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GA4 MeTMS


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillarySE-302522.Odén, Wang, et al., 199525. m/0.25 mm/0.25 «mu»m; Program: 80C(1min) => (20C/min) => 200C => (4C/min) => 250C
CapillaryDB-12514.Tanno, Yokota, et al., 1992Column length: 15. m; Column diameter: 0.258 mm; Program: 130C(2m) => 32C/min => 220(4min) => 8C/min270C(2min)
PackedNonpolar2528.Poling, 1991Program: not specified
PackedNonpolar2528.Poling, 1991Program: not specified

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryPE-1HT2498.Frisse, Pimenta, et al., 200330. m/0.32 mm/0.1 «mu»m, He; Program: 60C => 45C/min => 220C => 4C/min => 300C
CapillaryHP-12506.Kim, Lee, et al., 200330. m/0.25 mm/0.25 «mu»m, He; Program: 60C (1min) => 15C/min => 200C => 5C/min => 285C
CapillaryHP-12506.Kim, Lee, et al., 200330. m/0.25 mm/0.25 «mu»m, He; Program: 60C (1min) => 15C/min => 200C => 5C/min => 285C
CapillaryDB-12500.Hisamatsu, Koshioka, et al., 199815. m/0.25 mm/0.33 «mu»m; Program: 120(2min) => (16C/min) => 216(5min) => (8C/min) => 280C
CapillaryOV-12503.Webb, Appleford, et al., 199825. m/0.2 mm/0.25 «mu»m; Program: 60C(2min) => 10C/min => 150C => 3C/min => 300C
CapillaryBP-12515.Webb, Appleford, et al., 199825. m/0.2 mm/0.1 «mu»m; Program: 60C(2min) => 10C/min => 150C => 3C/min => 300C
CapillaryDB-12507.Grünzweig, Rabinowitch, et al., 1997He; Column length: 30. m; Column diameter: 0.25 mm; Program: 40C (2min) => 10C/min => 150C => 3C/min => 300C
CapillaryDB-12509.Grünzweig, Rabinowitch, et al., 1997He; Column length: 30. m; Column diameter: 0.25 mm; Program: 40C (2min) => 10C/min => 150C => 3C/min => 300C
CapillaryCP Sil 5 CB2522.Kappers, Jordi, et al., 199730. m/0.25 mm/0.4 «mu»m, He; Program: 200C => 25C/min => 250C => 4C/min => 280C(4min)
CapillaryCP Sil 5 CB2522.Kappers, Jordi, et al., 199730. m/0.25 mm/0.4 «mu»m, He; Program: 200C => 25C/min => 250C => 4C/min => 280C(4min)
CapillaryDB-12510.Rijnders, Yang, et al., 199715. m/0.25 mm/0.25 «mu»m, He; Program: 80C(1min) => 30C/min => 245C => 5C/min => 300C
CapillaryBP-12493.MacMillan and Gaskin, 199625. m/0.2 mm/0.1 «mu»m, He; Program: 60C(2min) => 10C/min => 150C => 3C/min => 300C(10min)
CapillaryDB-12501.Ridoutt, Pharis, et al., 199515. m/0.25 mm/0.25 «mu»m, He; Program: 60C(1min) => 20C/min => 200C => 4C/min => 260C
CapillaryDB-12502.Ridoutt, Pharis, et al., 199515. m/0.25 mm/0.25 «mu»m, He; Program: 60C(1min) => 20C/min => 200C => 4C/min => 260C
CapillaryDB-12519.Pearce, Koshioka, et al., 199415. m/0.22 mm/0.25 «mu»m; Program: 60(0.1 min)-200 0C at 20 deg/min; 200-300 0C at 5 deg/min
CapillarySE-522496.Hedden, Hoad, et al., 199325. m/0.22 mm/0.25 «mu»m, He; Program: 50C => 15C/min => 240C => 4C/min => 300C
CapillarySE-522497.Hedden, Hoad, et al., 199325. m/0.22 mm/0.25 «mu»m, He; Program: 50C => 15C/min => 240C => 4C/min => 300C
CapillaryOV-12510.Kobayashi, Gaskin, et al., 199325. m/0.2 mm/0.25 «mu»m; Program: 50C(2min) => 10C/min => 150C => 3C/min => 300C
CapillaryOV-12497.Gaskin, Gilmour, et al., 1984He; Column length: 25. m; Column diameter: 0.2 mm; Program: 60C(2min) => 13C/min => 150C => 3C/min => 280C(10min)

