Pentanoic acid, 5-hydroxy-2-propyl, bis-TMS


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-51484.Kimura, Yamamoto, et al., 199930. m/0.25 mm/1. μm, He, 100. C @ 4. min, 4. K/min, 290. C @ 10. min
PackedOV-11484.Tanaka, Hine, et al., 1980N2, 100-120 mesh, 70. C @ 0.5 min, 28. K/min; Column length: 1.8 m; Tend: 290. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-11462.Rettenmeier, Howald, et al., 198960. m/0.32 mm/0.25 μm, He; Program: 40 0C "rapidly" -> 80 0C 2 0C/min -> 120 0C 4 0C/min -> 180 0C "rapidly" -> 250 0C
PackedOV-1011484.Tanaka and Hine, 1982Program: not specified

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Kimura, Yamamoto, et al., 1999
Kimura, M.; Yamamoto, T.; Yamaguchi, S., Automated metabolic profiling and interpretation of GC/MS data for organic acidemia screening: a personal computer-based system, Tohoku J. Exp. Med., 1999, 188, 4, 317-334, https://doi.org/10.1620/tjem.188.317 . [all data]

Tanaka, Hine, et al., 1980
Tanaka, K.; Hine, D.G.; West-Dull, A.; Lynn, T.B., Gas-chromatographic method of analysis for urinary organic acids. I. Retention indices of 155 metabolically important compounds, Clin. Chem., 1980, 26, 13, 1839-1846. [all data]

Rettenmeier, Howald, et al., 1989
Rettenmeier, A.W.; Howald, W.N.; Levy, R.H.; Witek, D.J.; Gordon, W.P.; Porubek, D.J.; Baillie, T.A., Quantitative metabolic profiling of valproic acid in humans using automated gas chromatographic/mass spectrometric techniques, Biomed. Environ. Mass Spectrom., 1989, 18, 3, 192-199, https://doi.org/10.1002/bms.1200180308 . [all data]

Tanaka and Hine, 1982
Tanaka, K.; Hine, D.G., Compilation of Gas Chromatographic Retention Indices of 163 Metabolically Important Organic Acids, and Their Use in Detection of Patients with Organic Acidurias, J. Chromatogr., 1982, 239, 301-322, https://doi.org/10.1016/S0021-9673(00)81990-1 . [all data]


Notes

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