSSLB-5 MSDB-1-MS
Column length (m) 30.30.10.10.60.
Carrier gas HeliumHydrogenHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.100.100.25
Phase thickness (μm) 0.250.250.100.100.25
Tstart (C) 100.70.50.50.30.
Tend (C) 220.290.250.250.200.
Heat rate (K/min) 2.5.10.10.2.
Initial hold (min)     4.
Final hold (min)     35.
I 924.930.924.925.923.
ReferencePripdeevech, Chumpolsri, et al., 2010Radulovic, Dordevic, et al., 2010Scandinaro, Tranchida, et al., 2010Scandinaro, Tranchida, et al., 2010Takeoka, Hobbs, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-5DB-5OV-101SE-54
Column length (m) 25.30.30.50.30.
Carrier gas  HeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.150.250.250.250.25
Tstart (C) 50.80.40.70.60.
Tend (C) 230.240.250.220.260.
Heat rate (K/min) 3.3.10.2.2.
Initial hold (min)   1. 5.
Final hold (min)  2.3. 999.
I 926.926.930.916.928.
ReferenceUsman, Zubair, et al., 2010Vahirua-Lechat, Mitermite, et al., 2010Yang, Zhang, et al., 2010Benites, Moiteiro, et al., 2009Dayisoylu and Alma, 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSSPB-5DB-5DB-5HP-5MS
Column length (m) 30.60.30.50.60.
Carrier gas HeliumNitrogenHeliumNitrogenHelium
Substrate      
Column diameter (mm) 0.250.350.250.200.25
Phase thickness (μm) 0.250.250.250.320.25
Tstart (C) 60.60.50.60.70.
Tend (C) 250.230.250.220.250.
Heat rate (K/min) 2.4.5.5.3.
Initial hold (min) 8. 2.3. 
Final hold (min) 15.40.   
I 937.930.930.931.930.
ReferenceFarhat, Ginies, et al., 2009Gauvin-Bialecki and Marodon, 2009Ho, Wang, et al., 2009Kazemi and Akhavani, 2009Males, Plazibat, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase VF-1 MSRTX-1RTX-1DB-5DB-5
Column length (m) 30.60.60.30.30.
Carrier gas HeliumHeliumHeliumHeliumNitrogen
Substrate      
Column diameter (mm) 0.250.220.220.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.45.40.
Tend (C) 280.230.230.250.250.
Heat rate (K/min) 4.2.2.3.3.
Initial hold (min) 5.  3.1.
Final hold (min) 10.30.30.5.10.
I 922.921.932.929.926.
ReferenceMarchesini, Prada, et al., 2009Museli, Pau, et al., 2009Museli, Pau, et al., 2009Porto, Decorti, et al., 2009Rahmi-Nasrabadi, Gholivand, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5 MSHP-5MSHP-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas NitrogenHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.40.50.40.50.
Tend (C) 230.250.240.240.280.
Heat rate (K/min) 2.4.5.4.9.
Initial hold (min)  2. 4.3.
Final hold (min)  2.  3.
I 931.928.928.926.930.
ReferenceScrivanti, Anton, et al., 2009Su, Wang, et al., 2009Wannes, Mhamdi, et al., 2009Zhannan, Shiqiong, et al., 2009Aicha, Ines, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5SLB-5 MSZB-1DB-5DB-5 MS
Column length (m) 30.30.30.60.30.
Carrier gas N2HeliumNitrogenNitrogenHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.45.60.50.
Tend (C) 220.250.230.250.300.
Heat rate (K/min) 5.3.3.5.5.
Initial hold (min) 10.2.  5.
Final hold (min)  10. 10.5.
I 933.925.922.929.929.
ReferenceFlamini, Tebano, et al., 2008Lo Presti, Sciarrone, et al., 2008Mierendorff, Stahl-Biskup, et al., 2008Mosayebi, Amin, et al., 2008Noudogbessi, Yedomonhan, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Elite-1BPX-5RTX-5HP-5OV-1
Column length (m) 30.7.520.25.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.320.100.180.250.25
Phase thickness (μm) 0.2510.0.200.250.25
Tstart (C) 60.60.50.60.65.
Tend (C) 246.240.280.240.260.
Heat rate (K/min) 3.3.4.4.6.
Initial hold (min)   1.2. 
Final hold (min)      
I 923.926.929.933.931.
ReferenceRaj, Baby, et al., 2008Shellie, 2008Skalicka-Wozniak, Los, et al., 2008Verdian-rizi, 2008Wang, Yi, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSDB-5MSDB-5HP-5 MSHP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeHeHeliumN2
Substrate      
Column diameter (mm) 0.250.250.260.320.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.60.60.60.50.
Tend (C) 230.240.240.280.240.
Heat rate (K/min) 3.3.3.4.5.
Initial hold (min) 10.  5.1.
Final hold (min) 10.   4.
I 931.931.924.927.931.
ReferenceAdams, Beauchamp, et al., 2007Andrade, Oliveira, et al., 2007Bos, Woerdenbag, et al., 2007Capetanos, Saroglou, et al., 2007Cheraif, Ben Jannet, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5MSDB-1Col-Elite 5MS
Column length (m) 60.30.30.60.30.
Carrier gas HeHeliumHeNitrogenHe
Substrate      
Column diameter (mm) 0.250.260.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.60.60.60.30.
Tend (C) 220.290.250.250.246.
Heat rate (K/min) 3.3.2.4.3.
Initial hold (min)   8.1. 
Final hold (min)   15.10. 
I 935.924.920.926.930.
ReferenceChyau, Tsai, et al., 2007Elfami, Bos, et al., 2007Ferhat, Meklati, et al., 2007Ghasempour, Shirinpour, et al., 2007Gudaityte and Venskutonis R.P., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1RTX-5 MSDB-5MSZB-5HP-5
Column length (m) 30.30.30.30.25.
Carrier gas HeHeHe H2
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (μm) 0.250.250.250.250.33
Tstart (C) 60.45.60.60.60.
Tend (C) 240.210.280.220.240.
Heat rate (K/min) 2.3.3.4.3.
Initial hold (min)    5. 
