5-Hepten-2-one, 6-methyl-

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Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5CP-Sil PONA GBSPB-5DB-5
Column length (m) 30.30.100.60.30.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.251.0.25
Tstart (C) 60.40.140.40.60.
Tend (C) 240.250.230.230.240.
Heat rate (K/min) 3.5.5.3.3.
Initial hold (min)  1.10.2. 
Final hold (min)  10.25.10. 
I 988.987.958.987.986.
ReferenceBaccouri, Ben Temime, et al., 2007Benzo, Gilardoni, et al., 2007Cunicao, Lopes, et al., 2007Engel and Ratel, 2007Flamini, Cioni, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RH-5MSDB-5DB-PetroDB-PetroHP-5MS
Column length (m) 60.30.50.50.30.
Carrier gas  He  He
Substrate      
Column diameter (mm) 0.250.250.20.20.25
Phase thickness (μm) 0.250.250.50.50.25
Tstart (C) 40.60.50.50.60.
Tend (C) 350.240.270.270.280.
Heat rate (K/min) 4.3.2.2.4.
Initial hold (min) 2.   5.
Final hold (min) 10.    
I 989.987.960.960.980.
ReferenceHashizume M., Gordon M.H., et al., 2007Maccioni, Baldini, et al., 2007Pang T., Zhu S., et al., 2007Pang T., Zhu S., et al., 2007Saroglou, Arfan, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5HP-5DB-1HP-5MS
Column length (m) 30.30.30.25.30.
Carrier gas HeN2He He
Substrate      
Column diameter (mm) 0.250.250.250.20.25
Phase thickness (μm) 0.250.250.250.330.25
Tstart (C) 50.60.60.50.60.
Tend (C) 250.220.260.300.280.
Heat rate (K/min) 3.5.3.4.3.
Initial hold (min)  10.   
Final hold (min) 10.    
I 982.987.984.972.965.
ReferenceYu, Liao, et al., 2007Flamini, Tebano, et al., 2006Javidnia, Miri, et al., 2006Osorio, Alarcon, et al., 2006Pavlovic, Kovacevic, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBRTX-5BP-1RTX-1BPX-5
Column length (m) 25.30.50.60.25.
Carrier gas H2N2He He
Substrate      
Column diameter (mm) 0.250.250.220.220.25
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 80.40.60.60.50.
Tend (C) 270.300.220.220.300.
Heat rate (K/min) 10.5.2.2.5.
Initial hold (min)  2.  5.
Final hold (min)  10.20.20. 
I 972.980.2960.963.999.
ReferenceZiegenbein, Hanssen, et al., 2006Ádámová, Orinák, et al., 2005Boti J.B., Koukoua G., et al., 2005Cozzani, Muselli, et al., 2005Dickschat J.S., Wagner-Dobler I., et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Sil 8CB-MSDB-1HP-5HP-5HP-5
Column length (m) 0.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.25 0.25
Tstart (C) 40.40.60.60.60.
Tend (C) 280.250.260.260.260.
Heat rate (K/min) 4.3.3.3.3.
Initial hold (min) 2.    
Final hold (min) 5.20.   
I 987.969.986.985.983.
ReferenceElmore, Cooper, et al., 2005Gancel, Ollitrault, et al., 2005Javidnia, Miri, et al., 2005Javidnia, Miri, et al., 2005, 2Javidnia, Miri, et al., 2005, 3
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSSE-54HP-5HP-5
Column length (m) 30.60.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.50.
Tend (C) 250.200.260.240.290.
Heat rate (K/min) 4.2.2.3.4.
Initial hold (min) 2. 5.  
Final hold (min) 20.10.   
I 985.986.987.986.989.
ReferencePino, Mesa, et al., 2005Smadja, Rondeau, et al., 2005Alma, Nitz, et al., 2004Flamini, Bader, et al., 2004Flach A., Dondon R.C., et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5RSL-200SPB-5
Column length (m) 30.30.30.30.30.
Carrier gas N2HeHeH2He
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 60.60.60.40.60.
Tend (C) 220.260.260.280.250.
Heat rate (K/min) 5.3.3.6.4.
Initial hold (min) 10.  5.2.
Final hold (min)    5.20.
