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GA5, MeTMS


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-12482.Nakayama, Yokota, et al., 1996He; Column length: 15. m; Column diameter: 0.258 mm; Program: 130C (2min) => 32C/min => 220C (4min) => 8C/min => 270C (5min)

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryOV-12479.Davis, Kobayashi, et al., 199925. m/0.2 mm/0.25 «mu»m, He; Program: 60C(2min) => 10C/min => 150C => 3C/min => 300C(10min)
CapillaryCP-Sil5 CB MS2512.Roberts, Blake, et al., 1999He; Column length: 25. m; Column diameter: 0.25 mm; Program: 90C(1min) => 20C/min => 220C => 4C/min => 290C
CapillaryCP-Sil5 CB MS2513.Roberts, Blake, et al., 1999He; Column length: 25. m; Column diameter: 0.25 mm; Program: 90C(1min) => 20C/min => 220C => 4C/min => 290C
CapillaryOV-12485.Spray, Kobayashi, et al., 199625. m/0.2 mm/0.25 «mu»m, He; Program: 60C(2min) => 10min/C => 150C => 3C/min => 300C
CapillaryCP Sil 5 CB2512.Blake and Browning, 1994He; Column length: 25. m; Column diameter: 0.25 mm; Program: 50C(1min) => 15C/min => 220C => 2C/min => 300C
CapillaryCP Sil 5 CB2513.Blake and Browning, 1994He; Column length: 25. m; Column diameter: 0.25 mm; Program: 50C(1min) => 15C/min => 220C => 2C/min => 300C
CapillaryDB-12495.Pearce, Koshioka, et al., 199415. m/0.22 mm/0.25 «mu»m; Program: 60(0.1 min)-200 0C at 20 deg/min; 200-300 0C at 5 deg/min
CapillaryCP Sil 5 CB2510.Taylor, Blake, et al., 1994He; Column length: 25. m; Column diameter: 0.25 mm; Program: 60C(0.3min) => 20C/min => 220C => 4C/min => 300C
CapillaryCP Sil 5 CB2510.Taylor, Blake, et al., 1994He; Column length: 25. m; Column diameter: 0.25 mm; Program: 60C(0.3min) => 20C/min => 220C => 4C/min => 300C
CapillaryOV-12476.Waycott, Smith, et al., 199125. m/0.22 mm/0.25 «mu»m; Program: 60C(2min) => 10C/min => 150C => 3C/min => 310C

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-52534.Koshioka, Pharis, et al., 198815. m/0.25 mm/0.25 «mu»m, 25. K/min; Tstart: 60. C; Tend: 250. C
CapillaryDB-52534.Koshioka, Pharis, et al., 198815. m/0.25 mm/0.25 «mu»m, 25. K/min; Tstart: 60. C; Tend: 250. C
CapillaryDB-52534.Koshioka, Pharis, et al., 198815. m/0.25 mm/0.25 «mu»m, 25. K/min; Tstart: 60. C; Tend: 250. C
CapillaryDB-52534.Koshioka, Pharis, et al., 198815. m/0.25 mm/0.25 «mu»m, 25. K/min; Tstart: 60. C; Tend: 250. C
CapillaryDB-52534.Koshioka, Pharis, et al., 198815. m/0.25 mm/0.25 «mu»m, 25. K/min; Tstart: 60. C; Tend: 250. C
CapillaryDB-52534.Koshioka, Pharis, et al., 198815. m/0.25 mm/0.25 «mu»m, 25. K/min; Tstart: 60. C; Tend: 250. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryUltra-22466.Talon, Zeevaart, et al., 199125. m/0.32 mm/0.52 «mu»m; Program: 50C => 40C/min => 220C => 8C/min => 280C

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Nakayama, Yokota, et al., 1996
Nakayama, M.; Yokota, T.; Sohma, R.; Mander, L.N.; Twitchin, B.; Komatsu, H.; Matsui, H.; Bukovac, M.J., Gibberellins in immature seed of Prunus cerasus: structure determination and synthesis of gibberellin, GA95 (1,2-didehydro-GA20), Phytochemistry, 1996, 42, 4, 913-920, https://doi.org/10.1016/0031-9422(96)00035-0 . [all data]

Davis, Kobayashi, et al., 1999
Davis, G.; Kobayashi, M.; Phinney, B.O.; Lange, T.; Croker, S.J.; Gaskin, P.; MacMillan, J., Gibberellin biosynthesis in maize. Metabolic studies with GA15, GA24, GA25, GA7, and 2,3-dehydro-GA9, Plant Physiol., 1999, 121, 3, 1037-1045, https://doi.org/10.1104/pp.121.3.1037 . [all data]

Roberts, Blake, et al., 1999
Roberts, A.V.; Blake, P.S.; Lewis, R.; Taylor, J.M.; Dunstan, D.I., The effect of gibberellins on flowering in roses, J. Plant Growth Regul., 1999, 18, 3, 113-119, https://doi.org/10.1007/PL00007058 . [all data]

Spray, Kobayashi, et al., 1996
Spray, C.R.; Kobayashi, M.; Suzuki, Y.; Phinney, B.O.; Gaskin, P.; MacMillan, J., The dwarf-1 (dl) mutant of Zea mays blocks three steps in the gibberellin-biosynthetic pathway, Proc. Nat. Acad. Sci. U.S.A., 1996, 93, 19, 10515-10518, https://doi.org/10.1073/pnas.93.19.10515 . [all data]

Blake and Browning, 1994
Blake, P.S.; Browning, G., Gibberellins in developing fruits of Prunus avium, Phytochemistry, 1994, 35, 6, 1383-1386, https://doi.org/10.1016/S0031-9422(00)86860-0 . [all data]

Pearce, Koshioka, et al., 1994
Pearce, D.W.; Koshioka, M.; Pharis, R.P., Chromatography of gibberellins, J. Chromatogr. A, 1994, 658, 1, 91-122, https://doi.org/10.1016/0021-9673(94)85210-3 . [all data]

Taylor, Blake, et al., 1994
Taylor, D.R.; Blake, P.S.; Browning, G., Identification of gibberellins in leaf tissues of strawberry (Fragaria × ananassa Duch.) grown under different photoperiods, Plant Growth Regul., 1994, 15, 3, 235-240, https://doi.org/10.1007/BF00029896 . [all data]

Waycott, Smith, et al., 1991
Waycott, W.; Smith, V.A.; Gaskin, P.; MacMillan, J.; Taiz, L., The endogenous gibberellins of dwarf mutants of lettuce, Plant Physiol., 1991, 95, 4, 1169-1173, https://doi.org/10.1104/pp.95.4.1169 . [all data]

Koshioka, Pharis, et al., 1988
Koshioka, M.; Pharis, R.P.; Matsuta, N.; Mander, L.N., Metabolism of [3H]gibberellin A5 and [2H]gibberellin A5 in cell suspension cultures of prunus persica, Phytochemistry, 1988, 27, 12, 3799-3805, https://doi.org/10.1016/0031-9422(88)83020-6 . [all data]

Talon, Zeevaart, et al., 1991
Talon, M.; Zeevaart, J.A.D.; Gage, D.A., Identification of gibberellins in spinach and effects of light and darkness on their levels, Plant Physiol., 1991, 97, 4, 1521-1526, https://doi.org/10.1104/pp.97.4.1521 . [all data]


Notes

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