Final hold (min) 20. 30.20. 
I 921.928.906.926.931.
ReferenceHachicha, Skanji, et al., 2007Hudaib and Aburjai, 2007Marongiu B., Piras A., et al., 2007Mohottalage, Tabacchi, et al., 2007Oliveira, Leitão, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1SPB-1SPB-5BPX-5DB-1
Column length (m) 50.30.30.50.60.
Carrier gas HeHeHeHeNitrogen
Substrate      
Column diameter (mm) 0.250.20.250.220.25
Phase thickness (μm) 0.250.20.251.0.25
Tstart (C) 95.70.50.50.60.
Tend (C) 240.220.250.300.250.
Heat rate (K/min) 4.3.2.4.4.
Initial hold (min)    1.1.
Final hold (min)  15. 10.10.
I 927.923.924.940.926.
ReferencePala-Paul, Brophy, et al., 2007Pinto, Salgueiro, et al., 2007Raal, Orav, et al., 2007Rali, Wossa, et al., 2007Reza, Ebrahim, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSDB-5DBP-5DB-5DB-5
Column length (m) 60.30.25.30.30.
Carrier gas HydrogenHeHelium Helium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.220.25 
Tstart (C) 60.50.40.40.60.
Tend (C) 260.240.250.250.200.
Heat rate (K/min) 4.4.3.2.2.
Initial hold (min)   1.  
Final hold (min) 20. 10.33.20.
I 923.926.899.933.927.
ReferenceRojas, Velasco, et al., 2007Sefidkon, Abbasi, et al., 2007Sereshti and Samadi, 2007Sylvestre, Pichette, et al., 2007Tiwary, Nail, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSHP-5 MSHP-5MSHP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeHeliumHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 60.60.60.40.40.
Tend (C) 200.280.280.250.260.
Heat rate (K/min) 2.3.3.3.4.
Initial hold (min)    5. 
Final hold (min) 20.  10. 
I 931.909.930.923.927.0
ReferenceTiwary, Nail, et al., 2007Tzakou, Bazos, et al., 2007Vagionas, Graikou, et al., 2007Vichi, Riu-Aumatell, et al., 2007Zizovic, Stamenic, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5DB-5HP-1ZB-5
Column length (m) 30.30.30.50.30.
Carrier gas N2N2HeN2 
Substrate      
Column diameter (mm) 0.250.250.250.20.25
Phase thickness (μm) 0.250.250.250.330.25
Tstart (C) 50.50.50.60.40.
Tend (C) 280.280.265.250.300.
Heat rate (K/min) 9.9.2.52.2.
Initial hold (min) 3.3.1.  
Final hold (min) 3.3.20.20. 
I 928.928.929.929.929.
ReferenceAbdelwahed, Hayder, et al., 2006Abdelwahed, Hayder, et al., 2006Bazargani, Almasirad, et al., 2006Berlioz, Cordella, et al., 2006Biondi, Sari, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase AT-5BP-1SPB-1HP-5DB-5
Column length (m) 60.50.30.30.30.
Carrier gas He HeliumHe 
Substrate      
Column diameter (mm) 0.250.220.200.320.32
Phase thickness (μm) 0.250.250.200.250.25
Tstart (C) 60.60.70.60.60.
Tend (C) 200.220.220.246.230.
Heat rate (K/min) 4.2.3.3.3.
Initial hold (min)      
Final hold (min) 20.20.15. 15.
I 934.924.922.928.931.
ReferenceBorges, Rojas, et al., 2006Boti, Yao, et al., 2006Cavaleiro, Pinto, et al., 2006Coronel, Cerda-Garcia-Rojas, et al., 2006Damjanovic, Skala, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5BP-1HP-5HP-1
Column length (m) 30.30.50.30.50.
Carrier gas  HeliumHeHeHe
Substrate      
Column diameter (mm) 0.250.260.220.250.2
Phase thickness (μm) 0.250.250.250.250.33
Tstart (C) 60.60.60.50.60.
Tend (C) 280.290.220.300.250.
Heat rate (K/min) 4.3.2.5.2.
Initial hold (min)    5. 
Final hold (min)   20.5.40.
I 932.924.922.926.923.
ReferenceEbrahim Sajjadi and Mehregan, 2006Elfami, Komar, et al., 2006Fanciullino, Tomi, et al., 2006Figuérédo, Cabassu, et al., 2006Filippi, Lanfranchi, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5CP Sil 5 CBHP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.50.40.60.
Tend (C) 240.240.250.220.240.
Heat rate (K/min) 5.5.3.3.4.
Initial hold (min) 2.2.   
Final hold (min)   10.3. 
I 933.933.929.930.931.
ReferenceGohari, Hadjiakhoondi, et al., 2006Gohari A.R., Hadjiakhoondi A., et al., 2006Havlik, Kokoska, et al., 2006Hymete, Rohloff, et al., 2006Ibañez and Usubillaga, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSMethyl SiliconeHP-5CP Sil 5 CBCP Sil 5 CB
Column length (m) 30.25.30.30.30.
Carrier gas HeHeHeliumN2N2
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.90.60.60.50.
Tend (C) 280.220.260.300.200.
Heat rate (K/min) 5.7.5.5.5.
Initial hold (min) 4.2.2.4. 
Final hold (min) 10. 13.  
I 932.922.928.924.922.
ReferenceKim, El-Aty, et al., 2006Kitchlu, Bakshi, et al., 2006Kucuk, Gulec, et al., 2006Kurowska and Galazka, 2006Martin, Joseph, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1DB-5DB-5CP-Sil 5 CBNB-30
Column length (m) 25.30.30.25.30.
Carrier gas HeHeHeHydrogenHe
Substrate      
Column diameter (mm) 0.30.250.250.250.2
Phase thickness (μm)  0.250.250.150.25
Tstart (C) 70.60.50.50.50.
Tend (C) 220.220.250.230.250.
Heat rate (K/min) 4.4.4.3.2.
Initial hold (min) 2.    
Final hold (min) 10.    
I 936.931.928.933.920.
