1-Octanol

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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Optima-5RTX-1HP-5DB-5VF-5 MS
Column length (m) 30.60.30.30.60.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.220.250.250.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.30.
Tend (C) 246.230.240.240.260.
Heat rate (K/min) 3.2.3.3.2.
Initial hold (min) 1.    
Final hold (min)  5.  28.
I 1069.1063.1068.1071.1073.
ReferenceAl-Qudah, Muhaidat, et al., 2012Bendiabdellah, El Amine Dib, et al., 2012Bertoli, Lepnardi, et al., 2011Fraternale, Ricci, et al., 2011Leffingwell and Alford, 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase VF-5 MSVF-5 MSDB-1HP-5 MSHP-5
Column length (m) 60.30.50.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.320.250.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 30.40.60.40.50.
Tend (C) 260.250.250.260.300.
Heat rate (K/min) 2.5.8.4.50.
Initial hold (min)  3.  5.
Final hold (min) 28.3. 5.5.
I 1076.1076.1055.1074.1072.
ReferenceLeffingwell and Alford, 2011Liu, Lu, et al., 2011Misharina T., 2011Miyazawa, Marumoto, et al., 2011Bi Kouame, Bedi, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1HP-5 MSHP-5 MSHP-5HP-5 MS
Column length (m) 60.30.30.30.30.
Carrier gas HeliumHeliumHeliumHydrogenHelium
Substrate      
Column diameter (mm) 0.220.320.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.70.70.70.
Tend (C) 230.240.290.290.290.
Heat rate (K/min) 2.4.5.5.5.
Initial hold (min)  2.   
Final hold (min) 30.10.10. 10.
I 1061.1069.1069.1070.1067.
ReferenceDib, Djabou, et al., 2010Pino, Marquez, et al., 2010Radulovic, Blagojevic, et al., 2010Radulovic, Dordevic, et al., 2010Radulovic, Dordevic, et al., 2010, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSHP-5 MSHP-5 MSDB-1HP-5
Column length (m) 30.30.30.30.10.
Carrier gas HeliumHeliumHeliumHeHelium
Substrate      
Column diameter (mm) 0.320.250.250.250.10
Phase thickness (μm) 0.250.250.250.250.40
Tstart (C) 40.35.50.30.40.
Tend (C) 230.195.230.210.280.
Heat rate (K/min) 6.2.4.5.20.
Initial hold (min) 2.5.4. 1.
Final hold (min) 20.30.10. 1.
I 1082.1071.1068.1052.1091.
ReferenceChen, Song, et al., 2009Kim and Chung, 2009Forero, Quijano, et al., 2008Kumazawa, Itobe, et al., 2008Mildner-Szkudlarz and Jelen, 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSHP-5 MSRTX-5HP-5 MSOV-1
Column length (m) 30.30.20.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.180.250.25
Phase thickness (μm) 0.250.250.200.250.25
Tstart (C) 50.50.50.50.65.
Tend (C) 300.240.280.250.260.
Heat rate (K/min) 5.3.4.6.56.
Initial hold (min) 5. 1.1.5 
Final hold (min) 5.  10. 
I 1069.1046.1076.1074.1077.
ReferenceNoudogbessi, Yedomonhan, et al., 2008Sarikurkcu, Tepe, et al., 2008Skalicka-Wozniak, Los, et al., 2008Thakeow, Angeli, et al., 2008Wang, Yi, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase 5 % Phenyl methyl siloxaneHP-5MSHP-101DB-1SPB-5
Column length (m) 30.30.25.60.60.
Carrier gas  HeHeNitrogen 
Substrate      
Column diameter (mm) 0.250.250.20.250.32
Phase thickness (μm) 0.250.250.20.251.
Tstart (C) 50.60.70.60.40.
Tend (C) 250.250.200.250.230.
Heat rate (K/min) 3.2.3.5.3.
Initial hold (min)  8.2. 5.
Final hold (min)  15. 10.5.
I 1076.1069.1057.1053.1070.
ReferenceZellner, Bicchi, et al., 2008Ferhat, Tigrine-Kordjani, et al., 2007Jerkovic, Mastelic, et al., 2007Sonboli, Kanani, et al., 2007Vasta, Ratel, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-1DB-5DB-5MSHP-101
Column length (m) 30.50.30.30.25.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.320.20.320.250.2
Phase thickness (μm) 0.250.51.0.250.2
Tstart (C) 40.60.40.60.70.
Tend (C) 250.250.230.280.200.
Heat rate (K/min) 4.2.6.3.3.
Initial hold (min) 2. 2. 2.
Final hold (min) 5.120.15.30.15.