I 986.985.985.981.985.
ReferenceFlamini, Luigi Cioni, et al., 2004Javidnia, Miri, et al., 2004Javidnia, Miri, et al., 2004, 2Ngassoum, Ousmaila, et al., 2004Pino, Marbot, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5HP-5MSHP-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeN2N2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.50.60.60.60.
Tend (C) 290.310.280.220.220.
Heat rate (K/min) 4.4.3.5.5.
Initial hold (min)    10.10.
Final hold (min)      
I 980.989.965.993.988.
ReferenceReis, Pansarim, et al., 2004Singer, Flach, et al., 2004Tzakou, Vagias, et al., 2004Campeol, Flamini, et al., 2003Campeol, Flamini, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1DB-5DB-5HP-5HP-5
Column length (m) 60.30.30.30.30.
Carrier gas HeHeHeN2N2
Substrate      
Column diameter (mm) 0.220.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 230.240.240.220.220.
Heat rate (K/min) 2.3.3.5.5.
Initial hold (min)    10.10.
Final hold (min) 45.    
I 961.987.988.986.988.
ReferenceCavalli, Tomi, et al., 2003Flamini, Cioni, et al., 2003Flamini, Luigi Cioni, et al., 2003Flamini, Luigi Cioni, et al., 2003, 2Flamini, Luigi Cioni, et al., 2003, 3
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-1DB-5HP-5CP Sil 5 CB
Column length (m) 30.30.25.30.60.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 60.40.60.60.60.
Tend (C) 220.250.260.280.280.
Heat rate (K/min) 5.3.4.3.3.
Initial hold (min) 10.   10.
Final hold (min)  20.  60.
I 987.969.987.985.961.
ReferenceFlamini, Luigi Cioni, et al., 2003, 4Gancel, Ollitrault, et al., 2003Javidnia, Miri, et al., 2003Ngassapa, Runyoro, et al., 2003Pino, Almora, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5Mega 5MSDB-5BPX-5
Column length (m) 30.30.30.30.50.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.250.251.0.5
Tstart (C) 40.60.40.50.60.
Tend (C) 240.280.240.200.250.
Heat rate (K/min) 3.4.3.2.54.
Initial hold (min)  5.2. 5.
Final hold (min)     20.
I 986.985.981.984.81003.
ReferenceShellie and Marriott, 2003Skaltsa, Demetzos, et al., 2003Verzera, Trozzi, et al., 2003Xu, van Stee, et al., 2003Bredie, Mottram, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5DB-5HP-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.251.0.250.250.25
Tstart (C) 60.50.60.60.60.
Tend (C) 300.200.240.220.260.
Heat rate (K/min) 3.2.53.5.4.
Initial hold (min)    10. 
Final hold (min)      
I 985.984.988.986.985.
ReferenceCouladis, Chinou, et al., 2002Dallüge, van Stee, et al., 2002Flamini, Cioni, et al., 2002Flamini, Cioni, et al., 2002, 2Javidnia, Miri, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1RTX-5HP-1CP Sil 8 CBCP Sil 5 CB
Column length (m) 50.30.24.60.30.
Carrier gas HeHeHeHeH2
Substrate      
Column diameter (mm) 0.220.250.320.250.25
Phase thickness (μm) 0.250.250.170.250.25
Tstart (C) 60.45.60.40.60.
Tend (C) 220.300.250.250.280.
Heat rate (K/min) 2.3.4.4.2.
Initial hold (min)  6.2.8.10.
Final hold (min) 20.10.20.10.40.
I 942.988.961.984.951.
ReferenceLota, de Rocca Serra, et al., 2002Mondello, Zappia, et al., 2002Nath, Sarma, et al., 2002Oruna-Concha, Ames, et al., 2002Pino, Marbot, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBHP-5HP-5BP-1CP Sil 5 CB
Column length (m) 50.30.30.50.50.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.250.250.220.32
Phase thickness (μm) 0.40.250.250.250.4
Tstart (C) 60.60.60.60.60.
Tend (C) 280.260.380.220.280.
Heat rate (K/min) 3.3.3.2.3.
Initial hold (min) 10.   10.
Final hold (min) 60.10.  60.
