4-Aminobenzoic acid, 2TMS derivative
- Formula: C13H23NO2Si2
- Molecular weight: 281.4982
- IUPAC Standard InChI: InChI=1S/C13H23NO2Si2/c1-17(2,3)14-12-9-7-11(8-10-12)13(15)16-18(4,5)6/h7-10,14H,1-6H3
- IUPAC Standard InChIKey: UNEXFOGMEVUYSY-UHFFFAOYSA-N
- CAS Registry Number: 18406-05-8
- Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript. - Other names: Benzoic acid, 4-[(trimethylsilyl)amino]-, trimethylsilyl ester; Benzoic acid, p-[(trimethylsilyl)amino]-, trimethylsilyl ester; p-Aminobenzoic acid (tms); 4-Aminobenzoic acid, TMS; Benzoic acid, 4-amino, TMS; 4-Aminobenzoic acid, N-(trimethylsilyl)-, trimethylsilyl ester; Trimethylsilyl 4-[(trimethylsilyl)amino]benzoate
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Van Den Dool and Kratz RI, non-polar column, temperature ramp
Go To: Top, References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
| Column type | Capillary | Packed |
|---|---|---|
| Active phase | VF-5MS | OV-1 |
| Column length (m) | 30. | 2. |
| Carrier gas | He | He |
| Substrate | Chromosorb W HP (80-100 mesh) | |
| Column diameter (mm) | 0.25 | |
| Phase thickness (μm) | 0.25 | |
| Tstart (C) | 60. | 100. |
| Tend (C) | 270. | 325. |
| Heat rate (K/min) | 10. | |
| Initial hold (min) | ||
| Final hold (min) | ||
| I | 1836. | 1813. |
| Reference | Todua, 2011 | Butts, 1972 |
| Comment | MSDC-RI | MSDC-RI |
References
Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Todua, 2011
Todua, N.G.,
Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2011. [all data]
Butts, 1972
Butts, W.C.,
Two-Column Gas Chromatography of Trimethylsilyl Derivatives of Biochemically Significant Compounds,
Anal. Biochemistry, 1972, 46, 1, 187-199, https://doi.org/10.1016/0003-2697(72)90411-3
. [all data]
Notes
Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References
- Symbols used in this document:
Tend Final temperature Tstart Initial temperature - Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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