Benzene, 1,2,4-trichloro-

Data at NIST subscription sites:

NIST subscription sites provide data under the NIST Standard Reference Data Program, but require an annual fee to access. The purpose of the fee is to recover costs associated with the development of data collections included in such sites. Your institution may already be a subscriber. Follow the links above to find out more about the data in these sites and their terms of usage.


Van Den Dool and Kratz RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5DB-5DB-1
Column length (m) 60.60.60.60.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.320.320.320.25
Phase thickness (μm) 1.1.1.1.0.25
Tstart (C) 60.60.60.60.40.
Tend (C) 180.180.180.180.325.
Heat rate (K/min) 3.3.4.4.3.
Initial hold (min) 2.82.82.82.8 
Final hold (min)      
I 1192.671193.061196.721196.781141.6
ReferenceHarangi, 2003Harangi, 2003Harangi, 2003Harangi, 2003Sun and Stremple, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1DB-5DB-5DB-5DB-1
Column length (m)  30.30.30.30.
Carrier gas  N2N2N2N2
Substrate      
Column diameter (mm)  0.530.530.530.235
Phase thickness (μm)  1.51.51.50.25
Tstart (C) 35.50.50.50.100.
Tend (C) 300.    
Heat rate (K/min) 8.2.2.2.10.
Initial hold (min)     0.
Final hold (min)      
I 1158.51160.141166.231171.691168.
ReferenceGautzsch and Zinn, 1996Gerbino, Garbarino, et al., 1996Gerbino, Garbarino, et al., 1996Gerbino, Garbarino, et al., 1996Gerbino and Castello, 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1DB-1Petrocol DH
Column length (m) 30.30.30.100.
Carrier gas N2N2N2He
Substrate     
Column diameter (mm) 0.2350.2350.2350.25
Phase thickness (μm) 0.250.250.250.5
Tstart (C) 100.50.50.30.
Tend (C)    220.
Heat rate (K/min) 5.10.5.1.
Initial hold (min) 0.0.0. 
Final hold (min)     
I 1162.1157.1150.1152.
ReferenceGerbino and Castello, 1995Gerbino and Castello, 1995Gerbino and Castello, 1995White, Hackett, et al., 1992
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Harangi, 2003
Harangi, J., Short communication. Retention index calculation without n-alkanes -- the virtual carbon number, J. Chromatogr. A, 2003, 993, 1-2, 187-195, https://doi.org/10.1016/S0021-9673(03)00320-0 . [all data]

Sun and Stremple, 2003
Sun, G.; Stremple, P., Retention index characterization of flavor, fragrance, and many other compounds on DB-1 and DB-XLB, 2003, retrieved from http://www.chem.agilent.com/cag/cabu/pdf/b-0279.pdf. [all data]

Gautzsch and Zinn, 1996
Gautzsch, R.; Zinn, P., Use of incremental models to estimate the retention indexes of aromatic compounds, Chromatographia, 1996, 43, 3/4, 163-176, https://doi.org/10.1007/BF02292946 . [all data]

Gerbino, Garbarino, et al., 1996
Gerbino, T.C.; Garbarino, G.; Petit-Bon, P., Programmed temperature retention indices: calculation of linear programmed temperature retention indices of halogenated benzenes from isothermal data, Ann. Chim. (Rome), 1996, 86, 63-75. [all data]

Gerbino and Castello, 1995
Gerbino, T.C.; Castello, G., Prediction of programmed temperature retention indices on capillary columns of different polarities, J. Chromatogr. A, 1995, 699, 1-2, 161-171, https://doi.org/10.1016/0021-9673(95)00024-H . [all data]

White, Hackett, et al., 1992
White, C.M.; Hackett, J.; Anderson, R.R.; Kail, S.; Spock, P.S., Linear temperature programmed retention indices of gasoline range hydrocarbons and chlorinated hydrocarbons on cross-linked polydimethylsiloxane, J. Hi. Res. Chromatogr., 1992, 15, 2, 105-120, https://doi.org/10.1002/jhrc.1240150211 . [all data]


Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References