β-Testosterone, TMS
- Formula: C25H44O2Si2
- Molecular weight: 432.7867
- IUPAC Standard InChI: InChI=1S/C25H44O2Si2/c1-24-15-13-19(26-28(3,4)5)17-18(24)9-10-20-21-11-12-23(27-29(6,7)8)25(21,2)16-14-22(20)24/h13,17,20-23H,9-12,14-16H2,1-8H3/t20?,21?,22?,23-,24?,25?/m1/s1
- IUPAC Standard InChIKey: OGAHQMPXQGCDNO-MCZOVZSXSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Stereoisomers:
- Other names: Testosterone, bis-TMS (2,4-diene); Androst-4-en-3-on-17B-ol, TMS
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Kovats' RI, non-polar column, isothermal
| Column type | Active phase | Temperature (C) | I | Reference | Comment |
|---|---|---|---|---|---|
| Packed | OV-1 | 210. | 2630. | Brooks, Thawley, et al., 1971 |
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | HP-1 | 2606. | Schänzer, Horning, et al., 1995 | 17. m/0.2 mm/0.11 μm, He, 5. K/min; Tstart: 180. C; Tend: 320. C |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Brooks, Thawley, et al., 1971
Brooks, C.J.W.; Thawley, A.R.; Rocher, P.; Middleditch, B.S.; Anthony, G.M.; Stillwell, W.G.,
Characterization of Steroidal Drug Metabolites by Combined Gas Chromatography-Mass Spectrometry,
J. Chromatogr. Sci., 1971, 9, 1, 35-43, https://doi.org/10.1093/chromsci/9.1.35
. [all data]
Schänzer, Horning, et al., 1995
Schänzer, W.; Horning, S.; Donike, M.,
Metabolism of anabolic steroids in humans: Synthesis of 6β-hydroxy metabolites of 4-chloro-1,2-dehydro-17α -methyltestosterone, fluoxymesterone, and metandienone,
Steroids, 1995, 60, 4, 353-366, https://doi.org/10.1016/0039-128X(95)00008-E
. [all data]
Notes
Go To: Top, Gas Chromatography, References
- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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