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GA53, MeTMS


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-52503.Morvan-Bertrand, Ernstsen, et al., 2001Program: not specified
CapillaryHP-52504.Morvan-Bertrand, Ernstsen, et al., 2001Program: not specified
CapillaryDB-12493.Koshioka, Miyamoto, et al., 199815. m/0.25 mm/0.25 «mu»m; Program: not specified
CapillaryDB-12503.Tanno, Yokota, et al., 1992Column length: 15. m; Column diameter: 0.258 mm; Program: 130C(2m) => 32C/min => 220(4min) => 8C/min270C(2min)
CapillaryUltra-22464.Talon, Koornneef, et al., 199025. m/0.32 mm/0.52 «mu»m; Program: 50C => 40C/min => 220C => 6C/min => 280C
CapillaryUltra-22468.Talon, Koornneef, et al., 199025. m/0.32 mm/0.52 «mu»m; Program: 50C => 40C/min => 220C => 6C/min => 280C
CapillaryUltra-22468.Talon, Koornneef, et al., 199025. m/0.32 mm/0.52 «mu»m; Program: 50C => 40C/min => 220C => 6C/min => 280C
CapillaryUltra-22468.Talon and Zeevaart, 199025. m/0.32 mm/0.52 «mu»m, He; Program: 50C => 40C/min => 220C => 6C/min => 280C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-12450.Kim, Lee, et al., 200330. m/0.25 mm/0.25 «mu»m, He; Program: 60C (1min) => 15C/min => 200C => 5C/min => 285C
CapillaryHP-12450.Kim, Lee, et al., 200330. m/0.25 mm/0.25 «mu»m, He; Program: 60C (1min) => 15C/min => 200C => 5C/min => 285C
CapillaryOV-12505.Kobayashi, MacMillan, et al., 2000He; Column length: 25. m; Column diameter: 0.2 mm; Program: 60C(2min) => 13C/min => 150C => 3C/min => 280C(10min)
CapillaryDB-12495.Hisamatsu, Koshioka, et al., 199815. m/0.25 mm/0.33 «mu»m; Program: 120(2min) => (16C/min) => 216(5min) => (8C/min) => 280C
CapillaryOV-12497.Webb, Appleford, et al., 199825. m/0.2 mm/0.25 «mu»m; Program: 60C(2min) => 10C/min => 150C => 3C/min => 300C
CapillaryBP-12504.Webb, Appleford, et al., 199825. m/0.2 mm/0.1 «mu»m; Program: 60C(2min) => 10C/min => 150C => 3C/min => 300C
CapillaryBP-12505.Webb, Appleford, et al., 199825. m/0.2 mm/0.1 «mu»m; Program: 60C(2min) => 10C/min => 150C => 3C/min => 300C
CapillaryDB-12501.Grünzweig, Rabinowitch, et al., 1997He; Column length: 30. m; Column diameter: 0.25 mm; Program: 40C (2min) => 10C/min => 150C => 3C/min => 300C
CapillaryCP Sil 5 CB2516.Kappers, Jordi, et al., 199730. m/0.25 mm/0.4 «mu»m, He; Program: 200C => 25C/min => 250C => 4C/min => 280C(4min)
CapillaryDB-12505.Rijnders, Yang, et al., 199715. m/0.25 mm/0.25 «mu»m, He; Program: 80C(1min) => 30C/min => 245C => 5C/min => 300C
CapillaryOV-12497.Kobayashi, Spray, et al., 199625. m/0.2 mm/0.25 «mu»m; Program: 50C(2min) => 10C/min => 150C => 3C/min => 300C
CapillaryOV-12497.Kobayashi, Spray, et al., 199625. m/0.2 mm/0.25 «mu»m; Program: 50C(2min) => 10C/min => 150C => 3C/min => 300C
CapillaryOV-12497.Kobayashi, Spray, et al., 199625. m/0.2 mm/0.25 «mu»m; Program: 50C(2min) => 10C/min => 150C => 3C/min => 300C
CapillaryOV-12499.Kobayashi, Spray, et al., 199625. m/0.2 mm/0.25 «mu»m; Program: 50C(2min) => 10C/min => 150C => 3C/min => 300C
CapillaryOV-12505.Talo, Spray, et al., 1995He; Column length: 25. m; Column diameter: 0.2 mm; Program: 60C(2min) => 13C/min => 150C => 3C/min => 280C(10min)
CapillaryOV-12505.Talo, Spray, et al., 1995He; Column length: 25. m; Column diameter: 0.2 mm; Program: 60C(2min) => 13C/min => 150C => 3C/min => 280C(10min)
CapillaryDB-12508.Pearce, Koshioka, et al., 199415. m/0.22 mm/0.25 «mu»m; Program: 60(0.1 min)-200 0C at 20 deg/min; 200-300 0C at 5 deg/min
CapillarySE-522492.Hedden, Hoad, et al., 199325. m/0.22 mm/0.25 «mu»m, He; Program: 50C => 15C/min => 240C => 4C/min => 300C
CapillarySE-522493.Hedden, Hoad, et al., 199325. m/0.22 mm/0.25 «mu»m, He; Program: 50C => 15C/min => 240C => 4C/min => 300C
CapillaryOV-12497.Waycott, Smith, et al., 199125. m/0.22 mm/0.25 «mu»m; Program: 60C(2min) => 10C/min => 150C => 3C/min => 310C
CapillaryOV-12492.Heupel R.C., Phinney B.O., et al., 1985He; Program: 50C(1min) => 15C/min => 200C => 4C/min => 260C

