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Androsta-3,5-diene, 3,17«beta»-bis(trimethylsiloxy)-


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-12652.Schänzer, Horning, et al., 199517. m/0.2 mm/0.11 «mu»m, He, 5. K/min; Tstart: 180. C; Tend: 320. C

Normal alkane RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillaryOV-101240.2671.Krupcik, Rutten, et al., 1976Column length: 30. m; Column diameter: 0.25 mm
CapillaryOV-101251.2691.Krupcik, Rutten, et al., 1976Column length: 30. m; Column diameter: 0.25 mm

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-12696.Bowers and Borts, 199630. m/0.25 mm/0.1 «mu»m, He; Program: 170C => 20C/min => 260C => 2.7C/min => 305C => 20C/min => 320C
CapillaryBPX-52699.Bowers and Borts, 199630. m/0.22 mm/0.25 «mu»m, He; Program: 170C => 20C/min => 260C => 2.7C/min => 305C => 20C/min => 320C

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Schänzer, Horning, et al., 1995
Schänzer, W.; Horning, S.; Donike, M., Metabolism of anabolic steroids in humans: Synthesis of 6«beta»-hydroxy metabolites of 4-chloro-1,2-dehydro-17«alpha» -methyltestosterone, fluoxymesterone, and metandienone, Steroids, 1995, 60, 4, 353-366, https://doi.org/10.1016/0039-128X(95)00008-E . [all data]

Krupcik, Rutten, et al., 1976
Krupcik, J.; Rutten, G.A.F.M.; Rijks, J.A., The influence of temperature on the separation and characterization of steroids on non-polar glass capillary columns, Chem. zvesti, 1976, 30, 4, 469-479. [all data]

Bowers and Borts, 1996
Bowers, L.D.; Borts, D.J., Separation and confirmation of anabolic steroids with quadrupole ion trap tandem mass spectrometry, J. Chromatogr. B, 1996, 687, 1, 69-78, https://doi.org/10.1016/S0378-4347(96)00231-9 . [all data]


Notes

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