5-Hepten-2-one, 6-methyl-
- Formula: C8H14O
- Molecular weight: 126.1962
- IUPAC Standard InChIKey: UHEPJGULSIKKTP-UHFFFAOYSA-N
- CAS Registry Number: 110-93-0
- Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript. - Other names: 6-Methyl-5-heptene-2-one; 6-Methyl-5-hepten-2-one; 2-Methyl-2-hepten-6-one; 6-Methyl hept-5-en-2-one; Sulcatone; NSC 15294; Prenylacetone; 129085-68-3; Methyl heptenone; 2-methyl-6-heptenone; methyl-5-hepten-2-one; 2-methylhept-2-en-6-one; 6-Methyl hept-5-ene-2-one; (E)-6-methylhept-5-en-2-one; 6-methyI-5-hepten-2-one
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Normal alkane RI, non-polar column, temperature ramp
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | Optima-5 | HP-5 MS | DB-5 | HP-5 | DB-5 |
Column length (m) | 30. | 30. | 30. | 30. | 30. |
Carrier gas | Helium | Helium | Helium | Helium | Helium |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.32 | 0.32 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Tstart (C) | 60. | 50. | 60. | 60. | 50. |
Tend (C) | 246. | 320. | 240. | 240. | 300. |
Heat rate (K/min) | 3. | 5. | 3. | 3. | 4. |
Initial hold (min) | 1. | 5. | 2. | 4. | |
Final hold (min) | 5. | ||||
I | 986. | 988. | 984. | 984. | 989. |
Reference | Al-Qudah, Muhaidat, et al., 2012 | Nawrath, Mgode, et al., 2012 | Fraternale, Ricci, et al., 2011 | Kahriman, Tosun, et al., 2011 | Osorio, Carriazo, et al., 2011 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | OV-1 | DB-5 MS | BP-1 | HP-5 MS | HP-5 MS |
Column length (m) | 50. | 60. | 30. | 30. | |
Carrier gas | Helium | Nitrogen | Helium | Helium | |
Substrate | |||||
Column diameter (mm) | 0.32 | 0.25 | 0.32 | 0.25 | |
Phase thickness (μm) | 0.50 | 0.25 | 0.25 | 0.25 | |
Tstart (C) | 40. | 40. | 60. | 50. | 70. |
Tend (C) | 270. | 250. | 220. | 240. | 290. |
Heat rate (K/min) | 2. | 5. | 5. | 4. | 5. |
Initial hold (min) | 15. | 10. | 2. | ||
Final hold (min) | 10. | 15. | 30. | 10. | 10. |
I | 963. | 986. | 966. | 988. | 986. |
Reference | Da Costa, Yang, et al., 2010 | Mesa-Arango, Betancur-Galvis, et al., 2010 | Mishra, Chaudhary, et al., 2010 | Pino, Marquez, et al., 2010 | Radulovic, Blagojevic, et al., 2010 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-1 | DB-5 MS | VF-5 | BP-1 | DB-1 MS |
Column length (m) | 30. | 30. | 30. | 50. | 30. |
Carrier gas | Helium | Helium | Helium | Helium | Helium |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.22 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Tstart (C) | 50. | 50. | 60. | 60. | 40. |
Tend (C) | 220. | 250. | 300. | 220. | 250. |
Heat rate (K/min) | 4. | 2. | 10. | 2. | 6. |
Initial hold (min) | 2. | 5. | 2. | 1. | |
Final hold (min) | 2. | 10. | 20. | 4. | |
I | 961. | 986. | 990. | 961. | 964. |
Reference | Xu, Tang, et al., 2010 | Koba, Sanda, et al., 2009 | Li and Zhao, 2009 | Ottavioli, Bighelli, et al., 2009 | Seo, Kim, et al., 2009 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | SPB-5 | HP-5 MS | DB-5 | HP-5 MS | DB-5 |
Column length (m) | 60. | 30. | 30. | 30. | 30. |
Carrier gas | Helium | Helium | He | ||
Substrate | |||||
Column diameter (mm) | 0.32 | 0.25 | 0.25 | 0.25 | 0.26 |
