GA5, MeTMS


Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1CP-Sil5 CB MSCP-Sil5 CB MSOV-1CP Sil 5 CB
Column length (m) 25.25.25.25.25.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.20.250.250.20.25
Phase thickness (μm) 0.25  0.25 
Program 60C(2min) => 10C/min => 150C => 3C/min => 300C(10min)90C(1min) => 20C/min => 220C => 4C/min => 290C90C(1min) => 20C/min => 220C => 4C/min => 290C60C(2min) => 10min/C => 150C => 3C/min => 300C50C(1min) => 15C/min => 220C => 2C/min => 300C
I 2479.2512.2513.2485.2512.
ReferenceDavis, Kobayashi, et al., 1999Roberts, Blake, et al., 1999Roberts, Blake, et al., 1999Spray, Kobayashi, et al., 1996Blake and Browning, 1994
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-1CP Sil 5 CBCP Sil 5 CBOV-1
Column length (m) 25.15.25.25.25.
Carrier gas He HeHe 
Substrate      
Column diameter (mm) 0.250.220.250.250.22
Phase thickness (μm)  0.25  0.25
Program 50C(1min) => 15C/min => 220C => 2C/min => 300C60(0.1 min)-200 0C at 20 deg/min; 200-300 0C at 5 deg/min60C(0.3min) => 20C/min => 220C => 4C/min => 300C60C(0.3min) => 20C/min => 220C => 4C/min => 300C60C(2min) => 10C/min => 150C => 3C/min => 310C
I 2513.2495.2510.2510.2476.
ReferenceBlake and Browning, 1994Pearce, Koshioka, et al., 1994Taylor, Blake, et al., 1994Taylor, Blake, et al., 1994Waycott, Smith, et al., 1991
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Davis, Kobayashi, et al., 1999
Davis, G.; Kobayashi, M.; Phinney, B.O.; Lange, T.; Croker, S.J.; Gaskin, P.; MacMillan, J., Gibberellin biosynthesis in maize. Metabolic studies with GA15, GA24, GA25, GA7, and 2,3-dehydro-GA9, Plant Physiol., 1999, 121, 3, 1037-1045, https://doi.org/10.1104/pp.121.3.1037 . [all data]

Roberts, Blake, et al., 1999
Roberts, A.V.; Blake, P.S.; Lewis, R.; Taylor, J.M.; Dunstan, D.I., The effect of gibberellins on flowering in roses, J. Plant Growth Regul., 1999, 18, 3, 113-119, https://doi.org/10.1007/PL00007058 . [all data]

Spray, Kobayashi, et al., 1996
Spray, C.R.; Kobayashi, M.; Suzuki, Y.; Phinney, B.O.; Gaskin, P.; MacMillan, J., The dwarf-1 (dl) mutant of Zea mays blocks three steps in the gibberellin-biosynthetic pathway, Proc. Nat. Acad. Sci. U.S.A., 1996, 93, 19, 10515-10518, https://doi.org/10.1073/pnas.93.19.10515 . [all data]

Blake and Browning, 1994
Blake, P.S.; Browning, G., Gibberellins in developing fruits of Prunus avium, Phytochemistry, 1994, 35, 6, 1383-1386, https://doi.org/10.1016/S0031-9422(00)86860-0 . [all data]

Pearce, Koshioka, et al., 1994
Pearce, D.W.; Koshioka, M.; Pharis, R.P., Chromatography of gibberellins, J. Chromatogr. A, 1994, 658, 1, 91-122, https://doi.org/10.1016/0021-9673(94)85210-3 . [all data]

Taylor, Blake, et al., 1994
Taylor, D.R.; Blake, P.S.; Browning, G., Identification of gibberellins in leaf tissues of strawberry (Fragaria × ananassa Duch.) grown under different photoperiods, Plant Growth Regul., 1994, 15, 3, 235-240, https://doi.org/10.1007/BF00029896 . [all data]

Waycott, Smith, et al., 1991
Waycott, W.; Smith, V.A.; Gaskin, P.; MacMillan, J.; Taiz, L., The endogenous gibberellins of dwarf mutants of lettuce, Plant Physiol., 1991, 95, 4, 1169-1173, https://doi.org/10.1104/pp.95.4.1169 . [all data]


Notes

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