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-12501.Oyama, Yamauchi, et al., 1996160. C @ 2. min, 16. K/min; Column length: 15. m; Column diameter: 0.258 mm; Tend: 280. C
CapillaryDB-12502.Oyama, Yamauchi, et al., 1996160. C @ 2. min, 16. K/min; Column length: 15. m; Column diameter: 0.258 mm; Tend: 280. C
CapillaryDB-12500.Oyama, Yamauchi, et al., 1996, 2160. C @ 2. min, 16. K/min; Column length: 15. m; Column diameter: 0.258 mm; Tend: 280. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryOV-12528.Suzuki, Ishiyama, et al., 2005Program: not specified
CapillaryDB-12484.Chung, Kuo, et al., 200315. m/0.25 mm/0.25 «mu»m; Program: 60 0C (0.1 min) 20 0C -> 200 0C 5 0C/min -> 300 0C
CapillaryDB-12518.Yamazaki, Nishijima, et al., 200230. m/0.25 mm/0.25 «mu»m, He; Program: 60C92min) => 30C/min => 210C => 2C/min => 280C(5min)
CapillarySE-302520.Wang, Little, et al., 199625. m/0.25 mm/0.25 «mu»m; Program: 60 (2min) => 20C/min => 200C => 4C/min => 260C
CapillarySE-302521.Wang, Little, et al., 199625. m/0.25 mm/0.25 «mu»m; Program: 60 (2min) => 20C/min => 200C => 4C/min => 260C
CapillarySE-302521.Wang, Little, et al., 199625. m/0.25 mm/0.25 «mu»m; Program: 60 (2min) => 20C/min => 200C => 4C/min => 260C
CapillarySE-302521.Wang, Little, et al., 199625. m/0.25 mm/0.25 «mu»m; Program: 60 (2min) => 20C/min => 200C => 4C/min => 260C
CapillaryDB-12533.Kawaide, Sassa, et al., 1995He; Column length: 15. m; Column diameter: 0.25 mm; Program: 80C(1min) => 30C/min => 245C => 5C/min => 300C
CapillaryDB-12499.Koshioka, Nishijama, et al., 199515. m/0.25 mm/0.25 «mu»m; Program: not specified
CapillaryPolydimethyl siloxane2504.Tanno, Nakayama, et al., 1995Program: not specified
CapillaryPolydimethyl siloxane2509.Tanno, Nakayama, et al., 1995Program: not specified
CapillaryBP-12546.Lange, Hedden, et al., 199325. m/0.25 mm/0.33 «mu»m, He; Program: 60C(1min) => 20C/min => 240C => 4C/min => 300C
CapillaryDB-12490.Nishijima, Murakami, et al., 199315; Column diameter: 0.257 mm; Phase thickness: 0.25 «mu»m; Program: not specified
CapillaryUltra 22489.Talon, Zacarias, et al., 199222. m/0.32 mm/0.52 «mu»m, Helium; Program: not specified
CapillaryHP-12508.Matheussen, Morgan, et al., 199112. m/0.2 mm/0.33 «mu»m, He; Program: 60C(1min) => 15C/min => 200C => 5C/min => 270C
CapillaryOV-12493.Yamane, Fujioka, et al., 198825. m/0.20 mm/0.25 «mu»m; Program: not specified
CapillaryOV-12493.Yamane, Fujioka, et al., 198825. m/0.20 mm/0.25 «mu»m; Program: not specified
CapillaryOV-12493.Yamane, Fujioka, et al., 198825. m/0.20 mm/0.25 «mu»m; Program: not specified
CapillaryOV-12493.Yamane, Fujioka, et al., 198825. m/0.20 mm/0.25 «mu»m; Program: not specified