Phase thickness (μm) | 1.00 | 0.25 | 0.25 | 0.25 | |
Tstart (C) | 40. | 50. | 60. | 60. | 60. |
Tend (C) | 230. | 280. | 220. | 280. | 240. |
Heat rate (K/min) | 3. | 4. | 3. | 3. | 3. |
Initial hold (min) | 5. | ||||
Final hold (min) | 10. | ||||
I | 987. | 986. | 982. | 985. | 979. |
Reference | Sivadier, Ratel, et al., 2009 | Zhao, Zeng, et al., 2009 | Bastos, Ishimoto, et al., 2008 | Baziou, Couladis, et al., 2008 | Bos, Woerdenbag, et al., 2007 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-5 | 5 % Phenyl methyl siloxane | DB-5 | DB-1 | DB-5 |
Column length (m) | 30. | 60. | 60. | 30. | 30. |
Carrier gas | Helium | He | Helium | Helium | He |
Substrate | |||||
Column diameter (mm) | 0.26 | 0.25 | 0.32 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 1.0 | 0.25 | 0.25 |
Tstart (C) | 60. | 90. | 35. | 50. | 60. |
Tend (C) | 290. | 225. | 240. | 260. | 320. |
Heat rate (K/min) | 3. | 3. | 15. | 2.5 | 10. |
Initial hold (min) | 7. | 1. | |||
Final hold (min) | 15. | 10. | 20. | 4. | |
I | 979. | 986. | 985. | 957. | 984. |
Reference | Elfami, Bos, et al., 2007 | Gil A., Van Baren C.M., et al., 2007 | Gogus, Ozel, et al., 2007 | Monser-Esfahani, Karamkhani, et al., 2007 | Smelcerovic, Spiteller, et al., 2007 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | HP-5 | HP-5 | HP-5 MS | SPB-5 | HP-5MS |
Column length (m) | 25. | 25. | 30. | 60. | 30. |
Carrier gas | Helium | He | |||
Substrate | |||||
Column diameter (mm) | 0.2 | 0.2 | 0.25 | 0.32 | 0.25 |
Phase thickness (μm) | 0.32 | 0.32 | 0.25 | 1. | 0.25 |
Tstart (C) | 40. | 40. | 60. | 40. | 40. |
Tend (C) | 250. | 250. | 280. | 230. | 250. |
Heat rate (K/min) | 5. | 5. | 3. | 3. | 3. |
Initial hold (min) | 1. | 1. | 5. | 5. | |
Final hold (min) | 5. | 10. | |||
I | 982. | 984. | 986. | 986. | 989. |
Reference | Tapia, Perich, et al., 2007 | Tapia, Perich, et al., 2007 | Vagionas, Graikou, et al., 2007 | Vasta, Ratel, et al., 2007 | Vichi, Riu-Aumatell, et al., 2007 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-5 | HP-1 | DB-1 | DB-5 | DB-5 |
Column length (m) | 30. | 50. | 60. | 30. | 30. |
Carrier gas | He | He | Nitrogen | Helium | Helium |
Substrate | |||||
Column diameter (mm) | 0.32 | 0.2 | 0.25 | 0.26 | 0.25 |
Phase thickness (μm) | 0.25 | 0.33 | 0.25 | 0.25 | |
Tstart (C) | 40. | 60. | 40. | 60. | 60. |
Tend (C) | 250. | 250. | 200. | 290. | 260. |
Heat rate (K/min) | 4. | 2. | 2. | 3. | 3. |
Initial hold (min) | 2. | 4. | 1. | ||
Final hold (min) | 5. | 30. | 9. | ||
I | 985. | 961. | 963. | 979. | 984. |
Reference | Xu, Fan, et al., 2007 | Castel, Fernandez, et al., 2006 | Chen, Sheu, et al., 2006 | Elfami, Komar, et al., 2006 | Javidnia, Miri, et al., 2006 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-5 | DB-5 | PE-5 | SPB-5 | DB-5 |
Column length (m) | 30. | 25. | 50. | 30. | 30. |
Carrier gas | He | N2 | He | Helium | Hydrogen |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.32 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.15 | 0.25 | 0.25 | 0.25 |
Tstart (C) | 60. | 50. | 100. | 60. | 70. |
Tend (C) | 220. | 200. | 280. | 250. | 280. |
Heat rate (K/min) | 4. | 4. | 3. | 4. | 4. |
Initial hold (min) | 5. | 3. | 1. | 2. | 4. |
