1-Octanol

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Normal alkane RI, polar column, custom temperature program

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxSupelco CO Wax-10Supelco CO Wax-10Supelco CO Wax-10DB-Wax
Column length (m) 60.60.60.60.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.200.320.320.320.25
Phase thickness (μm) 0.250.250.250.250.25
Program 40 0C (3 min) 2 0C/min -> 150 0C 4 0C/min -> 220 0C (20 min) 5 0C/min -> 230 0C35 0C (6 min) 2 0C/min -> 60 0C (5 min) 5 0C/min -> 200 0C 25 0C/min -> 250 0C (6 min)not specifiednot specifiednot specified
I 1561.1555.1563.1570.1557.
ReferenceGyawali and Kim, 2012Prompona, Kandylis, et al., 2012Prompona, Kandylis, et al., 2012Prompona, Kandylis, et al., 2012Welke, Manfroi, et al., 2012
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxSOLGel-WaxSOLGel-WaxDB-WaxSupelko CO Wax
Column length (m) 30.30.30.30.60.
Carrier gas HeliumHeliumHeliumHydrogenHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.250.250.250.25
Program not specified40 0C (2 min) 5 0C/min -> 140 0C 10 0C/min -> 250 0C (3 min)not specified35 0C (9 min) 5 0C/min -> 80 0C 1 0C/min -> 100 0C 16 0C/min -> 210 0C (20 min) 
I 1558.1568.1561.1566.1561.
ReferenceWelke, Manfroi, et al., 2012Johanningsmeier and McFeeters, 2011Johanningsmeier and McFeeters, 2011Sampaio, Garruti, et al., 2011Vekiari, Orepoulou, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelko CO WaxSupelko CO WaxDB-WaxDB-WaxDB-Wax
Column length (m) 60.60.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.320.320.250.250.32
Phase thickness (μm) 0.250.250.250.250.50
Program 40 0C (5 min) 4 0C/min -> 75 0C 5 0C/min -> 250 0C (10 min)not specified40 0C (4 min) 2.5 0C/min -> 80 0C 5 0C/min -> 110 0C 10 0C/min -> 220 0C (5 min)not specified40 0C 7 0C/min -> 110 0C 15 0C/min -> 250 0C (3 min)
I 1564.1562.1566.1565.1568.
ReferenceVekiari, Orepoulou, et al., 2010Vekiari, Orepoulou, et al., 2010Canuti, Conversano, et al., 2009Canuti, Conversano, et al., 2009Valappil, Fan, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxCP-Wax 52 CBDB-WaxDB-WaxSupelcowax-10
Column length (m) 30.50.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHe
Substrate      
Column diameter (mm) 0.250.250.320.320.25
Phase thickness (μm) 0.250.290.250.250.25
Program not specified33 0C (1 min) 2 0C/min -> 130 0C 10 0C/min -> 220 0C50 0C 20 0C/min -> 80 0C 3 0C/min -> 230 0C40 0C (4 min) 3 0C/min -> 50 0C 5 0C/min -> 120 0C 7 0C/min -> 175 0C 10 0C/min -> 230 0C (8 min)40C(10min) => 2C/min => 200C(1min) => 2C/min => 250C (10min)
I 1559.1540.1548.1605.1561.
ReferenceZhao, Xu, et al., 2009Kaack and Christensen, 2008Tao, Wenlai, et al., 2008Yongsheng, Hua, et al., 2008Bosch-Fuste, Riu-Aumatell, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase AquaWaxDB-WaxHP Innowax FSPDB-WaxSupelcowax-10
Column length (m)  30.60.30.30.
Carrier gas  HydrogenN2HeHe
Substrate      
Column diameter (mm)  0.320.250.250.25
Phase thickness (μm)  0.500.250.250.25
Program not specified60 0C (3 min) 2 0C/min -> 220 0C 3 0C/min -> 245 0C (20 min)60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C50 0C (2 min) 6 0C/min -> 150 0C 8 0C/min -> 230 0C (15 min)40C(3min) => 4C/min => 75C => 8C/min => 250C(5min)
I 1574.1543.1562.1557.1563.
ReferenceLiolios, Laouer, et al., 2007Selli, 2007Tabanca N., Demirci B., et al., 2007Tian, Zhang, et al., 2007Vichi, Guadayol, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Innowax FSCInnowax FSCInnowax FSCHP-InnowaxHP-Innowax FSC
Column length (m) 60.60.60.60.60.
Carrier gas HeHeHeNitrogenN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 60C(10min) => 4C/min => 220C (10min) => 1C/min => 240C60C(10min) => 4C/min >220C (10min) => 1C/min => 240C60C(10min) => 4C/min >220C (10min) => 1C/min => 240C50 0C (4 min) -> 40 0C 4 0C/min -> 220 0C60C(10min) => 4C/min => 220C => (10min) => 1C/min => 240C
I 1562.1562.1562.1550.1562.
ReferenceBaser K.H.C., Ozek G., et al., 2006Baser, Özek, et al., 2006Baser, Özek, et al., 2006Quijano and Pino, 2006Tabanca, Demirci, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxCarbowax 20MCarbowax 20MInnowax FSCHP-Innowax FSC
Column length (m) 30.  60.60.
Carrier gas He  HeHe
Substrate      
Column diameter (mm) 0.25  0.250.25
Phase thickness (μm) 0.25  0.250.25
Program not specifiednot specifiednot specified60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
I 1536.1538.1539.1562.1562.
