GA86, MeTMSi
- Formula: C32H58O8Si4
- Molecular weight: 683.1401
- IUPAC Standard InChI: InChI=1S/C32H58O8Si4/c1-20-26(39-43(10,11)12)30-19-32(20,40-44(13,14)15)23(38-42(7,8)9)18-21(30)31-17-16-22(37-41(4,5)6)29(2,28(34)36-31)25(31)24(30)27(33)35-3/h21-26H,1,16-19H2,2-15H3/t21?,22-,23-,24+,25?,26+,29+,30+,31+,32-/m1/s1
- IUPAC Standard InChIKey: QYEAQQUMULDDTF-VWTZYVOOSA-N
- Chemical structure:
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Van Den Dool and Kratz RI, non-polar column, custom temperature program
Go To: Top, References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
| Column type | Capillary | Capillary | Capillary |
|---|---|---|---|
| Active phase | XTI-5 | CP Sil 5 CB | DB-1 |
| Column length (m) | 30. | 25. | 15. |
| Carrier gas | He | He | |
| Substrate | |||
| Column diameter (mm) | 0.25 | 0.25 | 0.22 |
| Phase thickness (μm) | 0.25 | 0.25 | |
| Program | 60C(1min) => 20C/min => 220C => 4C/min => 300C | 50C(1min) => 15C/min => 220C => 2C/min => 300C | 60(0.1 min)-200 0C at 20 deg/min; 200-300 0C at 5 deg/min |
| I | 2996. | 2984. | 2975. |
| Reference | Blake, Browning G., et al., 2000 | Blake and Browning, 1994 | Pearce, Koshioka, et al., 1994 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI |
References
Go To: Top, Van Den Dool and Kratz RI, non-polar column, custom temperature program, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Blake, Browning G., et al., 2000
Blake, P.S.; Browning G.; Benjamin, L.J.; Mander, L.N.,
Gibberellins in seedlings and flowering trees of Prunus avium L.,
Phytochemistry, 2000, 53, 4, 519-528, https://doi.org/10.1016/S0031-9422(99)00597-X
. [all data]
Blake and Browning, 1994
Blake, P.S.; Browning, G.,
Gibberellins in developing fruits of Prunus avium,
Phytochemistry, 1994, 35, 6, 1383-1386, https://doi.org/10.1016/S0031-9422(00)86860-0
. [all data]
Pearce, Koshioka, et al., 1994
Pearce, D.W.; Koshioka, M.; Pharis, R.P.,
Chromatography of gibberellins,
J. Chromatogr. A, 1994, 658, 1, 91-122, https://doi.org/10.1016/0021-9673(94)85210-3
. [all data]
Notes
Go To: Top, Van Den Dool and Kratz RI, non-polar column, custom temperature program, References
- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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