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-12490.Oyama, Yamauchi, et al., 1996160. C @ 2. min, 16. K/min; Column length: 15. m; Column diameter: 0.258 mm; Tend: 280. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-52540.Chang, Chen, et al., 2001Column length: 15. m; Column diameter: 0.25 mm
CapillaryDB-52544.Chang, Chen, et al., 2001Column length: 15. m; Column diameter: 0.25 mm; Program: 60 0C (0.5 min) 25 K/min -> 200 0C 20 K/min -> 300 0C
CapillaryHP-12531.Fos, Nuez, et al., 200025. m/0.20 mm/0.33 «mu»m, Helium; Program: 60 0C (1 min) 20 0C/min -> 240 0C 4 0C/min -> 300 0C
CapillaryHP-12532.Fos, Nuez, et al., 200025. m/0.20 mm/0.33 «mu»m, Helium; Program: 60 0C (1 min) 20 0C/min -> 240 0C 4 0C/min -> 300 0C
CapillaryDB-12498.Motosugi, Nishijima, et al., 199615. m/0.25 mm/0.25 «mu»m; Program: not specified
CapillaryPolydimethyl siloxane2501.Tanno, Nakayama, et al., 1995Program: not specified
CapillaryPolydimethyl siloxane2500.Tanno, Nakayama, et al., 1995Program: not specified
CapillaryPolydimethyl siloxane2500.Tanno, Nakayama, et al., 1995Program: not specified
CapillaryPolydimethyl siloxane2500.Tanno, Nakayama, et al., 1995Program: not specified
CapillaryDB-12488.Nishijima, Murakami, et al., 199315; Column diameter: 0.257 mm; Phase thickness: 0.25 «mu»m; Program: not specified
CapillaryUltra 22466.Talon, Zacarias, et al., 199222. m/0.32 mm/0.52 «mu»m, Helium; Program: not specified
CapillaryHP-12504.Beall, Morgan, et al., 199112. m/0.2 mm/0.33 «mu»m, He; Program: 60C(1min) => 15C/min => 200C => 5C/min => 270C
CapillaryHP-12508.Matheussen, Morgan, et al., 199112. m/0.2 mm/0.33 «mu»m, He; Program: 60C(1min) => 15C/min => 200C => 5C/min => 270C
CapillaryUltra-22466.Talon, Zeevaart, et al., 199125. m/0.32 mm/0.52 «mu»m; Program: 50C => 40C/min => 220C => 8C/min => 280C

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Morvan-Bertrand, Ernstsen, et al., 2001
Morvan-Bertrand, A.; Ernstsen, A.; Lindgård, B.; Koshioka, M.; le Saos, J.; Boucaud, J.; Prud'homme, M.-P.; Junttila, O., Endogenous gibberellins in Lolium perenne and influence of defoliation on their contents in elongating leaf bases and in leaf sheaths, Physiol. Plant., 2001, 111, 2, 225-231, https://doi.org/10.1034/j.1399-3054.2001.1110214.x . [all data]

Koshioka, Miyamoto, et al., 1998
Koshioka, M.; Miyamoto, K.; Horio, T.; Namura, S.; Hisamatsu, T.; Kubota, S.; Ernstsen, A.; Junttila, O.; Mander, L.N., Identification of endogenous gibberellins in stems and leaves in vegetative growth stage of Gentiana triflora, J. Plant Physiol., 1998, 153, 1-2, 230-232, https://doi.org/10.1016/S0176-1617(98)80071-0 . [all data]

Tanno, Yokota, et al., 1992
Tanno, N.; Yokota, T.; Abe, M.; Okagami, N., Identification of endogenous gibberellins in dormant bulbils of Chinese yam, Dioscorea opposita, Plant Physiol., 1992, 100, 4, 1823-1826, https://doi.org/10.1104/pp.100.4.1823 . [all data]

