Naringenin, 3TMS derivative


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillaryDB-1280.2861.8Stremple, 199630. m/0.25 mm/0.25 μm, H2
CapillaryDB-5280.2907.9Stremple, 199630. m/0.25 mm/0.25 μm, H2

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryMethyl Silicone2851.Greenaway and Whatley, 199025. m/0.32 mm/0.5 μm, He, 3. K/min; Tstart: 75. C; Tend: 300. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryVF-5MS2872.2Tret'yakov, 200730. m/0.25 mm/0.25 μm, He; Program: Multi-step temperature program; T(initial)=60C; T(final)=270C

Normal alkane RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
PackedOV-1210.2843.Katagi, Horii, et al., 1973Nitrogen; Column length: 2. m

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Stremple, 1996
Stremple, P., Improved separation and identification of aglycon flavonoids by gas chromatography on phenylmethylsilicone copolymers, J. Hi. Res. Chromatogr., 1996, 19, 10, 581-584, https://doi.org/10.1002/jhrc.1240191010 . [all data]

Greenaway and Whatley, 1990
Greenaway, W.; Whatley, F.R., Resolution of complex mixtures of phenolics in poplar bud exudate by analysis of gas chromatography-mass spectrometry data, J. Chromatogr., 1990, 519, 1, 145-158, https://doi.org/10.1016/0021-9673(90)85143-J . [all data]

Tret'yakov, 2007
Tret'yakov, K.V., Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2007. [all data]

Katagi, Horii, et al., 1973
Katagi, T.; Horii, A.; Oomura, Y.; Miyakawa, H.; Kyu, T.; Ikeda, Y.; Isoi, K., Gas chromatography of flavonoids, J. Chromatogr., 1973, 79, 45-56, https://doi.org/10.1016/S0021-9673(01)85272-9 . [all data]


Notes

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