Final hold (min) | 20. | ||||
I | 988. | 983. | 982. | 985. | 985. |
Reference | Morteza-Semnani K., Saeedi M., et al., 2006 | Ouamba, Ouabonzi, et al., 2006 | Pandey-Rai S., Mallavarapu G.R., et al., 2006 | Pino, Marquez, et al., 2006 | Pino, Marbot, et al., 2006 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-5 | DB-5 | HP-5MS | DB-1 | Ultra-2 |
Column length (m) | 30. | 30. | 30. | 60. | 50. |
Carrier gas | Hydrogen | He | He | He | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.32 |
Tstart (C) | 70. | 60. | 60. | 70. | 50. |
Tend (C) | 280. | 200. | 280. | 230. | 270. |
Heat rate (K/min) | 4. | 2. | 4. | 2. | 2. |
Initial hold (min) | 4. | 2. | |||
Final hold (min) | 60. | 20. | |||
I | 985. | 992. | 987. | 959. | 986. |
Reference | Pino, Marbot, et al., 2006 | Rout, Naik, et al., 2006 | Sajjadi, 2006 | Sawamura, Onishi, et al., 2006 | Schlumpberger B.O., Clery R.A., et al., 2006 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-5 | HP-1 | BPX-5 | DB-5 | HP-1 |
Column length (m) | 30. | 50. | 50. | 30. | 50. |
Carrier gas | H2 | He | He | He | |
Substrate | |||||
Column diameter (mm) | 0.20 | 0.2 | 0.22 | 0.25 | 0.2 |
Phase thickness (μm) | 0.18 | 0.5 | 1. | 0.25 | 0.5 |
Tstart (C) | 60. | 60. | 70. | 60. | 60. |
Tend (C) | 240. | 250. | 280. | 210. | 250. |
Heat rate (K/min) | 3. | 2. | 4. | 3. | 2. |
Initial hold (min) | 5. | ||||
Final hold (min) | 40. | 4. | 60. | ||
I | 985. | 964. | 996. | 990. | 962. |
Reference | Silva, Oliveira, et al., 2006 | Valette, Fernandez, et al., 2006 | Wohlmuth, Smith, et al., 2006 | Askari and Sefidkon, 2005 | Bendimerad and Bendiab, 2005 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-5 | DB-5 | BPX5 | BPX-5 | HP-5 |
Column length (m) | 50. | 25. | 25. | 25. | 25. |
Carrier gas | Helium | He | He | ||
Substrate | |||||
Column diameter (mm) | 0.3 | 0.25 | 0.22 | 0.22 | 0.2 |
Phase thickness (μm) | 0.25 | 0.15 | 0.25 | 0.25 | 0.33 |
Tstart (C) | 60. | 40. | 50. | 50. | 60. |
Tend (C) | 240. | 220. | 320. | 320. | 240. |
Heat rate (K/min) | 2. | 3. | 5. | 5. | 3. |
Initial hold (min) | 5. | 5. | 5. | ||
Final hold (min) | 7. | ||||
I | 986. | 982. | 999. | 997. | 984. |
Reference | Chagonda and Chalchat, 2005 | Chagonda and Chalchat, 2005, 2 | Dickschat, Bode, et al., 2005 | Dickschat, Martens, et al., 2005 | Duarte, Figueira, et al., 2005 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | RTX-5Sil | BPX-5 | HP-5 | HP-5MS | CP Sil 5 CB |
Column length (m) | 30. | 30. | 60. | 30. | 30. |
Carrier gas | He | He | He | ||
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.32 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Tstart (C) | 45. | 40. | 30. | 50. | 40. |
Tend (C) | 200. | 200. | 260. | 250. | 220. |
Heat rate (K/min) | 3. | 5. | 2. | 3. | 4. |
Initial hold (min) | 5. | 8. | 2. | 10. | 1. |
Final hold (min) | 10. | 28. | 5. | ||
I | 993. | 1011. | 995.4 | 993. | 986. |
Reference | Holland, Larkov, et al., 2005 | Kalua, Allen, et al., 2005 | Leffingwell and Alford, 2005 | Melkani, Dev, et al., 2005 | Rohloff and Bones, 2005 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | CP Sil 5 CB | HP-5MS | HP-5MS | HP-5 | HP-5 |