ReferenceMoody, Gundidza, et al., 2006Morteza-Semnani, Akbarzadeh, et al., 2006Najafpour Navaei, Mirza, et al., 2006Olawore, Usman, et al., 2006Orav, Raal, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-52DB-1DB-5HP-5MSHP-5MS
Column length (m) 50.50.30.30.30.
Carrier gas HeliumN2HydrogenHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 50.95.70.60.50.
Tend (C) 240.240.280.280.250.
Heat rate (K/min) 3.4.4.3.10.
Initial hold (min)   4. 5.
Final hold (min)      
I 931.927.931.909.927.
ReferenceOzcan, Chalchat, et al., 2006Pala-Paul J., Perez-Alonso M.J., et al., 2006Pino, Marbot, et al., 2006Pitarokili, Tzakou, et al., 2006Robinson, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5ZB-5FSOT-RSL-200DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHydrogenHe
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.40.40.50.
Tend (C) 200.260.300.280.240.
Heat rate (K/min) 2.5.2.6.4.
Initial hold (min)    5. 
Final hold (min) 60.  5. 
I 934.927.929.930.931.
ReferenceRout, Naik, et al., 2006Sabulal, Dan, et al., 2006Sari M., Biondi D.M., et al., 2006Schmidt, Jirovetz, et al., 2006Sefidkon, Abbasi, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-1DB-5HP-5
Column length (m) 30.30.60.30.25.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (μm) 0.250.25 0.250.33
Tstart (C) 50.40.40.40.30.
Tend (C) 240.240.250.260.280.
Heat rate (K/min) 4.4.4.2.3.
Initial hold (min)    5. 
Final hold (min)    20. 
I 927.930.927.930.930.
ReferenceSefidkon, Abbasi, et al., 2006Sefidkon and Jamzad, 2006Sefidkon, Jamzad, et al., 2006Senatore, Landolfi, et al., 2006Shafi, Jose, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-1Methyl SiliconeSPB-5DB-5
Column length (m) 25.30.25.60.30.
Carrier gas   N2HeN2
Substrate      
Column diameter (mm) 0.250.320.30.320.25
Phase thickness (μm)  0.250.151.0.25
Tstart (C) 50.60.50.40.60.
Tend (C) 230.230.210.230.240.
Heat rate (K/min) 3.3.2.3.4.
Initial hold (min)  3.5.5. 
Final hold (min)  10. 2. 
I 928.926.934.934.933.
ReferenceTesso, Kubeczka, et al., 2006Tohar, Mohd, et al., 2006Tonzibo, Coffy, et al., 2006Tornambe, Cornu, et al., 2006Trilles, Bombarda, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1SPB-1SPB-1DB-5HP-5MS
Column length (m) 50.50.30.30.30.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (μm) 0.250.330.250.250.25
Tstart (C) 90.50.50.40.60.
Tend (C) 240.220.250.250.280.
Heat rate (K/min) 4.4.4.4.3.
Initial hold (min)  1.1.  
Final hold (min)  10.10.  
I 916.922.933.922.925.
ReferenceVelasco-Negueruela, Pérez-Alonso, et al., 2006Wong, Lim, et al., 2006Wong, Sivasothy, et al., 2006Yadegarinia, Gachkar, et al., 2006Basta, Tzakou, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1DB-5MSDB-1DB-5Methyl Silicone
Column length (m) 50.30.25.50.60.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.20.250.250.30.3
Phase thickness (μm) 0.50.250.250.25 
Tstart (C) 60.60.50.60.50.
Tend (C) 250.240.250.240.240.
Heat rate (K/min) 2.3.3.2.3.
Initial hold (min)   3.  
Final hold (min) 60.    
I 922.929.926.930.924.
ReferenceBendimerad and Bendiab, 2005Busman, Zoghbi, et al., 2005Cégiéla-Carlioz, Bessière, et al., 2005Chagonda and Chalchat, 2005Chalchat and Özcan, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5HP-1HP-5RSL-200DB-5
Column length (m) 60.50.30.30.30.
Carrier gas He He He
Substrate      
Column diameter (mm) 0.320.20.250.250.25
Phase thickness (μm) 1.0.250.250.250.25
Tstart (C) 40.60.50.40.60.
Tend (C) 230.250.300.280.230.
Heat rate (K/min) 3.2.5.6.3.
Initial hold (min) 5.60.5.2. 
Final hold (min)   5.10. 
I 934.923.926.930.921.
ReferenceCornu, Kondjoyan, et al., 2005Fernandez, Lizzani-Cuvelier, et al., 2005Figuérédo, Cabassu, et al., 2005Jirovetz, Buchbauer, et al., 2005Limberger, Sobral, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5CP Sil 5 CBDB-5HP-5MS
Column length (m) 30.30.25.30.30.
Carrier gas HeHe He 
Substrate      
Column diameter (mm) 0.250.250.250.320.2
Phase thickness (μm) 0.250.250.150.25 
Tstart (C) 60.60.50.40.60.
Tend (C) 220.220.230.250.280.
Heat rate (K/min) 4.4.3.5.3.
Initial hold (min) 5.4. 0.5 
Final hold (min)    2. 
I 930.932.933.938.930.
ReferenceMorteza-Semnani, Akbarzadeh, et al., 2005Morteza-Semnani and Saeedi, 2005Ogunwande, Olawore, et al., 2005Özel, Gögüs, et al., 2005Petrakis, Roussis, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-1CP Sil 5 CBCP Sil 5 CBHP-5
Column length (m) 30.60.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.320.250.250.25 
Tstart (C) 60.50.40.40.60.
Tend (C) 250.250.220.220.240.
Heat rate (K/min) 5.4.4.4.5.
Initial hold (min) 3. 1.1. 
Final hold (min)      
I 924.916.930.930.933.
ReferencePourmortazavi, Ghadiri, et al., 2005Rasooli and Owlia, 2005Rohloff and Bones, 2005Rohloff and Bones, 2005Saeidnia, Gohari, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSHP-5MSDB-1DB-1
Column length (m) 30.30.30.60.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.50.
Tend (C) 280.275.280.250.265.
Heat rate (K/min) 4.4.4.5.2.5
Initial hold (min)     1.
Final hold (min)    10.20.
I 928.929.927.926.921.