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Odén, Wang, et al., 1995
Odén, P.C.; Wang, Q.; Högberg, K.-A.; Werner, M., Transport and metabolism of gibberellins in relation to flower bud differentiation in Norway spruce (Picea abies), Tree Physiol., 1995, 15, 7-8, 451-456, https://doi.org/10.1093/treephys/15.7-8.451 . [all data]

Tanno, Yokota, et al., 1992
Tanno, N.; Yokota, T.; Abe, M.; Okagami, N., Identification of endogenous gibberellins in dormant bulbils of Chinese yam, Dioscorea opposita, Plant Physiol., 1992, 100, 4, 1823-1826, https://doi.org/10.1104/pp.100.4.1823 . [all data]

Poling, 1991
Poling, S.M., Identification of endogenous gibberellins in immature navel orange fruit, J. Agric. Food Chem., 1991, 39, 4, 677-680, https://doi.org/10.1021/jf00004a010 . [all data]

Frisse, Pimenta, et al., 2003
Frisse, A.; Pimenta, M.J.; Lange, T., Expression studies of gibberellin oxidases in developing pumpkin seeds, Plant Physiol., 2003, 131, 3, 1220-1227, retrieved from http://www.plantphysiol.org, https://doi.org/10.1104/pp.015206 . [all data]

Kim, Lee, et al., 2003
Kim, S.-K.; Lee, S.-C.; Shin, D.-H.; Jang, S.-W.; Nam, J.-W.; Park, T.-S.; Lee, I.-J., Quantification of endogenous gibberellins in leaves and tubers of Chinese yam, Dioscorea opposita Thunb. cv. Tsukune during tuber enlargement, Plant Growth Regul., 2003, 39, 2, 125-130, https://doi.org/10.1023/A:1022569506883 . [all data]

Hisamatsu, Koshioka, et al., 1998
Hisamatsu, T.; Koshioka, M.; Kubota, S.; Nishijima, T.; Yamane, H.; King, R.W.; Mander, L.N., Isolation and identification of GA112 (12«beta»-hydroxy-GA12) in Matthiola incana, Phytochemistry, 1998, 47, 1, 3-6, https://doi.org/10.1016/S0031-9422(97)00543-8 . [all data]

Webb, Appleford, et al., 1998
Webb, S.E.; Appleford, N.E.J.; Gaskin, P.; Lenton, J.R., Gibberellins in internodes and ears of wheat containing different dwarfing alleles, Phytochemistry, 1998, 47, 5, 671-677, https://doi.org/10.1016/S0031-9422(97)00684-5 . [all data]

Grünzweig, Rabinowitch, et al., 1997
Grünzweig, J.M.; Rabinowitch, H.D.; Katan, J.; Wodner, M.; Ben-Tal, Y., Endogenous gibberellins in foliage of tomato (Lycopersicon esculentum), Phytochemistry, 1997, 46, 5, 811-815, https://doi.org/10.1016/S0031-9422(97)00383-X . [all data]

Kappers, Jordi, et al., 1997
Kappers, I.F.; Jordi, W.; Maas, F.M.; van der Plas, L.H.W., Gibberellins in leaves of Alstroemeria hybrida: identification and quantification in relation to leaf age, J. Plant Growth Regul., 1997, 16, 4, 219-225, https://doi.org/10.1007/PL00007000 . [all data]

