15-Methyltritriacontane


Mass spectrum (electron ionization)

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Spectrum

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Additional Data

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Owner NIST Mass Spectrometry Data Center
Collection (C) 2014 copyright by the U.S. Secretary of Commerce
on behalf of the United States of America. All rights reserved.
Origin J. Klune, Insect Chem. Ecol. Lab., USDA, Beltsville, MD 20705
NIST MS number 131203

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Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-5MS3332.Steiner, Steidle, et al., 200530. m/0.32 mm/0.25 μm, He, 2. K/min; Tstart: 150. C; Tend: 300. C
CapillaryUltra-13332.Nelson, Adams, et al., 2003150. C @ 4. min, 4. K/min, 320. C @ 30. min; Column length: 12. m; Column diameter: 0.2 mm
CapillaryHT-53325.Goh S.H., Ooi K.E., et al., 199325. m/0.53 mm/0.22 μm, N2, 15. K/min, 320. C @ 20. min; Tstart: 150. C
CapillaryHT-53329.Goh S.H., Ooi K.E., et al., 199325. m/0.53 mm/0.22 μm, N2, 15. K/min, 320. C @ 20. min; Tstart: 150. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-13335.Bernier, Carlson, et al., 199830. m/0.32 mm/0.25 μm; Program: 60C (2min) => 10C/min => 220C => 3C/min => 310C

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryBP-13327.Lockey and Oraha, 199012. m/0.22 mm/0.25 μm, Helium, 2. K/min; Tstart: 100. C; Tend: 300. C
CapillaryBP-13333.Lockey and Oraha, 199012. m/0.22 mm/0.25 μm, Helium, 2. K/min; Tstart: 100. C; Tend: 300. C
PackedOV-1013333.Nelson, de Renobales, et al., 1989Helium, Gas-Chrom Q (100-120 mesh), 3. K/min, 320. C @ 25. min; Column length: 3. m; Tstart: 150. C
PackedDexsil 3003329.Lockey, 1976Nitrogen, Chromosorb W (80-100 mesh), 3.3 K/min; Column length: 2. m; Tstart: 80. C; Tend: 340. C
PackedDexsil 3003338.Lockey, 1976Nitrogen, Chromosorb W (80-100 mesh), 3.3 K/min; Column length: 2. m; Tstart: 80. C; Tend: 340. C

Normal alkane RI, non-polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryDB-13335.Carlson, Geden, et al., 199930. m/0.32 mm/0.25 μm, He; Program: 60C (2min) => 10C/min => 220C => 3C/min => 310C (12 - 42 min)
CapillaryCP Sil 5 CB3331.Kenig, Sinninghe Damsté, et al., 199525. m/0.32 mm/0.2 μm, He; Program: 50C => 20C/min => 130C => 4C/min => 300C (20min)
CapillaryDexsil 3003318.Lockey, 1981Column length: 15. m; Program: 50 0C 5 0C/min -> 200 0C 2 0C/min -> 340 0C
CapillaryDexsil 3003329.Lockey, 1981Column length: 15. m; Program: 50 0C 5 0C/min -> 200 0C 2 0C/min -> 340 0C

References

Go To: Top, Mass spectrum (electron ionization), Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Steiner, Steidle, et al., 2005
Steiner, S.; Steidle, J.L.M.; Ruther, J., Female sex pheromone in immature insect males - a case of pre-emergence chemical mimicry?, Behavioral Ecology and Sociobiology, 2005, 58, 2, 111-120, https://doi.org/10.1007/s00265-005-0930-x . [all data]

Nelson, Adams, et al., 2003
Nelson, D.R.; Adams, T.S.; Fatland, C.L., Hydrocarbons in the surface wax of eggs and adults of the Colorado potato beetle, Leptinotarsa decemlineata, Comp. Biochem. Physiol. B: Comp. Biochem., 2003, 134, 3, 447-466, https://doi.org/10.1016/S1096-4959(02)00262-2 . [all data]

Goh S.H., Ooi K.E., et al., 1993
Goh S.H.; Ooi K.E.; Chuah C.H.; Yong H.S.; Khoo S.G.; Ong S.H., Cuticular hydrocarbons from two species of Malaysian Bactrocera fruit flies, Biochem. Syst. Ecol., 1993, 21, 2, 215-226, https://doi.org/10.1016/0305-1978(93)90039-T . [all data]

Bernier, Carlson, et al., 1998
Bernier, U.R.; Carlson, D.A.; Geden, C.J., Gas chromatography/mass spectrometry analysis of the cuticular hydrocarbons from parasitic wasps of the genus Muscidifurax, J. Am. Soc. Mass Spectrom., 1998, 9, 4, 320-332, https://doi.org/10.1016/S1044-0305(97)00288-2 . [all data]

Lockey and Oraha, 1990
Lockey, K.H.; Oraha, V.S., Cuticular lipids of adult Locusta Migratoria Migratoriodes (R and F), Schstocerca Gregaria (Forskal) (Acrididae) and other orthopteran species - II. Hydrocarbons, Comp. Biochem. Physiol., 1990, 95B, 4, 721-744. [all data]

Nelson, de Renobales, et al., 1989
Nelson, D.R.; de Renobales, M.; Dwyer, L.A.; Zamboni, A.C.; Fatland, C.L.; Blomquist, G.J., Novel very long-chain methyl branched alcohols and their esters, and methyl branched alkanes in pupae of the gabbage looper, Trichoplusa ni (Hubner), Insect Biochem., 1989, 19, 2, 197-208, https://doi.org/10.1016/0020-1790(89)90092-9 . [all data]

Lockey, 1976
Lockey, K.H., Cuticular hydrocarbons of Locusta, Schistocerca, and Periplaneta, and their role in waterproofing, Insect Biochem., 1976, 6, 5, 457-472, https://doi.org/10.1016/0020-1790(76)90068-8 . [all data]

Carlson, Geden, et al., 1999
Carlson, D.A.; Geden, C.J.; Bernier, U.R., Identification of pupal exiviae of Nasania vitripennis and Muscidifurax raptorellus parasitoids using cuticular hydrocarbons, Biol. Control, 1999, 15, 2, 97-106, https://doi.org/10.1006/bcon.1999.0708 . [all data]

Kenig, Sinninghe Damsté, et al., 1995
Kenig, F.; Sinninghe Damsté, J.S.; Kock-van Dalen, A.C.; Rijpstra, W.I.C.; Huc, A.Y.; de Leeuw, J.W., Occurrence and origin of mono-, di-, and trimethylalkanes in modern and holocene cyanobacterial mats from Abu Dhabi, United Arab Emirates, Geochim. Cosmochim. Acta, 1995, 59, 14, 2999-3015, https://doi.org/10.1016/0016-7037(95)00190-5 . [all data]

Lockey, 1981
Lockey, K.H., Cuticular hydrocarbons of adult Cylindrinotus laevioctostriatus (Goeze) and Phylan gibbus (Fabricius) (Coleoptera: Tenebrionidae), Insect. Biochem., 1981, 11, 5, 549-561, https://doi.org/10.1016/0020-1790(81)90023-8 . [all data]


Notes

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