Column length (m) | 30. | 30. | 30. | 30. | 30. |
Carrier gas | He | He | He | Helium | Helium |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.32 | 0.32 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Tstart (C) | 40. | 60. | 50. | 40. | 40. |
Tend (C) | 220. | 280. | 240. | 300. | 250. |
Heat rate (K/min) | 4. | 3. | 3. | 4. | 5. |
Initial hold (min) | 1. | 5. | 3. | 2. | |
Final hold (min) | 5. | 5. | |||
I | 986. | 991. | 979. | 969. | 988. |
Reference | Rohloff and Bones, 2005 | Setzer, Noletto, et al., 2005 | Tepe B., Sokmen M., et al., 2005 | Utsunomia, Kawata, et al., 2005 | N/A |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | HP-5 | ZB-5 | DB-1 | DB-1 | DB-1 |
Column length (m) | 30. | 60. | 60. | 60. | 60. |
Carrier gas | Helium | He | He | He | He |
Substrate | |||||
Column diameter (mm) | 0.32 | 0.25 | 0.32 | 0.32 | 0.32 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Tstart (C) | 40. | 40. | 35. | 35. | 35. |
Tend (C) | 250. | 260. | 230. | 230. | 230. |
Heat rate (K/min) | 5. | 6. | 2. | 2. | 2. |
Initial hold (min) | 2. | 4.6 | 4. | 4. | 4. |
Final hold (min) | 5. | 1. | 25. | 25. | 25. |
I | 988. | 993. | 961. | 963. | 965. |
Reference | N/A | Jürgens and Dötterl, 2004 | Park, Lee, et al., 2004 | Park, Lee, et al., 2004 | Park, Lee, et al., 2004 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-1 | Methyl Silicone | HP-5 MS | HP-5MS | HP-5 |
Column length (m) | 60. | 60. | 30. | 30. | 25. |
Carrier gas | He | He | Helium | He | N2 |
Substrate | |||||
Column diameter (mm) | 0.32 | 0.25 | 0.25 | 0.25 | 0.2 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.5 |
Tstart (C) | 35. | 60. | 60. | 60. | 30. |
Tend (C) | 230. | 200. | 200. | 280. | 280. |
Heat rate (K/min) | 2. | 4. | 4. | 4. | 3. |
Initial hold (min) | 4. | 1. | 1. | ||
Final hold (min) | 25. | 20. | 20. | ||
I | 968. | 985. | 985. | 984. | 986. |
Reference | Park, Lee, et al., 2004 | Rojas, Usubillaga, et al., 2004 | Royas, Usubillaga, et al., 2004 | Sadeghpour, Asghari, et al., 2004 | Shafi, Nambiar, et al., 2004 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | HP-1 | HP-5 | HP-5 | SPB-5 | DB-5 |
Column length (m) | 50. | 30. | 30. | 60. | 30. |
Carrier gas | He | He | Helium | Helium | He |
Substrate | |||||
Column diameter (mm) | 0.2 | 0.25 | 0.32 | 0.32 | 0.25 |
Phase thickness (μm) | 0.5 | 0.25 | 1.0 | 0.25 | |
Tstart (C) | 60. | 60. | 70. | 30. | 60. |
Tend (C) | 220. | 275. | 210. | 230. | 240. |
Heat rate (K/min) | 2. | 4. | 2. | 3. | 3. |
Initial hold (min) | |||||
Final hold (min) | 45. | 60. | |||
I | 962. | 982. | 990. | 983. | 984. |
Reference | Fernandez, Lizzani-Cuvelier, et al., 2003 | Ghannadi and Zolfaghari, 2003 | Mookdasanit, Tamura, et al., 2003 | Sebastian, Viallon-Fernandez, et al., 2003 | da Silva, Luz, et al., 2003 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | HP-5 | HP-5 | HP-5 | SPB-1 | SPB-1 |
Column length (m) | 60. | 25. | 25. | 30. | 30. |
Carrier gas | Helium | Helium | He | He | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.32 | 0.32 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.53 | 0.53 | 0.25 | 0.25 |
Tstart (C) | 40. | 40. | 40. | 40. | 40. |
Tend (C) | 250. | 280. | 280. | 200. | 200. |