Talon, Koornneef, et al., 1990
Talon, M.; Koornneef, M.; Zeevaart, J.A.D., Endogenous gibberellins in Arabidopsis thaliana and possible steps blocked in the biosynthetic pathways of the semidwarf ga4 and ga5 mutants, Proc. Nat. Acad. Sci. U.S.A., 1990, 87, 20, 7983-7987, https://doi.org/10.1073/pnas.87.20.7983 . [all data]

Talon and Zeevaart, 1990
Talon, M.; Zeevaart, J.A.D., Gibberellins and stem growth as related to photoperiod in Silene armeria L., Plant Physiol., 1990, 92, 4, 1094-1100, https://doi.org/10.1104/pp.92.4.1094 . [all data]

Kim, Lee, et al., 2003
Kim, S.-K.; Lee, S.-C.; Shin, D.-H.; Jang, S.-W.; Nam, J.-W.; Park, T.-S.; Lee, I.-J., Quantification of endogenous gibberellins in leaves and tubers of Chinese yam, Dioscorea opposita Thunb. cv. Tsukune during tuber enlargement, Plant Growth Regul., 2003, 39, 2, 125-130, https://doi.org/10.1023/A:1022569506883 . [all data]

Kobayashi, MacMillan, et al., 2000
Kobayashi, M.; MacMillan, J.; Phinney, B.; Gaskin, P.; Spray, C.R.; Hedden, P., Gibberellin biosynthesis: metabolic evidence for three steps in the early 13-hydroxylation pathway of rice, Phytochemistry, 2000, 55, 4, 317-321, https://doi.org/10.1016/S0031-9422(00)00265-X . [all data]

Hisamatsu, Koshioka, et al., 1998
Hisamatsu, T.; Koshioka, M.; Kubota, S.; Nishijima, T.; Yamane, H.; King, R.W.; Mander, L.N., Isolation and identification of GA112 (12«beta»-hydroxy-GA12) in Matthiola incana, Phytochemistry, 1998, 47, 1, 3-6, https://doi.org/10.1016/S0031-9422(97)00543-8 . [all data]

Webb, Appleford, et al., 1998
Webb, S.E.; Appleford, N.E.J.; Gaskin, P.; Lenton, J.R., Gibberellins in internodes and ears of wheat containing different dwarfing alleles, Phytochemistry, 1998, 47, 5, 671-677, https://doi.org/10.1016/S0031-9422(97)00684-5 . [all data]

Grünzweig, Rabinowitch, et al., 1997
Grünzweig, J.M.; Rabinowitch, H.D.; Katan, J.; Wodner, M.; Ben-Tal, Y., Endogenous gibberellins in foliage of tomato (Lycopersicon esculentum), Phytochemistry, 1997, 46, 5, 811-815, https://doi.org/10.1016/S0031-9422(97)00383-X . [all data]

Kappers, Jordi, et al., 1997
Kappers, I.F.; Jordi, W.; Maas, F.M.; van der Plas, L.H.W., Gibberellins in leaves of Alstroemeria hybrida: identification and quantification in relation to leaf age, J. Plant Growth Regul., 1997, 16, 4, 219-225, https://doi.org/10.1007/PL00007000 . [all data]

Rijnders, Yang, et al., 1997
Rijnders, J.G.H.M.; Yang, Y.-Y.; Kamiya, Y.; Takahashi, N.; Barendse, G.W.M.; Blom, C.W.P.M.; Voesenek, L.A.C.J., Ethylene enhances gibberellin levels and petiole sensitivity in flooding-tolerant Rumex palustris but not in flooding-intolerant R. acetosa, Planta, 1997, 203, 1, 20-25, https://doi.org/10.1007/s00050160 . [all data]

Kobayashi, Spray, et al., 1996
Kobayashi, M.; Spray, C.R.; Phinney, B.O.; Gaskin, P.; MacMillan, J., Gibberellin metabolism in maize. The stepwise conversion of gibberellin A12-aldehyde to gibberellin A20, Plant Physiol., 1996, 110, 413-418. [all data]

Talo, Spray, et al., 1995
Talo, A.; Spray, C.R.; Somers, D.A.; Donovan, C.M.; Gaskin, P.; Macmillian, J.; Phinney, B.O., Endogenous gibberellins from callus cultures of maize, Phytochemistry, 1995, 40, 1, 11-15, https://doi.org/10.1016/0031-9422(95)00000-W . [all data]

Pearce, Koshioka, et al., 1994
Pearce, D.W.; Koshioka, M.; Pharis, R.P., Chromatography of gibberellins, J. Chromatogr. A, 1994, 658, 1, 91-122, https://doi.org/10.1016/0021-9673(94)85210-3 . [all data]