I 962.985.983.942.962.
ReferencePino, Marbot, et al., 2002, 2Couladis, Baziou, et al., 2001Couladis, Tsortanidou, et al., 2001Lota, Serra, et al., 2001Pino and Marbot, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBHP-5MSSE-54HP-5DB-5
Column length (m) 50.30.25.30.60.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.320.250.310.200.25
Phase thickness (μm) 0.40.25 0.250.25
Tstart (C) 60.60.35.60.40.
Tend (C) 280.280.230.180.290.
Heat rate (K/min) 3.4.4.4.4.
Initial hold (min) 10.5.3.8.2.
Final hold (min) 60. 10.2.5.
I 962.985.987.40982.975.
ReferencePino, Marbot, et al., 2001Skaltsa, Mavrommati, et al., 2001Yin, Xiu, et al., 2001Alonzo, Bosco, et al., 2000Bartley and Jacobs, 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5Mega 5MSCP Sil 8 CBDB-1DB-1
Column length (m) 30.30.50.60.60.
Carrier gas HeHe  He
Substrate      
Column diameter (mm) 0.250.250.320.320.32
Phase thickness (μm) 0.250.25 1. 
Tstart (C) 50.40.60.-50.60.
Tend (C) 280.240.220.175.230.
Heat rate (K/min) 4.3.4.6.3.
Initial hold (min) 5.2.5.2. 
Final hold (min)   30. 5.
I 984.981.984.965.5962.
ReferenceLazari, Skaltsa, et al., 2000Verzera, la Rosa, et al., 2000Chevance and Farmer, 1999Helmig, Klinger, et al., 1999Javidnia and Shafiee, 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1BP-1SPB-5SE-54SE-54
Column length (m) 50.50.60.25.25.
Carrier gas HeHeHeH2H2
Substrate      
Column diameter (mm) 0.220.220.320.310.31
Phase thickness (μm) 0.250.251.  
Tstart (C) 60.60.40.35.35.
Tend (C) 230.230.200.250.250.
Heat rate (K/min) 2.2.3.4.4.
Initial hold (min)   5.3.3.
Final hold (min) 35.35.2.  
I 942.942.986.987.988.
ReferenceLota, Serra, et al., 1999Lota, Serra, et al., 1999Verdier-Metz., Coulon, et al., 1998Li, Wang, et al., 1998Li, Wang, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1DB-5HP-101DB-5
Column length (m) 30.30.60.50.30.
Carrier gas    N2He
Substrate      
Column diameter (mm) 0.250.250.330.250.25
Phase thickness (μm) 1.1.0.25  
Tstart (C) -50.-50.-50.70.50.
Tend (C) 180.180.180.200.250.
Heat rate (K/min) 6.6.6.3.4.
Initial hold (min)      
Final hold (min)      
I 962.3942.4985.3973.984.
ReferenceHelmig, Pollock, et al., 1996Helmig, Pollock, et al., 1996Helmig, Pollock, et al., 1996Chung, Eiserich, et al., 1993Gómez, Ledbetter, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101DB-1DB-5OV-101
Column length (m) 50.50.60.0.3250.
Carrier gas N2N2 H2H2
Substrate      
Column diameter (mm) 0.250.250.321.0.32
Phase thickness (μm)      
Tstart (C) 80.80.50.30.50.
Tend (C) 200.200.250.180.200.
Heat rate (K/min) 2.2.4.1.52.
Initial hold (min)   0.15. 
Final hold (min)      
I 962.965.961.989.962.
ReferenceYang, Sugisawa, et al., 1992Yang, Sugisawa, et al., 1992Flath, Light, et al., 1990Guichard and Souty, 1988Pieribattesti, Smadja, et al., 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase SPB-1CP Sil 5 CB
Column length (m) 60.25.
Carrier gas He 
Substrate   
Column diameter (mm) 0.250.22
Phase thickness (μm) 0.25 
Tstart (C) 35.70.
Tend (C) 235.205.
Heat rate (K/min) 2.4.
Initial hold (min) 10. 
Final hold (min) 40. 
I 966.970.
ReferenceHuang, Bruechert, et al., 1987Hendriks and Bruins, 1983
Comment MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References