Heat rate (K/min) | 5. | 4. | 4. | 3. | 3. |
Initial hold (min) | 15. | 10. | 10. | ||
Final hold (min) | |||||
I | 985. | 984. | 986. | 965. | 968. |
Reference | Stashenko, Jaramillo, et al., 2003 | Velickovic, Ristic, et al., 2003 | Velickovic, Ristic, et al., 2003 | Vichi, Castellote, et al., 2003 | Vichi, Pizzale, et al., 2003 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | OV-101 | DB-5 | BP-1 | DB-5 | SPB-5 |
Column length (m) | 10. | 30. | 25. | 30. | 30. |
Carrier gas | He | N2 | He | Helium | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.50 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | |
Tstart (C) | 35. | 60. | 60. | 60. | 60. |
Tend (C) | 225. | 280. | 220. | 240. | 250. |
Heat rate (K/min) | 6. | 3. | 5. | 3. | 4. |
Initial hold (min) | 5. | 2. | |||
Final hold (min) | 30. | 10. | 20. | ||
I | 960. | 978. | 967. | 986. | 985. |
Reference | Bloss, Acree, et al., 2002 | Caredda, Marongiu, et al., 2002 | Das, Ram, et al., 2002 | Flamini, Ertugrul, et al., 2002 | Pino, Marbot, et al., 2002 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-5 | Optima-1 | BP-5 | HP-5 | SPB-1 |
Column length (m) | 30. | 25. | 50. | 30. | 30. |
Carrier gas | He | He | H2 | N2 | N2 |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.20 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 1. | 0.25 | 0.25 |
Tstart (C) | 60. | 50. | 60. | 60. | 70. |
Tend (C) | 240. | 250. | 270. | 220. | 180. |
Heat rate (K/min) | 3. | 3. | 6. | 5. | 2. |
Initial hold (min) | 3. | 10. | 2. | ||
Final hold (min) | 1. | ||||
I | 986. | 972. | 994. | 987. | 963. |
Reference | Tellez, Khan, et al., 2002 | Brun, Bessière, et al., 2001 | Doimo, 2001 | Gallori, Flamini, et al., 2001 | Kamath, Asha, et al., 2001 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | OV-101 | SPB-5 | OV-101 | OV-101 | Optima-1 |
Column length (m) | 50. | 60. | 50. | 50. | 25. |
Carrier gas | He | He | N2 | N2 | He |
Substrate | |||||
Column diameter (mm) | 0.2 | 0.32 | 0.25 | 0.25 | 0.20 |
Phase thickness (μm) | 0.5 | 1. | 0.25 | ||
Tstart (C) | 50. | 40. | 80. | 80. | 50. |
Tend (C) | 250. | 200. | 200. | 200. | 250. |
Heat rate (K/min) | 2. | 3. | 2. | 2. | 3. |
Initial hold (min) | 3. | ||||
Final hold (min) | |||||
I | 967. | 985. | 962. | 962. | 973. |
Reference | Orav, Kailas, et al., 2001 | Poligné, Collignan, et al., 2001 | Yang, 2001 | Yang, 2001, 2 | de Beck, Bessière, et al., 2000 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | HP-5 | HP-5 | OV-101 | Methyl Silicone | OV-1 |
Column length (m) | 30. | 60. | 50. | 60. | 25. |
Carrier gas | H2 | He | Nitrogen | H2 | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.32 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 1. | 0.25 | 0.25 | |
Tstart (C) | 40. | 40. | 40. | 40. | 40. |
Tend (C) | 280. | 240. | 200. | 220. | 220. |
Heat rate (K/min) | 3. | 3. | 2. | 5. | 3. |
Initial hold (min) | 10. | 10. | 10. | 5. | |
Final hold (min) | 10. | 5. | |||
I | 988. | 988. | 965. | 966.28 | 977. |
Reference | Bicalho, Pereira, et al., 2000 | García, Martín, et al., 2000 | Tamura, Boonbumrung, et al., 2000 | Baraldi, Rapparini, et al., 1999 | Oberhofer, Nikiforov, et al., 1999 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | Ultra-2 | DB-5 | DB-5 | DB-5 | DB-5 |
