p-Anisic acid, TMS derivative


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryVF-5MS1531.Todua, 201130. m/0.25 mm/0.25 μm, He; Tstart: 60. C; Tend: 270. C
CapillaryDB-51528.Jaroszynska and Ligor, 200530. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 320. C
CapillaryDB-51529.Jaroszynska and Ligor, 200530. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 320. C
CapillaryDB-51530.Jaroszynska and Ligor, 200530. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 320. C
CapillaryDB-51530.Jaroszynska and Ligor, 200530. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 320. C
CapillaryPE-5ht1522.Jaroszynska and Ligor, 200530. m/0.25 mm/0.1 μm, He, 3. K/min; Tstart: 50. C; Tend: 320. C
CapillaryPE-5ht1522.Jaroszynska and Ligor, 200530. m/0.25 mm/0.1 μm, He, 3. K/min; Tstart: 50. C; Tend: 320. C
CapillaryPE-5ht1522.Jaroszynska and Ligor, 200530. m/0.25 mm/0.1 μm, He, 3. K/min; Tstart: 50. C; Tend: 320. C
CapillaryPE-5ht1523.Jaroszynska and Ligor, 200530. m/0.25 mm/0.1 μm, He, 3. K/min; Tstart: 50. C; Tend: 320. C
CapillaryPE-5ms1519.Jaroszynska and Ligor, 200530. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 320. C
CapillaryPE-5ms1520.Jaroszynska and Ligor, 200530. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 320. C
CapillaryDB-51524.Jaroszynska, 200330. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 240. C
CapillaryDB-51530.Jaroszynska, 200330. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 240. C
CapillaryDB-51527.Jaroszynska, 200330. m/0.25 mm/0.25 μm, He, 7. K/min; Tstart: 50. C; Tend: 240. C
CapillaryDB-51534.Jaroszynska, 200330. m/0.25 mm/0.25 μm, He, 7. K/min; Tstart: 50. C; Tend: 240. C
PackedOV-11504.Butts, 1972He, Chromosorb W HP (80-100 mesh), 10. K/min; Column length: 2. m; Tstart: 100. C; Tend: 325. C

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-51526.Isidorov, Kotowska, et al., 200530. m/0.25 mm/0.25 μm, He, 5. K/min; Tstart: 50. C; Tend: 300. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryOV-1, SE-30, Methyl silicone, SP-2100, OV-101, DB-1, etc.1495.Waggott and Davies, 1984Hydrogen; Column length: 50. m; Column diameter: 0.32 mm; Program: not specified

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Todua, 2011
Todua, N.G., Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2011. [all data]

Jaroszynska and Ligor, 2005
Jaroszynska, J.; Ligor, T., The identification of phenolic compounds by a gas chromatographic method on three capillary columns with the same non-polar stationary phase, Anal. Chim. Acta., 2005, 539, 1-2, 11-15, https://doi.org/10.1016/j.aca.2005.03.024 . [all data]

Jaroszynska, 2003
Jaroszynska, J., Isolation of free phenolic compounds from arboreal leaves by use of the Florisil/C18 system, Anal. Bioanal. Chem., 2003, 377, 4, 702-708, https://doi.org/10.1007/s00216-003-2155-z . [all data]

Butts, 1972
Butts, W.C., Two-Column Gas Chromatography of Trimethylsilyl Derivatives of Biochemically Significant Compounds, Anal. Biochemistry, 1972, 46, 1, 187-199, https://doi.org/10.1016/0003-2697(72)90411-3 . [all data]

Isidorov, Kotowska, et al., 2005
Isidorov, V.A.; Kotowska, U.; Vinogorova, V.T., GC Identification of organic compounds based on partition coefficients of their TMS derivatives in a hexane-acetonitrile system and retention indices, Anal. Sci., 2005, 21, 12, 1483-1489, https://doi.org/10.2116/analsci.21.1483 . [all data]

Waggott and Davies, 1984
Waggott, A.; Davies, I.W., Identification of organic pollutants using linear temperature programmed retention indices (LTPRIs) - Part II, 1984, retrieved from http://dwi.defra.gov.uk/research/completed-research/reports/dwi0383.pdf. [all data]


Notes

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