1-Tricosanol, TMS derivative
- Formula: C26H56OSi
- Molecular weight: 412.8077
- IUPAC Standard InChI: InChI=1S/C26H56OSi/c1-5-6-7-8-9-10-11-12-13-14-15-16-17-18-19-20-21-22-23-24-25-26-27-28(2,3)4/h5-26H2,1-4H3
- IUPAC Standard InChIKey: NRKGQLYZSFTWCP-UHFFFAOYSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: Silane, trimethyl(tricosyloxy)-; Tricosoxy-trimethylsilane; 1-(Trimethylsilyloxy)tricosane; Tricosane, 1-trimethylsilyloxy-; (Tricosyloxy)trimethylsilane; 1-Tricosanol, trimethylsilyl ether; Tricosyl trimethylsilyl ether; 1-Tricosanol, TMS; Tricosan-1-ol trimethylsilyl ether
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | OV-5 | 2630. | García, Sáenz, et al., 1997 | 25. m/0.25 mm/0.23 μm, He, 230. C @ 6. min, 4. K/min; Tend: 300. C |
| Capillary | OV-1 | 2652. | Harvey, 1989 | 50. m/0.30 mm/0.52 μm, He, 2. K/min; Tstart: 130. C; Tend: 280. C |
Van Den Dool and Kratz RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | VF-5MS | 2635.8 | Tret'yakov, 2008 | 30. m/0.25 mm/0.25 μm, He; Program: Multi-step temperature program; T(initial)=60C; T(final)=270C |
| Capillary | VF-5MS | 2639.7 | Zheng and White, 2008 | 30. m/0.25 mm/0.25 μm, He; Program: not specified |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
García, Sáenz, et al., 1997
García, M.D.; Sáenz, M.T.; Ahumada, M.D.; Cert, A.,
Isolation of three triterpenes and several aliphatic alcohols from Crataegus monogyna Jacq.,
J. Chromatogr. A, 1997, 767, 1-2, 340-342, https://doi.org/10.1016/S0021-9673(96)01091-6
. [all data]
Harvey, 1989
Harvey, D.J.,
Identification of long-chain fatty acids and alcohols from human cerumen by the use of picolinyl and nicotinate esters,
Biomed. Environ. Mass Spectrom., 1989, 18, 9, 719-723, https://doi.org/10.1002/bms.1200180912
. [all data]
Tret'yakov, 2008
Tret'yakov, K.V.,
Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2008. [all data]
Zheng and White, 2008
Zheng, Y.; White, E.,
Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2008. [all data]
Notes
Go To: Top, Gas Chromatography, References
- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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