ReferenceBerlinet, Ducruet, et al., 2005Editorial paper, 2005Editorial paper, 2005Kosar, Özek, et al., 2005Sezik E., Kocakulak E., et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP Innowax FSPInnowax FSCCarbowax 20MFFAPHP-Innowax FSC
Column length (m) 60.60. 30.60.
Carrier gas N2He  He
Substrate      
Column diameter (mm) 0.250.25 0.320.25
Phase thickness (μm) 0.250.25 0.250.25
Program 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240Cnot specified35C (2min) => 40C/min => 60C (2min) => 6C/min => 180C => 10C/min => 230C (10min60C (10min) => 4C/min => 220C (10min) => 1C/min => 240C
I 1562.1562.1551.1549.1562.
ReferenceAltintas, Kose, et al., 2004Baser, Özek, et al., 2004Vinogradov, 2004Buettner, Mestres, et al., 2003Demirci, Baser, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-Innowax FSCPEG-20MCarbowax 20MDB-WaxHP Innowax FSP
Column length (m) 60.30. 30.60.
Carrier gas He  HeHe
Substrate      
Column diameter (mm) 0.250.25 0.320.25
Phase thickness (μm) 0.250.25 0.50.25
Program 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C50C(8min) => 4C/min => 110C => 16C/min => 200Cnot specified60C(2min) => 2C/min => 220C => 3C/min => 245C(20min)60C(10min) => 4C/min => 220C (10min) => 1C/min => 240C
I 1562.1567.1519.1556.1562.
ReferenceErdemoglu, Sener, et al., 2003Garruti, Franco, et al., 2003Krings, Banavara, et al., 2003Selli, Cabaroglu, et al., 2003Tasdemir, Demirci, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-InnowaxHP-InnowaxHP-Innowax FSCHP-Innowax FSCNukol
Column length (m) 60.60.60.60.25.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.25 
Program 60 0C (10 min) 4 K/min -> 220 0C (10 min) 1 K/min -> 240 0C60 0C (10 min) 10 K/min -> 220 0C (10 min) 1K/min -> 240 0C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C45C(5min) => 20C/min => 100C(1min) => 3C/min => 190C(40min)
I 1562.1562.1562.1562.1549.
ReferenceBaser, Demirci, et al., 2002Baser, Demirci, et al., 2001Kirimer N., Tabanea N., et al., 2001Kivcak B., Mert T., et al., 2001López and Dufour, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxInnowax FSCHP-Innowax FSCHP-InnowaxInnowax
Column length (m) 30.60.60.60.60.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 25 0C (0.5 min) 50 K/min -> 50 0C 3.5 K/min -> 150 0C 7.5 K/min -> 240 0C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60 0C (10 min) 4 K/min -> 220 0C (10 min) 1 K/min -> 240 0C
I 1519.1562.1562.1562.1562.
ReferenceMiranda, Nogueira, et al., 2001Saglam, Gozler, et al., 2001Tabanca, Kirimer, et al., 2001Tabanca, Kirimer, et al., 2001, 2Baser, Özek, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Innowax FSCInnowax FSCCP-Wax 52CBDB-WaxSupelcowax-10
Column length (m) 60.60.50.60.30.
Carrier gas HeHeliumHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.250.2 0.25
Program 60C(10 min) => 4C/min => 220C(10min) => 1C/min => 240C60 0C (10 min) 4 0C/min -> 220 0C (10 min) 1 0C/min -> 240 0C30C (1.5min) => 3C/min => 120C => 10C/min => 220C (3.5min)45C(4min) => 30C/min => 60C (5min) => 3C/min => 220C(40min)50C(2min) => 7C/min => 140C => 17.5C/min => 230C
I 1562.1562.1548.1568.1519.
ReferenceKirimer, Tabanca, et al., 2000Kirimer, Tabanca, et al., 1999Jakobsen, Hansen, et al., 1998Ziegleder, 1998Chang, Seitz, et al., 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Wax 52 CBCarbowax 20MSupelcowax-10NB-351DB-Wax
Column length (m) 50.60.30.25. 
Carrier gas  He   
Substrate      
Column diameter (mm) 0.320.250.250.32 
Phase thickness (μm) 0.200.25 0.2 
Program 50 0C (10 min) 2 0C/min -> 100 0C 5 0C/min -> 150 0C 7 0C/min -> 220 0C (20 min)not specifiednot specified40C(5min) => 4C/min => 150C => 8C/min => 240C(12min)not specified
I 1553.1507.1554.1573.1573.
ReferencePatterson and Stevenson, 1995Tirado, Stashenko, et al., 1995Jean, Garneau, et al., 1993Kerrola and Kallio, 1993Peng, Yang, et al., 1991
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxCarbowax 20MCarbowax 20M
Column length (m) 60.60.  
Carrier gas     
Substrate     
Column diameter (mm) 0.320.32  
Phase thickness (μm)     
Program not specifiednot specifiednot specifiednot specified
I 1557.1557.1519.1513.
ReferenceBinder, Flath, et al., 1989Binder and Flath, 1989Shibamoto, 1987Ramsey and Flanagan, 1982
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Gyawali and Kim, 2012
Gyawali, R.; Kim, K.-S., Bioactive volatile compounds of three medicinal plants from Nepal, Kathmandu Univ. J. Sci., Engineering and Technol., 2012, 8, 1, 51-62. [all data]