I 1070.1054.1075.1048.1073.
ReferenceXu, Fan, et al., 2007Castel, Fernandez, et al., 2006Fan and Qian, 2006Maronigiu, Piras, et al., 2006Mastelic, Jerkovic, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5Ultra-2HP-5 MSHP-5MSHP-5
Column length (m) 30.50.30.30.30.
Carrier gas HeliumHeHeliumHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.320.250.250.25
Tstart (C) 60.50.60.60.60.
Tend (C) 250.270.250.280.260.
Heat rate (K/min) 4.2.2.3.5.
Initial hold (min) 2. 8. 2.
Final hold (min) 20. 15. 14.
I 1070.1069.1069.1060.1068.
ReferencePino, Marquez, et al., 2006Schlumpberger B.O., Clery R.A., et al., 2006Tigrine-Kordiani, Meklati, et al., 2006Tzakou, Said, et al., 2006Yayli, Gülec, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-1BPX5Methyl SiliconeBPX-5
Column length (m) 30.50.25.60.30.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.320.20.200.30.25
Phase thickness (μm) 0.250.50.13 0.25
Tstart (C) 60.60.50.50.40.
Tend (C) 260.250.230.240.200.
Heat rate (K/min) 5.2.3.3.5.
Initial hold (min) 2. 2. 8.
Final hold (min) 14.60.  10.
I 1070.1051.1069.1068.1089.
ReferenceYayli, Gülec, et al., 2006Bendimerad and Bendiab, 2005Boustie, Rapior, et al., 2005Chalchat and Özcan, 2005Kalua, Allen, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5MSPE-5HP-5DB-1
Column length (m) 60.30.30.30.50.
Carrier gas HeHeH2Helium 
Substrate      
Column diameter (mm) 0.250.250.320.320.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.60.60.40.60.
Tend (C) 250.275.230.300.240.
Heat rate (K/min) 4.15.5.4.3.
Initial hold (min)   2.  
Final hold (min)   4.5. 
I 1039.1065.1065.1061.1048.
ReferenceRasooli and Owlia, 2005Shams-Ardakani, Ghannadi, et al., 2005Singh, Raina, et al., 2005Utsunomia, Kawata, et al., 2005Velasco-Negueruela, Pérez-Alonso, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5HP-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHe
Substrate      
Column diameter (mm) 0.320.320.320.320.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.40.40.40.40.
Tend (C) 250.250.250.250.250.
Heat rate (K/min) 5.5.5.5.5.
Initial hold (min) 2.2.2.2.2.
Final hold (min) 5.5.5.5.10.
I 1066.1069.1070.1076.1069.
ReferenceN/AN/AN/AN/AWu, Krings, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-15 % Phenyl methyl siloxaneDB-1HP-1HP-5
Column length (m) 25.0.60.30.25.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (μm) 0.251.0.250.330.33
Tstart (C) 60.40.50.40.40.
Tend (C) 220.250.250.260.190.
Heat rate (K/min) 5.7.4.2.4.
Initial hold (min)  10. 5. 
Final hold (min)  5. 20.5.
I 1059.1075.1039.1052.1054.
ReferenceMallavarapu, Kulkarni, et al., 2004Ramírez, Estévez, et al., 2004Rasooli and Razzaghi Abyaneh, 2004Senatore, Napolitano, et al., 2004Azodanlou, Darbellay, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5SPB-5MDN-5DB-5HP-5
Column length (m) 60.30.30.30.30.
Carrier gas HeHeHeH2He
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 35.40.40.60.60.
Tend (C) 280.220.280.280.280.
Heat rate (K/min) 5.5.20.4.4.
Initial hold (min) 2.1.1.10. 
Final hold (min) 4.20.1.40. 
I 1066.1077.1091.1070.1070.
ReferenceDhanda, Pegg, et al., 2003Ledauphin, Guichard, et al., 2003Mildner-Szkudlarz, Jelen, et al., 2003Pino, Marbot, et al., 2003Sajjadi and Mehregan, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5SPB-5SPB-1SPB-1HP-1
Column length (m) 30.60.30.30.30.
Carrier gas HeHeliumHeHeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.251.00.250.250.25
Tstart (C) 60.30.40.40.70.
Tend (C) 280.230.200.200.220.
Heat rate (K/min) 4.3.3.3.3.
Initial hold (min)   10.10. 
Final hold (min)     15.
I 1067.1067.1070.1061.1052.
ReferenceSajjadi and Mehregan, 2003, 2Sebastian, Viallon-Fernandez, et al., 2003Vichi, Castellote, et al., 2003Vichi, Pizzale, et al., 2003Cavaleiro, Salgueiro, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5DB-5RTX-5DB-1DB-5
Column length (m) 30.30.20.50.30.
