p-Xylene

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Normal alkane RI, polar column, isothermal

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Carbowax 20MCarbowax 20MCarbowax 20MCarbowax 20MDB-Wax
Column length (m) 30.30.30.30.50.
Carrier gas HeliumHeliumHeliumHeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.250.250.251.
Temperature (C) 100.120.60.80.60.
I 1165.1176.1142.1153.1155.
ReferenceSun, Siepmann, et al., 2006Sun, Siepmann, et al., 2006Sun, Siepmann, et al., 2006Sun, Siepmann, et al., 2006Shimadzu, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase PEG-40MPEG-40MPEG-40MPEG-40MPEG-40M
Column length (m) 50.50.50.50.50.
Carrier gas      
Substrate      
Column diameter (mm)      
Phase thickness (μm)      
Temperature (C) 100.100.120.140.60.
I 1150.1154.1168.1178.1132.
ReferenceNesterov, Nesterova, et al., 2000Nesterov, Nesterova, et al., 2000Nesterov, Nesterova, et al., 2000Nesterov, Nesterova, et al., 2000Nesterov, Nesterova, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase PEG-40MCarbowax 20M
Column length (m) 50. 
Carrier gas   
Substrate   
Column diameter (mm)   
Phase thickness (μm)   
Temperature (C) 80.90.
I 1141.1119.
ReferenceNesterov, Nesterova, et al., 2000Sutter, Peterson, et al., 1997
Comment MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, polar column, isothermal, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Sun, Siepmann, et al., 2006
Sun, L.; Siepmann, J.I.; Klotz, W.L.; Schure, M.R., retention in gas-liquid chromatography with a polyethylene oxide stationary phase: molecular simulation and experiment, J. Chromatogr. A, 2006, 1126, 1-2, 373-380, https://doi.org/10.1016/j.chroma.2006.05.084 . [all data]

Shimadzu, 2003
Shimadzu, Gas chromatography analysis of organic solvents using capillary columns (No. 3), 2003, retrieved from http://www.shimadzu.com/apps/form.cfm. [all data]

Nesterov, Nesterova, et al., 2000
Nesterov, I.A.; Nesterova, T.N.; Pimerzin, A.A.; Tsvetkov, V.S., Thermodynamics of alkylbenzene sorption and evaporation. IV. Enthalpies of evaporation and thermodynamics chracteristics of sorption by stationary phases OV-101 and PEG-40M, Izvestia vysshikh uchebnykh zavedenii. Khimia i khimicheskaia tekhnologia (Chemistry and chemical technology), 2000, 43, 4, 39-45. [all data]

Sutter, Peterson, et al., 1997
Sutter, J.M.; Peterson, T.A.; Jurs, P.C., Prediction of gas chromatographic retention indices of alkylbenzenes, Anal. Chim. Acta., 1997, 342, 2-3, 113-122, https://doi.org/10.1016/S0003-2670(96)00578-8 . [all data]


Notes

Go To: Top, Normal alkane RI, polar column, isothermal, References