Ethinyl estradiol, 2TMS derivative


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryUltra-22842.Daeseleire, de Guesquiere, et al., 199125. m/0.2 mm/0.33 μm, He, 5. K/min, 280. C @ 10. min; Tstart: 200. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryVF-5MS2815.3Tret'yakov, 200730. m/0.25 mm/0.25 μm, He; Program: Multi-step temperature program; T(initial)=60C; T(final)=270C

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Daeseleire, de Guesquiere, et al., 1991
Daeseleire, E.; de Guesquiere, A.; van Peteghem, C., Derivatization and gas chromatographic-mass spectrometric detection of anabolic steroid residues isolated from edible muscle tissue, J. Chromatogr., 1991, 562, 1-2, 673-679, https://doi.org/10.1016/0378-4347(91)80617-L . [all data]

Tret'yakov, 2007
Tret'yakov, K.V., Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2007. [all data]


Notes

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