Column length (m) | 25. | 60. | 60. | 30. | 30. |
Carrier gas | Helium | ||||
Substrate | |||||
Column diameter (mm) | 0.2 | 0.32 | 0.32 | 0.25 | 0.25 |
Phase thickness (μm) | 1. | 1. | 0.25 | 0.25 | |
Tstart (C) | 40. | 40. | 40. | 60. | 60. |
Tend (C) | 300. | 200. | 200. | 240. | 300. |
Heat rate (K/min) | 5. | 3. | 3. | 3. | 4. |
Initial hold (min) | 4. | 5. | 5. | 2. | |
Final hold (min) | 2. | 2. | 5. | ||
I | 984. | 985. | 987. | 985. | 984.0 |
Reference | Quiroz, Fuentes-Contreras, et al., 1999 | Kondjoyan, Viallon, et al., 1997 | Kondjoyan, Viallon, et al., 1997 | Tellez, Estell, et al., 1997 | Gawdzik, Mardarowicz, et al., 1996 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | BP-1 | BP-1 | HP-5 | HP-101 | OV-101 |
Column length (m) | 25. | 25. | 50. | 50. | |
Carrier gas | N2 | N2 | H2 | ||
Substrate | |||||
Column diameter (mm) | 0.50 | 0.50 | 0.32 | 0.25 | |
Phase thickness (μm) | 0.3 | ||||
Tstart (C) | 60. | 60. | 35. | 65. | 80. |
Tend (C) | 220. | 220. | 200. | 300. | 200. |
Heat rate (K/min) | 5. | 5. | 6. | 2. | 2. |
Initial hold (min) | 2. | 5. | |||
Final hold (min) | |||||
I | 967. | 967. | 991. | 961. | 962. |
Reference | Rajeswara, Kaul, et al., 1996 | Rajeswara, Kaul, et al., 1996 | Larsen and Frisvad, 1995 | Demarne and van der Walt, 1993 | Tamura, Yang, et al., 1993 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | OV-101 | OV-101 | DB-1 | DB-1 | DB-1 |
Column length (m) | 50. | 54. | 60. | 60. | 60. |
Carrier gas | He | He | |||
Substrate | |||||
Column diameter (mm) | 0.25 | 0.26 | 0.32 | 0.32 | |
Phase thickness (μm) | 1.2 | ||||
Tstart (C) | 80. | 50. | 30. | 50. | 30. |
Tend (C) | 200. | 230. | 240. | 230. | 200. |
Heat rate (K/min) | 2. | 3. | 3. | 4. | 4. |
Initial hold (min) | 10. | 25. | |||
Final hold (min) | 10. | 30. | |||
I | 965. | 970. | 966. | 966. | 961. |
Reference | Tamura, Yang, et al., 1993 | Zenkevich and Kulikova, 1993 | Ciccioli, Cecinato, et al., 1992 | Binder, Turner, et al., 1990 | Buttery, Takeoka, et al., 1990 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-1 | OV-101 | OV-101 | OV-101 | OV-101 |
Column length (m) | 60. | 50. | 50. | 50. | 50. |
Carrier gas | He | N2 | N2 | N2 | N2 |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | |||||
Tstart (C) | 30. | 80. | 80. | 80. | 80. |
Tend (C) | 200. | 200. | 200. | 200. | 200. |
Heat rate (K/min) | 4. | 2. | 2. | 2. | 2. |
Initial hold (min) | 25. | ||||
Final hold (min) | 5. | ||||
I | 961. | 963. | 963. | 965. | 960. |
Reference | Buttery, Teranishi, et al., 1990 | Yang and Sugisawa, 1990 | Yang and Sugisawa, 1990 | Sugisawa, Yamamoto, et al., 1989 | Sugisawa, Yang, et al., 1989 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | OV-101 | OV-101 | OV-101 | OV-101 | OV-1 |
Column length (m) | 50. | 50. | 50. | 50. | 40. |
Carrier gas | N2 | He | |||
Substrate | |||||
Column diameter (mm) | 0.25 | 0.30 | 0.30 | 0.30 | 0.5 |
Phase thickness (μm) | 0.75 | ||||
Tstart (C) | 80. | 40. | 40. | 40. | 30. |
Tend (C) | 200. | 230. | 230. | 230. | 220. |
Heat rate (K/min) | 2. | 3.5 | 3.5 | 3.5 | 3. |