Hedden, Hoad, et al., 1993
Hedden, P.; Hoad, G.V.; Gaskin, P.; Lewis, M.J.; Green, J.R.; Furber, M.; Mander, L.N., Kaurenoids and gibberellins, including the newly characterized gibberellin A88, in developing apple seeds, Phytochemistry, 1993, 32, 2, 231-237, https://doi.org/10.1016/S0031-9422(00)94973-2 . [all data]

Waycott, Smith, et al., 1991
Waycott, W.; Smith, V.A.; Gaskin, P.; MacMillan, J.; Taiz, L., The endogenous gibberellins of dwarf mutants of lettuce, Plant Physiol., 1991, 95, 4, 1169-1173, https://doi.org/10.1104/pp.95.4.1169 . [all data]

Heupel R.C., Phinney B.O., et al., 1985
Heupel R.C.; Phinney B.O.; Spray C.R.; Gaskin P.; MacMillan J.; Hedden P.; Graebe J.E., Native gibberellins and the metabolism of [14C] gibberellin A53 and of [17-C-13,17-3H)] gibberellin A-20 in tassels of Zea-mays, Phytochemistry, 1985, 24, 1, 47-53, https://doi.org/10.1016/S0031-9422(00)80805-5 . [all data]

Oyama, Yamauchi, et al., 1996
Oyama, N.; Yamauchi, T.; Yamane, H.; Murofushi, N.; Agatsuma, M.; Pour, M.; Mander, L.N., Identification of gibberellins and 9,15-cyclogibberellins in developing apple seeds, Biosci. Biotechnol. Biochem., 1996, 60, 2, 305-308, https://doi.org/10.1271/bbb.60.305 . [all data]

Chang, Chen, et al., 2001
Chang, S.-T.; Chen, W.-S.; Koshioka, M.; Mander, L.N.; Huang, K.-L.; Du, B.-S., Gibberellins in relation to flowering in Polianthes tuberosa, Physiol. Plant., 2001, 112, 3, 429-432, https://doi.org/10.1034/j.1399-3054.2001.1120317.x . [all data]

Fos, Nuez, et al., 2000
Fos, M.; Nuez, F.; Garcia-Martinez, J.L., The gene pat-2, which induces natural partenocarpy, alters the gibberellin content in unpollinated tomato ovaries, Plant Physiol., 2000, 122, 2, 471-479, https://doi.org/10.1104/pp.122.2.471 . [all data]

Motosugi, Nishijima, et al., 1996
Motosugi, H.; Nishijima, T.; Hiehata, N.; Koshioka, M.; Sugiura, A., Endogenous gibberellins in the xylem exudate from apple trees, Biosci. Biotechnol. Biochem., 1996, 60, 9, 1500-1502, https://doi.org/10.1271/bbb.60.1500 . [all data]

Tanno, Nakayama, et al., 1995
Tanno, N.; Nakayama, M.; Kurosawa, H.; Wakatsuki, M.; Tanno, M.; Abe, M.; Okagami, N.; Yokota, T., Endogenous gibberellins from three East Asian Stenophora species of the genus Dioscorea (Yams), Z. Naturforsch., 1995, 50c, 193-198. [all data]

Nishijima, Murakami, et al., 1993
Nishijima, T.; Murakami, F.; Koshioka, M.; Yamazaki, H., Endogenous gibberellins in Aralia cordata, Japan Society for Biosci. Biotechnol. Agrochem., 1993, 57, 1, 1953-1954, https://doi.org/10.1271/bbb.57.1953 . [all data]

Talon, Zacarias, et al., 1992
Talon, M.; Zacarias, L.; PRimo-Millo, E., Gibberellins and Partenocarpic ability in developing ovaries of seedless mandarins, Plant Physiol., 1992, 99, 4, 1575-1581, https://doi.org/10.1104/pp.99.4.1575 . [all data]

Beall, Morgan, et al., 1991
Beall, F.D.; Morgan, P.W.; Mander, L.N.; Miller, F.R.; Babb, K.H., Genetic regulation of development in Sorghum bicolor. V. The ma3R allele results in gibberellin enrichment, Plant Physiol., 1991, 95, 1, 116-125, https://doi.org/10.1104/pp.95.1.116 . [all data]

Matheussen, Morgan, et al., 1991
Matheussen, A.-M.; Morgan, P.W.; Frederiksen, R.A., Implication of gibberellins in head smut (Sporisorium reilianum) of Sorghum bicolor, Plant Physiol., 1991, 96, 2, 537-544, https://doi.org/10.1104/pp.96.2.537 . [all data]

Talon, Zeevaart, et al., 1991
Talon, M.; Zeevaart, J.A.D.; Gage, D.A., Identification of gibberellins in spinach and effects of light and darkness on their levels, Plant Physiol., 1991, 97, 4, 1521-1526, https://doi.org/10.1104/pp.97.4.1521 . [all data]


Notes

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