Prompona, Kandylis, et al., 2012
Prompona, K.-D.; Kandylis, P.; Tsakiris, A.; Kanellaki, M.; Kourkoutas, Y., Application of alternative technologies for elimination of artificial colorings in alcoholic beverages produced by Citrus medica and potential impact on human health, Food Nutrition Sci., 2012, 3, 07, 959-969, https://doi.org/10.4236/fns.2012.37127 . [all data]

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Welke, J.E.; Manfroi, V.; Zanus, M.; Lazarotto, M.; Zini, C.A., Characterization of the volatile profile of Brazilian merlot wines through comprehensive two dimensional gas chromatography time-of-flight mass spectrometric detection, J. Chromatogr. A, 2012, 1226, 124-139, https://doi.org/10.1016/j.chroma.2012.01.002 . [all data]

Johanningsmeier and McFeeters, 2011
Johanningsmeier, S.D.; McFeeters, R.F., Detection of volatile spoilage metabolites in fermented cucumbers using nontargeted, comprehensive 2-dimensional gas chromatography-time-of-flight mass spectrometry (GCxGCxTOFMS), J. Food Sci., 2011, 76, 1, c168-c177, https://doi.org/10.1111/j.1750-3841.2010.01918.x . [all data]

Sampaio, Garruti, et al., 2011
Sampaio, K.S.; Garruti, D.S.; Franco, M.R.B.; Janzantti, N.S.; Da Silva, M.A.AP., Aroma volatiles recovered in the water phase of cashew apple (Anacardium occidentale L.) juice during concentration, J. Sci. Food Agric., 2011, 91, 10, 1801-1809, https://doi.org/10.1002/jsfa.4385 . [all data]

Vekiari, Orepoulou, et al., 2010
Vekiari, S.A.; Orepoulou, V.; Kourkoutas, Y.; Kamoun, N.; Msallem, M.; Psimouli, V.; Arapoglou, D., Characterization and seasonal variations of the quality of virgin olive oil of the Thoumbolia and Koroneiki varieties from Southern Greece, Grasas y Aceites, 2010, 61, 3, 221-231, https://doi.org/10.3989/gya.108709 . [all data]

Canuti, Conversano, et al., 2009
Canuti, V.; Conversano, M.; Li Calzi, M.; Heymann, H.; Matthews, M.A.; Ebeler, S.E., Headspace solid-phase microextraction - gas chromatography - mass spectrometry for profiling free volatile compounds in Cabernet Sauvignon grapes and vines, J. Chromatogr. A., 2009, 1216, 15, 3012-3022, https://doi.org/10.1016/j.chroma.2009.01.104 . [all data]

Valappil, Fan, et al., 2009
Valappil, Z.A.; Fan, X.; Zhang, H.Q.; Rouseff, R.L., Impact of thermal and nonthermal processing technologies on unfermented apple cider aroma vilatiles, J. Agric. Food Chem., 2009, 57, 3, 924-929, https://doi.org/10.1021/jf803142d . [all data]

