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3-Methylbutanoic acid, TBDMS derivative


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spec Data Center, S.E. Stein, director

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-51147.Paik, Lee, et al., 200530. m/0.25 mm/0.25 «mu»m, Helium, 60. C @ 2. min, 4. K/min; Tend: 290. C
CapillaryDB-51150.Kim, Kim, et al., 199030. m/0.25 mm/0.25 «mu»m, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryDB-11126.Kim, Hahn, et al., 198930. m/0.32 mm/0.25 «mu»m, N2, 60. C @ 2. min, 4. K/min; Tend: 280. C
CapillaryDB-51151.Kim, Zlatkis, et al., 198715. m/0.32 mm/0.25 «mu»m, He, 60. C @ 2. min, 10. K/min; Tend: 200. C

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Paik, Lee, et al., 2005
Paik, M.-J.; Lee, H.-J.; Kim, K.-R., Simultaneous retention index analysis of urinary amino acids and carboxylic acids for graphic recognition of abnormal state, J. Chromatogr. B, 2005, 821, 1, 94-104, https://doi.org/10.1016/j.jchromb.2005.04.011 . [all data]

Kim, Kim, et al., 1990
Kim, K.-R.; Kim, J.-H.; Park, H.-K., Trace analysis as TBDMS derivatives of organic acids in aqueous samples, J. Korean Chem. Soc., 1990, 34, 4, 352-359. [all data]

Kim, Hahn, et al., 1989
Kim, K.R.; Hahn, M.K.; Zlatkis, A.; Horning, E.C.; Middleditch, B.S., Simultaneous gas chromatography of volatile and nonvolatile carboxylic acids as tert.-butyldimethylsilyl derivatives, J. Chromatogr., 1989, 468, 289-301, https://doi.org/10.1016/S0021-9673(00)96323-4 . [all data]

Kim, Zlatkis, et al., 1987
Kim, K.; Zlatkis, A.; Horning, E.C.; Middleditch, B.S., Gas chromatography of volatile fatty acids as tert-butyldimethylsilyl esters, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1987, 10, 9, 522-523, https://doi.org/10.1002/jhrc.1240100910 . [all data]


Notes

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