ReferenceSajjadi S.E. and Eskandari B., 2005Sajjadi and Ghannadi, 2005Sajjadi, 2005Salehi, Sonboli, et al., 2005Sarkhail, Amin, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5MSDB-5HP-5MSDB-1
Column length (m) 30.30.30.30.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 40.60.60.60.60.
Tend (C) 240.240.230.280.250.
Heat rate (K/min) 4.3.3.3.5.
Initial hold (min)      
Final hold (min)   20. 10.
I 930.931.930.923.922.
ReferenceSefidkon and Jamzad, 2005da Silva, Andrade, et al., 2005Skoula and Grayer, 2005Slavkovska, Couladis, et al., 2005Sonboli, Salehi, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSHP-5MSDB-1HP-5MS
Column length (m) 30.30.30.50.30.
Carrier gas  HeHe  
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.50.60.60.40.
Tend (C) 210.240.280.240.220.
Heat rate (K/min) 2.3.3.3.3.
Initial hold (min) 2.3.  5.
Final hold (min) 33.   10.
I 934.910.909.913.923.
ReferenceStevanovic, Garneau, et al., 2005Tepe B., Sokmen M., et al., 2005Tzakou, Bazos, et al., 2005Velasco-Negueruela, Pérez-Alonso, et al., 2005Vichi, Riu-Aumatell, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1CP Sil 5 CBDB-5HP-5 MSHP-5MS
Column length (m) 50.30.30.30.30.
Carrier gas HeN2HeHeliumHe
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (μm) 0.330.250.250.250.25
Tstart (C) 50.50.90.60.60.
Tend (C) 220.200.220.275.275.
Heat rate (K/min) 4.5.7.4.4.
Initial hold (min) 3. 2.  
Final hold (min) 30. 5.  
I 926.921.923.927.924.
ReferenceWong, Lee, et al., 2005Agnaniet, Menut, et al., 2004Agnihotri, Thappa, et al., 2004Ghannadi, Sajjadi, et al., 2004Hajhashemi V., Ghannadi A., et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5ZB-5DB-5RTX-1
Column length (m) 25.25.60.60.30.
Carrier gas  NitrogenHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.40.40.60.
Tend (C) 180.240.260.280.300.
Heat rate (K/min) 3.3.6.4.4.
Initial hold (min) 10. 4.64. 
Final hold (min) 10. 1.  
I 931.928.934.926.926.
Referencebin Jantan, Ayop, et al., 2004JAvidnia, Mojab, et al., 2004Jürgens and Dötterl, 2004Kalvandi, Sefidkon, et al., 2004Kalemba and Thiem, 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-54HP-5MSRTX-1DB-5NB-30
Column length (m) 30.30.30.30.50.
Carrier gas HeHeN2 He
Substrate      
Column diameter (mm) 0.250.250.320.250.2
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.60.40.50.
Tend (C) 260.230.300.210.250.
Heat rate (K/min) 2.5.4.2.2.
Initial hold (min) 5.2. 2. 
Final hold (min)  10. 33. 
I 928.908.916.934.923.
ReferenceKilic, Hafizoglu, et al., 2004Li and Jiang, 2004Lis, Boczek, et al., 2004Lopez Arze, Collin, et al., 2004Orav, Stulova, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase NB-30DB-1DB-1NB-30DB-1
Column length (m) 50.50.50.50.60.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.20.220.250.20.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.70.95.50.50.
Tend (C) 250.220.240.250.250.
Heat rate (K/min) 2.4.4.2.4.
Initial hold (min)      
Final hold (min)      
I 923.926.918.924.916.
ReferenceOrav, Stulova, et al., 2004Palá-Paúl, García-Jiménez, et al., 2004Palá-Paúl, Velasco-Negueruela, et al., 2004Raal, Arak, et al., 2004Rasooli and Razzaghi Abyaneh, 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5Methyl SiliconeHP-5 MSHP-5MSHP-5MS
Column length (m) 30.60.30.30.30.
Carrier gas HeHeHeliumHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 35.60.60.60.60.
Tend (C) 220.200.200.280.280.
Heat rate (K/min) 2.54.4.4.4.
Initial hold (min)  1.1.  
Final hold (min) 6.20.20.  
I 930.920.920.925.929.
ReferenceRohloff, Mordal, et al., 2004Rojas, Usubillaga, et al., 2004Royas, Usubillaga, et al., 2004Sadeghpour, Asghari, et al., 2004Sajjadi and Shahpiri, 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5HP-1HP-5HP-5
Column length (m) 30.30.30.25.25.
Carrier gas He HeN2H2
Substrate      
Column diameter (mm) 0.250.250.250.20.32
Phase thickness (μm) 0.250.250.330.50.52
Tstart (C) 50.50.40.30.40.
Tend (C) 265.250.260.280.240.
Heat rate (K/min) 2.53.2.3.4.
Initial hold (min) 1.5.5.  
Final hold (min) 20. 20.  
I 921.930.924.930.931.
ReferenceSarkhail, Amin, et al., 2004Sefidkon, Jamzad, et al., 2004Senatore, Napolitano, et al., 2004Shafi, Nambiar, et al., 2004Simic, Sokovic, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5CP Sil 5 CBBPX-5CP Sil 8 CBDB-5
Column length (m) 30.20.25.30.30.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.250.250.220.320.249
Phase thickness (μm) 0.250.251.0.250.25
Tstart (C) 60.100.60.50.60.
Tend (C) 240.270.250.200.300.
Heat rate (K/min) 3.8.3.5.3.
Initial hold (min)  2.5.5. 
Final hold (min)   10.  
I 927.921.933.929.925.
ReferenceTellez, Khan, et al., 2004Thappa, Bakshi, et al., 2004Vilaseca, Guy, et al., 2004Wang, Guo, et al., 2004Woerdenbag, Windono, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5DB-1RTX-5SilDB-1
Column length (m) 30.30.60.30.60.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 60.60.50.70.50.
Tend (C) 275.220.250.200.250.
Heat rate (K/min) 4.5.4.4.4.
Initial hold (min)  10.   
Final hold (min)    10. 
I 930.938.936.927.933.
