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«alpha»-D-Xylopyranose, 4TMS derivative


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillarySE-54180.1762.García-Raso, Martínez-Castro, et al., 1987Column length: 40. m; Column diameter: 0.18 mm
CapillarySE-54180.1762.Paez, Martínez-Castro, et al., 1987Column length: 45. m; Column diameter: 0.18 mm
PackedSE-30210.1729.Saura-Calixto, Cañellas, et al., 1984N2, Supelcoport (80-100mesh); Column length: 3. m

Kovats' RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-5MS1734.Medeiros and Simoneit, 200730. m/0.25 mm/0.25 «mu»m, He, 65. C @ 2. min, 6. K/min, 300. C @ 15. min

Kovats' RI, polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillaryCarbowax 20M160.1630.García-Raso, Martínez-Castro, et al., 1987Column length: 25. m; Column diameter: 0.22 mm

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryVF-5MS1703.7Tretyakov, 201130. m/0.25 mm/0.25 «mu»m, He; Tstart: 60. C; Tend: 270. C

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

García-Raso, Martínez-Castro, et al., 1987
García-Raso, A.; Martínez-Castro, I.; Páez, M.I.; Sanz, J.; García-Raso, J.; Saura-Calixto, F., Gas Chromatographic Behaviour of Carbohydrate Trimethylsilyl Ethers. I. Aldopentoses, J. Chromatogr., 1987, 398, 9-20, https://doi.org/10.1016/S0021-9673(01)96491-X . [all data]

Paez, Martínez-Castro, et al., 1987
Paez, M.; Martínez-Castro, I.; Sanz, J.; Olano, A.; García-Raso, A.; Saura-Calixto, F., Identification of the components of aldoses in a tautomeric equilibrium mixture as their trimethylsilyl ethers by capillary cas chromatography, Chromatographia, 1987, 23, 1, 43-46, https://doi.org/10.1007/BF02310417 . [all data]

Saura-Calixto, Cañellas, et al., 1984
Saura-Calixto, F.; Cañellas, J.; García-Raso, A., Gas chromatograph analysis of surgars and sugar-alcohols in the mesocarp, endocarp, and kernel of almond fruit, J. Agric. Food Chem., 1984, 32, 5, 1018-1020, https://doi.org/10.1021/jf00125a017 . [all data]

Medeiros and Simoneit, 2007
Medeiros, P.M.; Simoneit, B.R.T., Analysis of sugars in environmental samples by gas chromatography-mass spectrometry, J. Chromatogr. A, 2007, 1141, 2, 271-278, https://doi.org/10.1016/j.chroma.2006.12.017 . [all data]

Tretyakov, 2011
Tretyakov, K.V., Retention Data (March 2011). NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2011. [all data]


Notes

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