Initial hold (min) | 5. | 5. | 5. | ||
Final hold (min) | |||||
I | 963. | 968. | 972. | 987. | 975. |
Reference | Sugisawa, Yang, et al., 1989 | Nykanen, 1986 | Nykanen, 1986 | Nykanen, 1986 | de Pooter, de Buyck, et al., 1986 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|
Active phase | DB-1 | DB-1 | DB-1 | OV-1 |
Column length (m) | 50. | 50. | 60. | 183. |
Carrier gas | N2 | |||
Substrate | ||||
Column diameter (mm) | 0.32 | 0.32 | 0.32 | 0.762 |
Phase thickness (μm) | ||||
Tstart (C) | 0. | 50. | 50. | 0. |
Tend (C) | 250. | 250. | 250. | 230. |
Heat rate (K/min) | 3. | 3. | 4. | 1. |
Initial hold (min) | 0.1 | |||
Final hold (min) | 5. | |||
I | 961. | 963. | 961. | 962. |
Reference | Habu, Flath, et al., 1985 | Habu, Flath, et al., 1985 | Flath, Mon, et al., 1983 | Schreyen, Dirinck, et al., 1979 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
References
Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
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Rout, Naik, et al., 2006
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Sajjadi, 2006
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. [all data]
Schlumpberger B.O., Clery R.A., et al., 2006
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. [all data]
Silva, Oliveira, et al., 2006
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Valette, Fernandez, et al., 2006
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Chemical composition of the volatile extracts from Brassica oleracea L. var. botrytis 'Romanesco' cauliflower seeds,
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. [all data]
Wohlmuth, Smith, et al., 2006
Wohlmuth, H.; Smith, M.K.; Brooks, L.O.; Myers, S.P.; Leach, D.N.,
Essential oil composition of diploid and tetraploid clones of ginger (Zingiber officinale Roscoe) grown in Australia,
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. [all data]
Askari and Sefidkon, 2005
Askari, F.; Sefidkon, F.,
Volatile components of Pimpinella tragium Vill. from Iran,
Iran. J. Pharm. Res., 2005, 2, 117-120. [all data]
Bendimerad and Bendiab, 2005
Bendimerad, N.; Bendiab, S.A.T.,
Composition and antibacterial activity of Pseudocytisus integrifolius (Salisb.) essential oil from Algeria,
J. Agric. Food Chem., 2005, 53, 8, 2947-2952, https://doi.org/10.1021/jf047937u
. [all data]
Chagonda and Chalchat, 2005
Chagonda, L.S.; Chalchat, J.-C.,
The essential oil of wild and cultivated Hoslundia opposita Vahl. from Zimbabwe,
Flavour Fragr. J., 2005, 20, 2, 193-195, https://doi.org/10.1002/ffj.1402
. [all data]
Chagonda and Chalchat, 2005, 2
Chagonda, L.S.; Chalchat, J.-C.,
The essential oil of the fruit of Garcinia huillensis Welw. ex. Oliv. from Zimbabwe,
Flavour Fragr. J., 2005, 20, 3, 313-315, https://doi.org/10.1002/ffj.1420
. [all data]
Dickschat, Bode, et al., 2005
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Flavour Fragr. J., 1996, 11, 5, 289-293, https://doi.org/10.1002/(SICI)1099-1026(199609)11:5<289::AID-FFJ590>3.0.CO;2-7
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Notes
Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References
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