ReferenceAfsharypuor and Jahromy, 2003Bertoli, Menichini, et al., 2003Dabiri and Sefidkon, 2003Dudai, Larkov, et al., 2003Ebrahimzadeh, Yamini, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5MSDB-1HP-5MS
Column length (m) 60.60.30.30.30.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.320.320.250.250.25
Phase thickness (μm)   0.250.250.25
Tstart (C) 50.50.60.50.60.
Tend (C) 220.200.220.200.280.
Heat rate (K/min) 3.3.5.5.4.
Initial hold (min)   20.  
Final hold (min)   20.  
I 926.926.936.913.931.
ReferenceEdris and Farrag, 2003Edris, Shalaby, et al., 2003Feizbaksh, Saber Tehrani, et al., 2003Fekam Boyom, Ngouana, et al., 2003Ghasemi, Asghari, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSRSL-200RSL-200DB-5SE-30
Column length (m) 30.30.30.50.12.
Carrier gas HeH2H2HeHe
Substrate      
Column diameter (mm) 0.250.320.320.20.22
Phase thickness (μm) 0.250.250.250.250.3
Tstart (C) 60.40.40.50.70.
Tend (C) 275.280.280.220.220.
Heat rate (K/min) 4.6.6.3.3.
Initial hold (min)  5.5.2. 
Final hold (min)  5.5.10. 
I 927.927.927.917.920.
ReferenceHajhashemi, Ghannadi, et al., 2003Jirovetz, Buchbauer, et al., 2003Jirovetz, Buchbauer, et al., 2003, 2Juteau, Jerkovic, et al., 2003Kambouche and El-Abed, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-5MSDB-5CP Sil 5 CBZB-1
Column length (m) 25.30.50.25.30.
Carrier gas HeHeHe N2
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (μm) 0.250.250.250.390.25
Tstart (C) 35.60.50.60.45.
Tend (C) 280.240.220.220.230.
Heat rate (K/min) 5.3.3.5.3.
Initial hold (min) 2.5 2.  
Final hold (min)      
I 921.928.928.926.922.
ReferenceKanjilal, Kotoky, et al., 2003Maia, Taveira, et al., 2003Masotti, Juteau, et al., 2003Mazloomifar, Saber-Tehrani, et al., 2003Mierendorff, Stahl-Biskup, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5OV-101CP Sil 5 CBDB-1DB-5
Column length (m) 30.50.25.50.30.
Carrier gas HeliumHeH2N2H2
Substrate      
Column diameter (mm) 0.320.20.250.250.25
Phase thickness (μm)  0.50.150.250.25
Tstart (C) 70.50.50.95.60.
Tend (C) 210.250.230.240.280.
Heat rate (K/min) 2.2.3.4.4.
Initial hold (min)     10.
Final hold (min) 60.   40.
I 930.921.925.936.931.
ReferenceMookdasanit, Tamura, et al., 2003Orav, Kailas, et al., 2003Oyedeji, Ekundayo, et al., 2003Perez-Alonso, Velasco-Negueruela, et al., 2003Pino, Marbot, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-1DB-1HP-5DB-1
Column length (m) 30.60.60.30.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.40.40.60.40.
Tend (C) 280.220.220.280.260.
Heat rate (K/min) 3.4.4.4.4.
Initial hold (min)     5.
Final hold (min)      
I 909.923.923.930.935.
ReferencePitarokili, Tzakou, et al., 2003Rasooli and Mirmostafa, 2003Rasooli and Mirmostafa, 2003Sajjadi and Mehregan, 2003Sefidkon, Naderi Nik, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5CP Sil 5 CBDB-1HP-5
Column length (m) 60.60.25.50.25.
Carrier gas He  N2Helium
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.250.150.250.53
Tstart (C) 50.40.50.90.40.
Tend (C) 280.250.230.240.280.
Heat rate (K/min) 4.5.3.4.4.
Initial hold (min)  15.   
Final hold (min)      
I 935.928.927.903.922.
ReferenceShahmir, Ahmadi, et al., 2003Stashenko, Jaramillo, et al., 2003Taiwo and Bolanle, 2003Velasco-Negueruela, Pérez-Alonso, et al., 2003Velickovic, Ristic, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5DB-5DB-1
Column length (m) 25.25.30.25.60.
Carrier gas HeliumHeliumHeN2He
Substrate      
Column diameter (mm) 0.320.320.250.250.25
Phase thickness (μm) 0.530.530.320.250.25
Tstart (C) 40.40.60.50.60.
Tend (C) 280.280.250.250.220.
Heat rate (K/min) 4.4.5.4.4.
Initial hold (min)   30.  
Final hold (min)    10. 
I 928.930.937.928.936.
ReferenceVelickovic, Ristic, et al., 2003Velickovic, Ristic, et al., 2003Yassa, Akhani, et al., 2003Zrira, Elamrani, et al., 2003Baher, Mirza, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5OV-101DB-5HP-15 % Phenyl methyl siloxane
Column length (m) 30.25.30.30.30.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.2490.320.250.250.25
Phase thickness (μm) 0.25 0.250.250.25
Tstart (C) 60.50.60.70.75.
Tend (C) 300.200.280.220.200.
Heat rate (K/min) 3.5.3.3.3.
Initial hold (min)     4.
Final hold (min) 5. 30.15.8.
I 925.925.924.922.930.
ReferenceBos, Koulman, et al., 2002Boyom, Keumedjio, et al., 2002Caredda, Marongiu, et al., 2002Cavaleiro, Salgueiro, et al., 2002Cicció and Gómez-Laurito, 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5HP-5DB-1SE-30
Column length (m) 60.30.30.30.50.
Carrier gas HeN2N2H2He
Substrate      
Column diameter (mm) 0.320.250.250.320.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.50.50.40.70.
Tend (C) 200.250.250.245.240.
Heat rate (K/min) 3.4.4.3.4.
Initial hold (min) 6. 5.20. 
Final hold (min)      
I 921.931.930.914.934.