Zhao, Xu, et al., 2009
Zhao, Y.; Xu, Y.; Li, J.; Fan, W.; Jiang, W., Profile of volatile compounds in 11 brandies by headspace solid-phase microextraction followed by gas chromatography-mass spectrometry, J. Food. Sci., 2009, 74, 2, c90-c99, https://doi.org/10.1111/j.1750-3841.2008.01029.x . [all data]

Kaack and Christensen, 2008
Kaack, K.; Christensen, L.P., Effect of packing materials and storage time on volatile compounds in tea processes from flowers of black elder (Sambucus nigra L.), Eur. Food Res. Technol., 2008, 227, 4, 1259-1273, https://doi.org/10.1007/s00217-008-0844-8 . [all data]

Tao, Wenlai, et al., 2008
Tao, L.; Wenlai, F.; Yan, X., Characterization of volatile and semi-volatile compounds in Chinese rica wines by headspace solid phase microextraction followed by gas chromatography - mass spectrometry, J. Inst. Brew., 2008, 114, 2, 172-179, https://doi.org/10.1002/j.2050-0416.2008.tb00323.x . [all data]

Yongsheng, Hua, et al., 2008
Yongsheng, T.; Hua, L.; Hua, W.; Li, Z., Volatile composition of young Cabernet Savignon red wine from Changli Counti (China), J. Food Composition and Analysis, 2008, 21, 8, 689-694, https://doi.org/10.1016/j.jfca.2008.05.007 . [all data]

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Liolios, Laouer, et al., 2007
Liolios, C.; Laouer, H.; Boulaacheb, N.; Gortzi, O.; Chinou, I., Chemical Composition and Antimicrobial Activity of the Essential Oil of Algherian Phlomis bovei De Noe subsp. bovei, Molecules, 2007, 12, 4, 772-781, https://doi.org/10.3390/12040772 . [all data]

Selli, 2007
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Tabanca N., Demirci B., et al., 2007
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Tian, Zhang, et al., 2007
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Vichi, Guadayol, et al., 2007
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Baser K.H.C., Ozek G., et al., 2006
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Baser, Özek, et al., 2006
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Quijano and Pino, 2006
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Tabanca, Demirci, et al., 2006
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Editorial paper, 2005
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Kosar, Özek, et al., 2005
Kosar, M.; Özek, T.; Göger, F.; Kürkcüoglu, M.; Hüsnü Can Baser, K., Comparison of Microwave-Assisted Hydrodistillation and Hydrodistillation Methods for the Analysis of Volatile Secondary Metabolites, Pharm. Biol., 2005, 43, 6, 491-495, https://doi.org/10.1080/13880200500220136 . [all data]

Sezik E., Kocakulak E., et al., 2005
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Altintas, Kose, et al., 2004
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Baser, Özek, et al., 2004
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Vinogradov, 2004
Vinogradov, B.A., Production, composition, properties and application of essential oils, 2004, retrieved from http://viness.narod.ru. [all data]

Buettner, Mestres, et al., 2003
Buettner, A.; Mestres, M.; Fischer, A.; Guasch, J.; Schieberle, P., Evaluation of the most odour-active compounds in the peel oil of clementines ( citrus reticulata blanco cv. clementine), Eur. Food Res. Technol., 2003, 216, 11-14. [all data]

Demirci, Baser, et al., 2003
Demirci, B.; Baser, K.H.C.; Yildiz, B.; Bahcecioglu, Z., Composition of the essential oils of six endemic Salvia spp. from Turkey, Flavour Fragr. J., 2003, 18, 2, 116-121, https://doi.org/10.1002/ffj.1173 . [all data]

Erdemoglu, Sener, et al., 2003
Erdemoglu, N.; Sener, B.; Demirci, B.; Baser, K.H.C., The glycosidically bound volatile compounds of Taxus baccata, Chem. Nat. Compd. (Engl. Transl.), 2003, 39, 2, 195-198, https://doi.org/10.1023/A:1024870031960 . [all data]

Garruti, Franco, et al., 2003
Garruti, D.S.; Franco, M.R.B.; da Silva, M.A.A.P.; Janzantti, N.S.; Alves, G.L., Evaluation of volatile flavour compounds from cashew apple (Anacardium occidentale L) juice by the Osme gas chromatography/olfactometry technique, J. Sci. Food Agric., 2003, 83, 14, 1455-1462, https://doi.org/10.1002/jsfa.1560 . [all data]

Krings, Banavara, et al., 2003
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Notes

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