Carrier gas HeliumHeHeN2He
Substrate      
Column diameter (mm) 0.250.250.180.250.25
Phase thickness (μm) 0.250.250.40.250.25
Tstart (C) 60.60.20.60.60.
Tend (C) 250.300.290.240.240.
Heat rate (K/min) 4.2.40.3.3.
Initial hold (min) 2. 3.5  
Final hold (min) 20. 0.5  
I 1070.1069.1072.1048.1073.
ReferencePino, Marbot, et al., 2002Ruberto, Biondi, et al., 2002Sies A., Hirsch R., et al., 2002Velasco-Negueruela, Pérez-Alonso, et al., 2002Zoghbi, Andrade, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101CP Sil 5 CBDB-5OV-101
Column length (m) 50.50.25.30.50.
Carrier gas N2N2HeN2Nitrogen
Substrate      
Column diameter (mm) 0.250.250.250.220.25
Phase thickness (μm)   0.40.25 
Tstart (C) 80.80.60.70.40.
Tend (C) 200.200.260.230.200.
Heat rate (K/min) 2.2.5.4.2.
Initial hold (min)   40.2.10.
Final hold (min)    20. 
I 1052.1052.1050.1076.1053.
ReferenceYang, 2001Yang, 2001, 2Baser, Özek, et al., 2000Mitiku, Sawamura, et al., 2000Tamura, Boonbumrung, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30Methyl SiliconeOV-101DB-5DB-5
Column length (m) 30.60.50.30.30.
Carrier gas   N2H2He
Substrate      
Column diameter (mm) 0.250.250.20.320.25
Phase thickness (μm)  0.25  0.25
Tstart (C) 50.40.80.32.60.
Tend (C) 300.220.200.260.240.
Heat rate (K/min) 10.5.1.7.3.
Initial hold (min)  10. 5. 
Final hold (min) 4. 20.5. 
I 1053.1056.801056.1074.1072.
ReferenceZhou, Robards, et al., 2000Baraldi, Rapparini, et al., 1999Menon, Chacko, et al., 1999Sun and Petracek, 1999Tellez, Canel, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5CBP-1HP-5HP-1DB-1
Column length (m) 50.30.25.60.60.
Carrier gas  HeHeHe 
Substrate      
Column diameter (mm) 0.320.250.20.250.25
Phase thickness (μm) 0.52 0.330.25 
Tstart (C) 35.60.70.50.30.
Tend (C) 250.240.290.280.200.
Heat rate (K/min) 2.4.3.4.4.
Initial hold (min) 15. 8.5.25.
Final hold (min) 45. 20. 20.
I 1072.1084.1073.1069.1053.
ReferenceBoylston and Viniyard, 1998Lamarque, Maestri, et al., 1998Poiana, Sicari, et al., 1998Stashenko, Cervantes, et al., 1998Buttery, Ling, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5Ultra-2OV-101OV-101
Column length (m) 60.60.50.50.50.
Carrier gas   HeN2N2
Substrate      
Column diameter (mm) 0.320.320.320.250.25
Phase thickness (μm) 1.1.0.52  
Tstart (C) 40.40.40.80.80.
Tend (C) 200.200.250.200.200.
Heat rate (K/min) 3.3.4.2.2.
Initial hold (min) 5.5.3.  
Final hold (min) 2.2.30.  
I 1068.1075.1074.1048.1050.
ReferenceKondjoyan, Viallon, et al., 1997Kondjoyan, Viallon, et al., 1997King, Matthews, et al., 1995Tamura, Nakamoto, et al., 1995Tamura, Nakamoto, et al., 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1DB-5 MSCross-Linked MethylsiliconeOV-101
Column length (m) 60.60.30.25.50.
Carrier gas HeHeHeliumHe 
Substrate      
Column diameter (mm) 0.250.250.250.320.22
Phase thickness (μm) 0.250.25   
Tstart (C) 70.70.50.35.80.
Tend (C) 270.270.250.225.200.
Heat rate (K/min) 2.52.54.4.2.
Initial hold (min) 5.5. 3. 
Final hold (min)      
I 1074.1074.1068.1059.1061.
ReferenceTirado, Stashenko, et al., 1995Tirado, Stashenko, et al., 1995Gomez and Ledbetter, 1994Bravo and Hotchkiss, 1993Egolf and Jurs, 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5Ultra-2DB-5DB-5OV-101
Column length (m) 30.50.30.30.50.
Carrier gas  HeH2H2 
Substrate      
Column diameter (mm) 0.250.320.320.320.25
Phase thickness (μm) 0.2410.521.1. 