ReferenceCimanga, Apers, et al., 2002Farah, Fechtal, et al., 2002Farah, Fechtal. M., et al., 2002Gancel, Ollé, et al., 2002Iñigo, Palá-Paúl, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RSL-200DB-1SPB-5DB-5DB-5MS
Column length (m) 30.25.60.30.30.
Carrier gas H2HeHeHeHe
Substrate      
Column diameter (mm) 0.320.230.250.250.25
Phase thickness (μm) 0.250.200.250.250.25
Tstart (C) 40.50.50.60.60.
Tend (C) 280.200.240.240.240.
Heat rate (K/min) 6.3.5.3.3.
Initial hold (min) 5.3.3.  
Final hold (min) 5.30.10.  
I 938.934.931.931.928.
ReferenceJirovetz, Buchbauer, et al., 2002Khallouki, Younos, et al., 2002Kim and Lee, 2002Kobaisy, Tellez, et al., 2002Maia, Zoghbi, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101HP-5HP-5OV-101DB-5MS
Column length (m) 25.30.30.50.30.
Carrier gas He  HeHe
Substrate      
Column diameter (mm) 0.320.250.250.20.32
Phase thickness (μm)  0.250.250.50.25
Tstart (C) 50.60.60.50.40.
Tend (C) 200.240.240.250.280.
Heat rate (K/min) 5.3.3.2.4.
Initial hold (min)      
Final hold (min)     5.
I 920.931.932.923.937.
ReferenceMenut, Bessière, et al., 2002Novak, Langbehn, et al., 2002Novak, Langbehn, et al., 2002Orav, Kailas, et al., 2002Phutdhawong, Korth, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5DB-1DB-1DB-1DB-5MS
Column length (m) 30.60.60.50.30.
Carrier gas HeliumHeHeN2He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.25 0.250.250.25
Tstart (C) 60.40.40.60.60.
Tend (C) 250.250.280.240.270.
Heat rate (K/min) 4.4.4.3.3.
Initial hold (min) 2. 5.  
Final hold (min) 20.    
I 931.934.936.913.928.
ReferencePino, Marbot, et al., 2002Sefidkon, Dabiri, et al., 2002Sefidkon, 2002Velasco-Negueruela, Pérez-Alonso, et al., 2002Zoghbi, Andrade, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5DB-1DB-1DB-5MSOV-1
Column length (m) 60.60.60.60.30.
Carrier gas HeHeHeHeH2
Substrate      
Column diameter (mm) 0.320.250.250.250.32
Phase thickness (μm)  0.250.250.250.3
Tstart (C) 40.40.40.35.50.
Tend (C) 220.280.280.250.250.
Heat rate (K/min) 3.4.4.3.3.
Initial hold (min) 5.5.5.5.1.
Final hold (min) 15.   20.
I 934.921.922.930.923.
ReferenceCornu, Carnat, et al., 2001Dabiri and Sefidkon, 2001Dabiri and Sefidkon, 2001Fernando and Grün, 2001Gallori, Bilia, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5RTX-1BP-1CBP-1DB-1
Column length (m) 30.30.50.25.60.
Carrier gas N2N2HeNitrogenHe
Substrate      
Column diameter (mm) 0.250.250.220.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.50.50.
Tend (C) 220.300.230.210.270.
Heat rate (K/min) 5.4.2.3.4.
Initial hold (min) 10.  2. 
Final hold (min)   35.  
I 932.928.922.922.935.
ReferenceGallori, Flamini, et al., 2001Kalemba, Marschall, et al., 2001Lota, de Rocca Serra, et al., 2001Ly, Yamauchi, et al., 2001Mirza, Ahmadi, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-1DB-5DB-5CP Sil 5 CB
Column length (m) 50.30.60.30.25.
Carrier gas HeN2HeH2He
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (μm)  0.25 0.250.39
Tstart (C) 50.80.50.60.60.
Tend (C) 250.225.250.285.220.
Heat rate (K/min) 2.4.3.3.5.
Initial hold (min)   5.  
Final hold (min)      
I 921.917.931.924.926.
ReferenceOrav and Kann, 2001Palá-Paúl, Pérez-Alonso, et al., 2001Rousis, Papadogianni, et al., 2001Santos-Gomes and Fernandes-Ferreira, 2001Sayyah, Kamalinejad, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Sil 5 CBDB-5OV-101OV-101CP Sil 5 CB
Column length (m) 25.30.50.50.25.
Carrier gas NitrogenHeN2N2 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.390.25  0.15
Tstart (C) 60.60.80.80.50.
Tend (C) 220.240.200.200.230.
Heat rate (K/min) 5.3.2.2.3.
Initial hold (min)      
Final hold (min)      
I 926.931.929.929.925.
ReferenceSayyah, Kamalinejad, et al., 2001, 2Tellez M., Estell R., et al., 2001Yang, 2001Yang, 2001, 2Asekun and Ekundayo, 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1RSL-200HP-5DB-5DB-1
Column length (m) 60.60.30.30.25.
Carrier gas N2H2HeHeNitrogen
Substrate      
Column diameter (mm) 0.250.320.250.250.50
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 60.40.80.60.60.
Tend (C) 220.250.200.240.220.
Heat rate (K/min) 3.6.9.3.5.
Initial hold (min) 5.    
Final hold (min) 22. 10.  
I 932.935.921.929.925.
ReferenceBailac, Dellacasa, et al., 2000Jirovetz, Puschmann, et al., 2000Lis-Balchin and Roth, 2000Maia, Zoghbi, et al., 2000Mallavarapu, Rao, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5BP-1HP-5DB-1DB-5
Column length (m) 30.25.30.30.30.
Carrier gas N2N2HeHeHe
Substrate      
Column diameter (mm) 0.220.330.250.250.25
Phase thickness (μm) 0.251.00.250.250.25
Tstart (C) 70.60.60.40.60.
Tend (C) 230.275.275.260.240.
Heat rate (K/min) 4.4.4.2.3.
Initial hold (min) 2.  5. 
Final hold (min) 20.  2. 
I 928.928.929.927.932.
ReferenceMitiku, Sawamura, et al., 2000Mohagheghzadeh, Shams-Ardakani, et al., 2000Mohagheghzadeh, Shams-Ardakani, et al., 2000, 2Senatore, Napolitano, et al., 2000Tellez, Dayan, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1OV-101DB-1DB-5MSRTX-1
Column length (m) 50.52.60.25.30.