Rijnders, Yang, et al., 1997
Rijnders, J.G.H.M.; Yang, Y.-Y.; Kamiya, Y.; Takahashi, N.; Barendse, G.W.M.; Blom, C.W.P.M.; Voesenek, L.A.C.J., Ethylene enhances gibberellin levels and petiole sensitivity in flooding-tolerant Rumex palustris but not in flooding-intolerant R. acetosa, Planta, 1997, 203, 1, 20-25, https://doi.org/10.1007/s00050160 . [all data]

MacMillan and Gaskin, 1996
MacMillan, J.; Gaskin, P., Gibberellins in endosperm and embryos of Marah macrocarpus, Phytochemistry, 1996, 42, 5, 1263-1266, https://doi.org/10.1016/0031-9422(96)00179-3 . [all data]

Ridoutt, Pharis, et al., 1995
Ridoutt, B.G.; Pharis, R.P.; Sands, R., Identification and quantification of cambial region hormones of Eucalyptus globulus, Plant Cell Physiol., 1995, 36, 6, 1143-1147. [all data]

Pearce, Koshioka, et al., 1994
Pearce, D.W.; Koshioka, M.; Pharis, R.P., Chromatography of gibberellins, J. Chromatogr. A, 1994, 658, 1, 91-122, https://doi.org/10.1016/0021-9673(94)85210-3 . [all data]

Hedden, Hoad, et al., 1993
Hedden, P.; Hoad, G.V.; Gaskin, P.; Lewis, M.J.; Green, J.R.; Furber, M.; Mander, L.N., Kaurenoids and gibberellins, including the newly characterized gibberellin A88, in developing apple seeds, Phytochemistry, 1993, 32, 2, 231-237, https://doi.org/10.1016/S0031-9422(00)94973-2 . [all data]

Kobayashi, Gaskin, et al., 1993
Kobayashi, M.; Gaskin, P.; Spray, C.R.; Suzuki, Y.; Phinney, B.O.; MacMillan, J., Metabolism and biological activity of Gibberellin A4 in vegetative shoots of Zea mays, Oryza sativa, and Arabidopsis thaliana, Plant Physiol., 1993, 102, 379-386. [all data]

Gaskin, Gilmour, et al., 1984
Gaskin, P.; Gilmour, S.J.; Lenton, J.R.; MacMillan, J.; Sponsel, V.M., Endogenous gibberellins and kauranoids identified from developing and germinating barley grain, J. Plant Growth Regul., 1984, 2, 1-4, 229-242, https://doi.org/10.1007/BF02042252 . [all data]

Oyama, Yamauchi, et al., 1996
Oyama, N.; Yamauchi, T.; Yamane, H.; Yamaguchi, I.; Schraudolf, H.; Mander, L.N.; Murofushi, N., Gibberellins and antheridiogens in prothallia and sporophytes of Anemia phyllitidis, Biosci. Biotechnol. Biochem., 1996, 60, 2, 301-304, https://doi.org/10.1271/bbb.60.301 . [all data]

Oyama, Yamauchi, et al., 1996, 2
Oyama, N.; Yamauchi, T.; Yamane, H.; Murofushi, N.; Agatsuma, M.; Pour, M.; Mander, L.N., Identification of gibberellins and 9,15-cyclogibberellins in developing apple seeds, Biosci. Biotechnol. Biochem., 1996, 60, 2, 305-308, https://doi.org/10.1271/bbb.60.305 . [all data]

Suzuki, Ishiyama, et al., 2005
Suzuki, H.; Ishiyama, K.; Kobayashi, M.; Ogawa, T., Specific expression of the gibberellin 3«beta» -hydroxylase gene, HvGA3ox2, in the epithelium is important for Amy1 expression in germinating barley seeds, Plant Biotechnology, 2005, 22, 3, 195-200, https://doi.org/10.5511/plantbiotechnology.22.195 . [all data]

