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3-Methyltricosane


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillaryDB-1250.2374.Szafranek, Malinski, et al., 2001Ar; Column length: 30. m; Column diameter: 0.28 mm
CapillaryDexsil 300210.2366.Szafranek, Kusmierz, et al., 1982He; Column length: 30. m; Column diameter: 0.30 mm
CapillaryDexsil 300210.2372.Szafranek, Kusmierz, et al., 1982He; Column length: 30. m; Column diameter: 0.30 mm

Kovats' RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-5MS2372.Kenig, Simons, et al., 200530. m/0.25 mm/0.25 «mu»m, He; Program: 60C(1.5min) => 20C/min => 130C => 4C/min => 315C (90min)

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-5MS2372.Steinmetz, Schmolz, et al., 200330. m/0.32 mm/0.25 «mu»m, He, 3. K/min; Tstart: 150. C; Tend: 280. C
CapillaryDB-52371.Ruther, Sieben, et al., 199830. m/0.32 mm/0.25 «mu»m, He, 3. K/min; Tstart: 150. C; Tend: 280. C
CapillaryCross-Linked Methylsilicone2374.Khorasheh, Gray, et al., 19895. K/min; Tstart: 40. C; Tend: 300. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-52375.Zaikin and Borisov, 2002He; Column length: 30. m; Column diameter: 0.25 mm; Program: 30C => 5K/min=120C => 10C/min => 270C

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryOV-12374.7Krkosova, Kubinec, et al., 2007100. m/0.32 mm/0.25 «mu»m, Helium, 5. K/min, 310. C @ 5. min; Tstart: 30. C
CapillaryHP-52374.Farsam, Amanlou, et al., 200330. m/0.25 mm/0.25 «mu»m, Helium, 60. C @ 2. min, 4. K/min; Tend: 240. C
CapillaryDB-12374.Katritzky, Chen, et al., 200030. m/0.32 mm/0.25 «mu»m; Tstart: 60. C; Tend: 320. C
CapillaryOV-12375.Hebanowska, Malinski, et al., 19902. K/min; Column length: 40. m; Column diameter: 0.25 mm; Tstart: 140. C; Tend: 300. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryPolydimethyl siloxane2374.Junkes, Castanho, et al., 2003Program: not specified
CapillaryCP Sil 5 CB2371.Kenig, Sinninghe Damsté, et al., 199525. m/0.32 mm/0.2 «mu»m, He; Program: 50C => 20C/min => 130C => 4C/min => 300C (20min)

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Szafranek, Malinski, et al., 2001
Szafranek, B.; Malinski, E.; Nawrot, J.; Sosnowska, D.; Ruszkowska, M.; Pihlaja, K.; Trumpakaj, Z.; Szafranek, J., In Vitro effects of cuticular lipids of the aphids Sitobion avenae, Hyalopterus pruni and Brevicoryne brassicae on growth and sporulation of the Paecilomyces fumosoroseus and Beauveria bassiana, Arkivoc, 2001, 2001, 3, 81-94, https://doi.org/10.3998/ark.5550190.0002.311 . [all data]

Szafranek, Kusmierz, et al., 1982
Szafranek, J.; Kusmierz, J.; Czerwiec, W., Gas chromatographic-mass spectrometric investigations of high-boiling crude oil alkane fractions, J. Chromatogr., 1982, 245, 2, 219-228, https://doi.org/10.1016/S0021-9673(00)88591-X . [all data]

Kenig, Simons, et al., 2005
Kenig, F.; Simons, D.-J.H.; Crich, D.; Cowen, J.P.; Ventura, G.T.; Rehbein-Khalily, T., Structure and distribution of branched aliphatic alkanes with quaternary carbon atoms in Cenomanian and Turonian black shales of Pasquia Hills (Saskatchewan, Canada), Org. Geochem., 2005, 36, 1, 117-138, https://doi.org/10.1016/j.orggeochem.2004.06.014 . [all data]

Steinmetz, Schmolz, et al., 2003
Steinmetz, I.; Schmolz, E.; Ruther, J., Cuticular lipids as trail pheromone in a social wasp, Proc. R. Soc. London B:, 2003, 270, 1513, 385-391, https://doi.org/10.1098/rspb.2002.2256 . [all data]

Ruther, Sieben, et al., 1998
Ruther, J.; Sieben, S.; Schricker, B., Role of cuticular lipids in nestmate recognition of the European hornet Vespa crabro L. (Hymenoptera, Vespidae), Insectes Soc., 1998, 45, 2, 169-179, https://doi.org/10.1007/s000400050077 . [all data]

Khorasheh, Gray, et al., 1989
Khorasheh, F.; Gray, M.R.; Selucky, M.L., Correlation for Kováts retention index of C9-C26 monoalkyl and polymethyl alkanes and alkenes, J. Chromatogr., 1989, 481, 1-16, https://doi.org/10.1016/S0021-9673(01)96747-0 . [all data]

Zaikin and Borisov, 2002
Zaikin, V.G.; Borisov, R.S., Chromatographic-mass spectrometric analysis of Fishcer-Tropsch synthesis products, J. Anal. Chem. USSR (Engl. Transl.), 2002, 57, 6, 544-551. [all data]

Krkosova, Kubinec, et al., 2007
Krkosova, Z.; Kubinec, R.; Addova, G.; Jurdakova, H.; Blasko, J.; Ostrovsky, I.; Sojak, L., Gas chromatographic - mass spectrometric characterization of monomethylalkanes from fuel diesel, Petroleum Coal, 2007, 49, 3, 51-62. [all data]

Farsam, Amanlou, et al., 2003
Farsam, H.; Amanlou, M.; Amin, G.; Nezamivand-Chegini, G.; Salehi-Surmaghi, M.-H.; Shafiee, A., Anatomical and phytochemical study of Lilium Ledebourii (Baker) Boiss., a rare endemic species in Iran, DARU, 2003, 11, 4, 164-170. [all data]

Katritzky, Chen, et al., 2000
Katritzky, A.R.; Chen, K.; Maran, U.; Carlson, D.A., QSPR Correlation and predictions of GC retention indexes for methyl-branched hydrocarbons produced by insects, Anal. Chem., 2000, 72, 1, 101-109, https://doi.org/10.1021/ac990800w . [all data]

Hebanowska, Malinski, et al., 1990
Hebanowska, E.; Malinski, E.; Dubis, E.; Oksman, P.; Pihlaja, K.; Nawrot, J.; Szafranek, J., The cuticular hydrocarbons of the larvae of Anagasta kuehniella Z., Comp. Biochem. Physiol. B: Comp. Biochem., 1990, 95, 4, 699-703. [all data]

Junkes, Castanho, et al., 2003
Junkes, B.S.; Castanho, R.D.M.; Amboni, C.; Yunes, R.A.; Heinzen, V.E.F., Semiempirical Topological Index: A Novel Molecular Descriptor for Quantitative Structure-Retention Relationship Studies, Internet Electronic Journal of Molecular Design, 2003, 2, 1, 33-49. [all data]

Kenig, Sinninghe Damsté, et al., 1995
Kenig, F.; Sinninghe Damsté, J.S.; Kock-van Dalen, A.C.; Rijpstra, W.I.C.; Huc, A.Y.; de Leeuw, J.W., Occurrence and origin of mono-, di-, and trimethylalkanes in modern and holocene cyanobacterial mats from Abu Dhabi, United Arab Emirates, Geochim. Cosmochim. Acta, 1995, 59, 14, 2999-3015, https://doi.org/10.1016/0016-7037(95)00190-5 . [all data]


Notes

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