Aceturic acid, TMS derivative


Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryPackedPacked
Active phase CP Sil 5 CBOV-1OV-1
Column length (m)  2.1.8
Carrier gas N2N2N2
Substrate  Anakrom100-120 mesh
Column diameter (mm)    
Phase thickness (μm)    
Tstart (C) 60.80.70.
Tend (C) 280. 290.
Heat rate (K/min) 6.4.28.
Initial hold (min) 0.5 0.5
Final hold (min) 5.  
I 1253.1253.1253.
ReferenceWurth, Kumps, et al., 1989Ramsdell and Tanaka, 1980Tanaka, Hine, et al., 1980
Comment MSDC-RI MSDC-RI MSDC-RI

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Wurth, Kumps, et al., 1989
Wurth, C.; Kumps, A.; Mardens, Y., Urinary organic acids: Retention indices on two capillary gas chromatography columns, J. Chromatogr., 1989, 491, 186-192, https://doi.org/10.1016/S0378-4347(00)82831-5 . [all data]

Ramsdell and Tanaka, 1980
Ramsdell, H.S.; Tanaka, K., Gas chromatographic retention indices of twenty metabolically important acylglycines as trimethylsilyl derivatives, J. Chromatogr., 1980, 181, 1, 90-94, https://doi.org/10.1016/S0378-4347(00)81273-6 . [all data]

Tanaka, Hine, et al., 1980
Tanaka, K.; Hine, D.G.; West-Dull, A.; Lynn, T.B., Gas-chromatographic method of analysis for urinary organic acids. I. Retention indices of 155 metabolically important compounds, Clin. Chem., 1980, 26, 13, 1839-1846. [all data]


Notes

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