Chung, Kuo, et al., 2003
Chung, J.-D.; Kuo, S.-R.; Chien, C.-T., Identification and quantification of gibberellin transformation and dosage changes in good and poor flowering clones of Calocedrus formosana grafts, Taiwan J. For. Sci., 2003, 18, 4, 387-400. [all data]

Yamazaki, Nishijima, et al., 2002
Yamazaki, H.; Nishijima, T.; Koshioka, M.; Miura, H., Gibberellins do no act against abscisic acid in the regulation of bulb dormancy of Allium wakegi Araki, Plant Growth Regul., 2002, 36, 3, 223-229, https://doi.org/10.1023/A:1016577529378 . [all data]

Wang, Little, et al., 1996
Wang, Q.; Little, C.H.A.; Moritz, T.; Odén, P.C., Identification of endogenous gibberellins, and metabolism of tritiated and deuterated GA4, GA9, and GA20, in Scots pine (Pinus sylvestris) shoots, Physiol. Plant., 1996, 97, 4, 764-771, https://doi.org/10.1111/j.1399-3054.1996.tb00542.x . [all data]

Kawaide, Sassa, et al., 1995
Kawaide, H.; Sassa, T.; Kamiya, Y., Plant-like biosynthesis of gibberellin A1 in the fungus Phaeosphaeria Sp. L487, Phytochemistry, 1995, 39, 2, 305-310, https://doi.org/10.1016/0031-9422(95)00006-S . [all data]

Koshioka, Nishijama, et al., 1995
Koshioka, M.; Nishijama, T.; Mander, L.N., Gibberellin metabolism in suspension cultured cells of Raphanus Sativus, Phytochemistry, 1995, 38, 2, 359-363, https://doi.org/10.1016/0031-9422(94)00624-3 . [all data]

Tanno, Nakayama, et al., 1995
Tanno, N.; Nakayama, M.; Kurosawa, H.; Wakatsuki, M.; Tanno, M.; Abe, M.; Okagami, N.; Yokota, T., Endogenous gibberellins from three East Asian Stenophora species of the genus Dioscorea (Yams), Z. Naturforsch., 1995, 50c, 193-198. [all data]

Lange, Hedden, et al., 1993
Lange, T.; Hedden, P.; Graebe, J.E., Gibberellin biosynthesis in cell-free extracts from developing Cucurbita maxima embryos and the identification of new endogenous gibberellins, Planta, 1993, 189, 3, 350-358, https://doi.org/10.1007/BF00194431 . [all data]

Nishijima, Murakami, et al., 1993
Nishijima, T.; Murakami, F.; Koshioka, M.; Yamazaki, H., Endogenous gibberellins in Aralia cordata, Japan Society for Biosci. Biotechnol. Agrochem., 1993, 57, 1, 1953-1954, https://doi.org/10.1271/bbb.57.1953 . [all data]

Talon, Zacarias, et al., 1992
Talon, M.; Zacarias, L.; PRimo-Millo, E., Gibberellins and Partenocarpic ability in developing ovaries of seedless mandarins, Plant Physiol., 1992, 99, 4, 1575-1581, https://doi.org/10.1104/pp.99.4.1575 . [all data]

Matheussen, Morgan, et al., 1991
Matheussen, A.-M.; Morgan, P.W.; Frederiksen, R.A., Implication of gibberellins in head smut (Sporisorium reilianum) of Sorghum bicolor, Plant Physiol., 1991, 96, 2, 537-544, https://doi.org/10.1104/pp.96.2.537 . [all data]

Yamane, Fujioka, et al., 1988
Yamane, H.; Fujioka, S.; Spray, C.R.; Phinney, B.O.; MacMillan, J.; Gaskin, P.; Takahashi, N., Endogenous Gibberellines from Sporophytes of Two Tree Ferns, Cibotium glaucum and Dicksonia antarctica, Plant Phisiol., 1988, 86, 3, 857-862, https://doi.org/10.1104/pp.86.3.857 . [all data]


Notes

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