Carrier gas  HeliumHeHeN2
Substrate      
Column diameter (mm) 0.20.260.250.250.25
Phase thickness (μm) 0.330.130.250.250.25
Tstart (C) 60.50.50.55.60.
Tend (C) 260.220.230.350.300.
Heat rate (K/min) 4.3.4.4.4.
Initial hold (min)  0. 5. 
Final hold (min)  0.   
I 921.923.930.941.926.
ReferenceChoo, Wong, et al., 1999Dzumayev, Tkachenko, et al., 1999Eikani, Goodarznia, et al., 1999Griffiths, Robertson, et al., 1999Kalemba, 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1OV-101DB-5OV-1CP Sil 5 CB
Column length (m) 25.50.30.25.25.
Carrier gas HeN2 H2He
Substrate      
Column diameter (mm) 0.250.20.320.250.25
Phase thickness (μm) 0.25 1.0.25 
Tstart (C) 50.80.40.40.50.
Tend (C) 290.200.200.220.230.
Heat rate (K/min) 4.1.3.3.3.
Initial hold (min)   5.5. 
Final hold (min)  20. 5. 
I 925.935.928.922.934.
ReferenceKoulman, 1999Menon, Chacko, et al., 1999Meynier, Novelli, et al., 1999Oberhofer, Nikiforov, et al., 1999Oyedeji, Olawore, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1OV-101SE-30BP-1CP Sil 5 CB
Column length (m) 50.50.30.25.25.
Carrier gas HeHeHeliumN2He
Substrate      
Column diameter (mm) 0.250.250.250.50.25
Phase thickness (μm) 0.250.250.20 0.39
Tstart (C) 70.70.60.60.60.
Tend (C) 240.220.200.220.220.
Heat rate (K/min) 4.2.3.5.5.
Initial hold (min)  5.4. 5.
Final hold (min)    10.20.
I 917.912.925.925.927.
ReferencePalá-Paúl, Pérez-Alonso, et al., 1999Pateira, Nogueira, et al., 1999Prikhod'ko, Klyuev, et al., 1999Rao, Bhattacharya, et al., 1999Rustaiyan, Masoudi, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-1DB-5DB-1DB-1
Column length (m) 25.60.30.60.60.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.390.250.250.25 
Tstart (C) 60.40.40.50.60.
Tend (C) 220.280.220.220.230.
Heat rate (K/min) 5.4.4.4.3.
Initial hold (min)  5.5.  
Final hold (min)     5.
I 926.924.923.931.926.
ReferenceRustaiyan and Nadji, 1999Sefidkon, Dabiri, et al., 1999Sefidkon and Khajavi, 1999Sefidkon and Mirza, 1999Shafiee, Javidnia, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5SPB-5CP Sil 5 CBOV-101DB-5MS
Column length (m) 30.60.25.25.30.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.250.32 0.200.25
Phase thickness (μm) 0.251.0.39 0.25
Tstart (C) 60.40.60.80.60.
Tend (C) 240.200.220.240.240.
Heat rate (K/min) 3.3.5.6.3.
Initial hold (min)  5.   
Final hold (min)  2.   
I 931.933.928.921.929.
ReferenceTellez, Canel, et al., 1999Viallon C., Verdier-Metz I., et al., 1999Weyerstahl, Marschall, et al., 1999Zenkevich, Kosman, et al., 1999Zoghbi, Andrade, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5SE-30HP-5HP-1OV-101
Column length (m) 50.25.25.60.25.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.320.20.20.250.32
Phase thickness (μm) 0.25 0.330.25 
Tstart (C) 60.60.70.50.50.
Tend (C) 240.180.290.280.200.
Heat rate (K/min) 3.3.3.4.5.
Initial hold (min)  10.8.5. 
Final hold (min) 20. 20.  
I 928.926.934.927.930.
ReferenceDoneanu and Anitescu, 1998Jantan, Ahmad, et al., 1998Poiana, Sicari, et al., 1998Stashenko, Cervantes, et al., 1998Zollo, Biyiti, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-SulfurSPB-SulfurDB-1DB-5DB-5
Column length (m) 30.30. 30.30.
Carrier gas HeHe HeliumHe
Substrate      
Column diameter (mm) 0.320.32 0.250.25
Phase thickness (μm) 4.4. 0.25 
Tstart (C) 45.45.80.60.60.
Tend (C) 240.240.220.240.240.
Heat rate (K/min) 5.5.6.3.4.
Initial hold (min) 13.13.   
Final hold (min) 5.5.   
I 934.934.924.931.931.
ReferenceMariaca, Berger, et al., 1997Mariaca, Berger, et al., 1997Salgueiro, Vila, et al., 1997Tellez, Estell, et al., 1997Zunino, Novillo-Newton, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1OV-101OV-101DB-5DB-1
Column length (m) 23.50.50.30.60.
Carrier gas HeN2He He
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.170.17  0.25
Tstart (C) 60.50.50.40.50.
Tend (C) 250.220.250.210.250.
Heat rate (K/min) 5.5.2.2.2.5
Initial hold (min) 3.  2.5.
Final hold (min) 30.  33. 
I 921.933.922.934.927.
ReferenceAyedoun, Adeoti, et al., 1996Chacko, Jayalekshmy, et al., 1996Orav, Kailas, et al., 1996Sohounhloue, Dangou, et al., 1996Stashenko, Puertas, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1DB-1DB-1OV-1HP-101
Column length (m) 50.60.60.50.50.
Carrier gas HeHeHeN2H2
Substrate      
Column diameter (mm) 0.20.250.250.270.32
Phase thickness (μm) 0.330.250.250.20.3
Tstart (C) 40.70.70.80.65.
Tend (C) 200.270.270.240.300.
Heat rate (K/min) 3.2.52.53.2.
Initial hold (min) 3.5.5. 5.
Final hold (min) 30.    
I 923.924.924.923.921.