Tstart (C) 60.40.40.40.80.
Tend (C) 160.250.220.220.200.
Heat rate (K/min) 4.4.3.3.2.
Initial hold (min) 2.3.   
Final hold (min)  30.   
I 1068.341095.1072.1072.1052.
ReferenceKim, Kim, et al., 1993King, Hamilton, et al., 1993Moio, Dekimpe, et al., 1993Moio, Dekimpe, et al., 1993Tamura, Yang, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101DB-5HG-5Ultra-1
Column length (m) 50.52.60.50.25.
Carrier gas  HeliumHeHeHe
Substrate      
Column diameter (mm) 0.250.260.320.320.32
Phase thickness (μm)   1.00.520.25
Tstart (C) 80.40.40.35.80.
Tend (C) 200.200.240.250.260.
Heat rate (K/min) 2.3.3.3.3.
Initial hold (min)  0. 15. 
Final hold (min)  0. 45. 
I 1053.1060.1079.1073.1051.
ReferenceTamura, Yang, et al., 1993Tkachenko and Zenkevich, 1993Berdague, Denoyer, et al., 1991Drumm and Spanier, 1991Okumura, 1991
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101OV-101DB-1OV-101
Column length (m) 50.50.50.60.50.
Carrier gas  N2N2 N2
Substrate      
Column diameter (mm) 0.280.250.250.320.25
Phase thickness (μm)      
Tstart (C) 80.80.80.50.80.
Tend (C) 200.200.200.250.200.
Heat rate (K/min) 2.2.2.4.2.
Initial hold (min)    0.1 
Final hold (min)    5. 
I 1061.1054.1054.1054.1054.
ReferenceAnker, Jurs, et al., 1990Yang and Sugisawa, 1990Yang and Sugisawa, 1990Binder and Flath, 1989Sugisawa, Yamamoto, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101SE-54DB5-30WOV-1
Column length (m) 50.50.25.30.60.
Carrier gas N2N2N2HeHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.50
Phase thickness (μm)    0.251.2
Tstart (C) 80.80.60.60.40.
Tend (C) 200.200.260.300.220.
Heat rate (K/min) 2.2.6.5.2.
Initial hold (min)   2.  
Final hold (min)      
I 1053.1054.1069.1075.1058.
ReferenceSugisawa, Yang, et al., 1989Sugisawa, Yang, et al., 1989Bestmann, Classen, et al., 1988Schwab and Schreier, 1988Wahab, Aboutabl, et al., 1987
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1DB-1SP 2100SE-30
Column length (m) 50.50.60.40.50.
Carrier gas    Helium 
Substrate      
Column diameter (mm) 0.320.320.320.200.5
Phase thickness (μm)      
Tstart (C) 0.50.50.40.40.
Tend (C) 250.250.250.200.170.
Heat rate (K/min) 3.3.4.10.3.
Initial hold (min)   0.1 3.
Final hold (min)   5.  
I 1057.1056.1052.1057.1061.
ReferenceHabu, Flath, et al., 1985Habu, Flath, et al., 1985Flath, Mon, et al., 1983Labropoulos, Palmer, et al., 1982Heydanek and McGorrin, 1981
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedCapillary
Active phase Apiezon LOV-1
Column length (m) 2.183.
Carrier gas  N2
Substrate Chromosorb G-AW-DMCS 
Column diameter (mm)  0.762
Phase thickness (μm)   
Tstart (C) 25.0.
Tend (C)  230.
Heat rate (K/min) 10.1.
Initial hold (min)   
Final hold (min)   
I 1083.1057.
ReferenceDahlmann, Köser, et al., 1979Schreyen, Dirinck, et al., 1979
Comment MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Al-Qudah, Muhaidat, et al., 2012
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Fraternale, D.; Ricci, D.; Flamini, G.; Giomaro, G., Volatile profile of red apple from Marche region (Italy), Rec. Nat. Prod., 2011, 5, 3, 202-207. [all data]

Leffingwell and Alford, 2011
Leffingwell, J.; Alford, E.D., Volatile constituents of the giant pufball mushroom (Calvatia gigantea), Leffingwell Rep., 2011, 4, 1-17. [all data]

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Liu, S.; Lu, S.; Su, Y.; Guo, Y., Analysis of volatile compounds in Radix Bupleuri injection by GC-MS-MS, Chromatographia, 2011, 74, 5-6, 497-502, https://doi.org/10.1007/s10337-011-2082-7 . [all data]

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Misharina T., Headspace analysis of aroma compounds using porous adsorbents, Chemistry Chem. Technol., 2011, 5, 3, 347-354. [all data]

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Notes

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