ReferenceWong and Lai, 1996Tirado, Stashenko, et al., 1995Tirado, Stashenko, et al., 1995Ramanoelina, Viano, et al., 1994Demarne and van der Walt, 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Methyl SiliconeMethyl SiliconeCP Sil 5 CBMethyl SiliconeSE-54
Column length (m) 50.50.25.25.30.
Carrier gas N2N2  Hydrogen
Substrate      
Column diameter (mm) 0.250.250.250.500.25
Phase thickness (μm) 0.170.17  0.25
Tstart (C) 80.80.60.60.60.
Tend (C) 200.200.280.220.250.
Heat rate (K/min) 2.3.5.5.2.
Initial hold (min)     5.
Final hold (min)     2.
I 938.931.927.928.927.
ReferenceGopalakrishnan, Menon, et al., 1993Gopalakrishnan, Menon, et al., 1993Kaul, Singh, et al., 1993Mallavarapu, Ramesh, et al., 1993Kollmannsberger, Nitz, et al., 1992
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1OV-101OV-101BP-1OV-101
Column length (m) 30.50.50.50.50.
Carrier gas N2N2N2H2N2
Substrate      
Column diameter (mm)  0.250.250.300.25
Phase thickness (μm)      
Tstart (C) 80.80.80.40.80.
Tend (C) 220.200.200.250.200.
Heat rate (K/min) 4.2.2.10.2.
Initial hold (min)    1. 
Final hold (min)      
I 920.929.930.926.931.
ReferenceVelasco-Negueruela, Pérez Alonso, et al., 1991Yang and Sugisawa, 1990Yang and Sugisawa, 1990Brophy, Davies, et al., 1989Sugisawa, Yang, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-1OV-101OV-101OV-1
Column length (m) 50.60.50.50.40.
Carrier gas N2Helium  He
Substrate      
Column diameter (mm) 0.250.500.300.300.5
Phase thickness (μm)  1.2  0.75
Tstart (C) 80.40.40.40.30.
Tend (C) 200.220.230.230.220.
Heat rate (K/min) 2.2.3.53.53.
Initial hold (min)   5.5. 
Final hold (min)      
I 938.921.924.930.921.
ReferenceSugisawa, Yang, et al., 1989Wahab, Aboutabl, et al., 1987Nykanen, 1986Nykanen, 1986de Pooter, de Buyck, et al., 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase OV-1OV-101OV-101
Column length (m)  30.30.
Carrier gas HeHeHe
Substrate    
Column diameter (mm)  0.50.5
Phase thickness (μm)  0.80.8
Tstart (C) 40.40.40.
Tend (C) 220.220.220.
Heat rate (K/min) 2.2.2.
Initial hold (min)    
Final hold (min)    
I 921.921.921.
ReferenceDe Pooter, De Buyck, et al., 1986De Pooter and Schamp, 1986De Pooter and Schamp, 1986
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Cicció and Gómez-Laurito, 2002
Cicció, J.F.; Gómez-Laurito, J., Volatile constituents of the leaves of Siparuna thecaphora (Siparunaceae) from Turrialba, Costa Rica, Rev. Biol. Trop., 2002, 50, 3/4, 963-967. [all data]

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Fernando and Grün, 2001
Fernando, L.N.; Grün, I.U., Headspace-SPME analysis of volatiles of the ridge gourd (Luffa acutangula) and bitter gourd (Momordica charantia) flowers, Flavour Fragr. J., 2001, 16, 4, 289-293, https://doi.org/10.1002/ffj.999 . [all data]

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Asekun and Ekundayo, 2000
Asekun, O.T.; Ekundayo, O., Essential oil constituents of Hyptis suaveolens (L.) Poit. (Bush tea) leaves from Nigeria, J. Essent. Oil Res., 2000, 12, 227-230. [all data]

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Lis-Balchin and Roth, 2000
Lis-Balchin, M.; Roth, G., Composition of the essential oils of Pelargonium odoratissimum, P. exstipulatum, and P. x fragrans (Geraniaceae) and their bioactivity, Flavour Fragr. J., 2000, 15, 6, 391-394, https://doi.org/10.1002/1099-1026(200011/12)15:6<391::AID-FFJ929>3.0.CO;2-W . [all data]

Maia, Zoghbi, et al., 2000
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Tellez, Dayan, et al., 2000
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Choo, L.-C.; Wong, S.-M.; Liew, K.-Y., Essential oil of nutmeg pericarp, J. Sci. Food Agric., 1999, 79, 13, 1954-1957, https://doi.org/10.1002/(SICI)1097-0010(199910)79:13<1954::AID-JSFA460>3.0.CO;2-I . [all data]

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Koulman, 1999
Koulman, A., Podophyllotoxin: a study of biosynthesis, evolution, function, and use of podophyllotoxin and related lignans, University Library Groningen, Nederlands, 1999, 188, retrieved from http://www.ub.rug.nl/eldoc/dis/science/a.koulman/. [all data]

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Rustaiyan and Nadji, 1999
Rustaiyan, A.; Nadji, K., Composition of the essential oils of Nepeta ispahanica Boiss. and Nepeta binaludensis Jamzad from Iran, Flavour Fragr. J., 1999, 14, 1, 35-37, https://doi.org/10.1002/(SICI)1099-1026(199901/02)14:1<35::AID-FFJ776>3.0.CO;2-N . [all data]

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Sefidkon and Khajavi, 1999
Sefidkon, F.; Khajavi, M.S., Chemical composition of the essential oils of two Salvia species from Iran: Salvia verticillata L. and Salvia santolinifolia Boiss., Flavour Fragr. J., 1999, 14, 2, 77-78, https://doi.org/10.1002/(SICI)1099-1026(199903/04)14:2<77::AID-FFJ726>3.0.CO;2-9 . [all data]

Sefidkon and Mirza, 1999
Sefidkon, F.; Mirza, M., Chemical composition of the essential oils of two Salvia species from Iran, Salvia virgata Jacq. and Salvia syriaca L., Flavour Fragr. J., 1999, 14, 1, 45-46, https://doi.org/10.1002/(SICI)1099-1026(199901/02)14:1<45::AID-FFJ774>3.0.CO;2-S . [all data]

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Notes

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