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GA34 methyl ester TMS ether


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillarySE-302671.Odén, Wang, et al., 199525. m/0.25 mm/0.25 «mu»m; Program: 80C(1min) => (20C/min) => 200C => (4C/min) => 250C
CapillaryUltra-22620.Talon, Koornneef, et al., 199025. m/0.32 mm/0.52 «mu»m; Program: 50C => 40C/min => 220C => 6C/min => 280C
CapillaryBP-12687.Hedden, Croker, et al., 198925. m/0.32 mm/0.33 «mu»m, He; Program: 50C(1min) => 20C/min => 240C => 4C/min => 295C
CapillaryBP-12688.Hedden, Croker, et al., 198925. m/0.32 mm/0.33 «mu»m, He; Program: 50C(1min) => 20C/min => 240C => 4C/min => 295C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryBPX-52669.Frisse, Pimenta, et al., 200330. m/0.25 mm/0.25 «mu»m, He; Program: 60C => 45C/min => 220C => 4C/min => 300C
CapillaryHP-12672.Pearce, Hutt, et al., 2002Column length: 12. m; Column diameter: 0.22 mm; Program: 60C(0.5min) => 20C/min => 200C => 5C/min => 300C
CapillaryHP-12673.Pearce, Hutt, et al., 2002Column length: 12. m; Column diameter: 0.22 mm; Program: 60C(0.5min) => 20C/min => 200C => 5C/min => 300C
CapillaryDB-52654.Pearce, Hutt, et al., 2002Column length: 15. m; Column diameter: 0.25 mm; Program: 60C(0.5min) => 20C/min => 200C => 5C/min => 300C
CapillaryDB-52655.Pearce, Hutt, et al., 2002Column length: 15. m; Column diameter: 0.25 mm; Program: 60C(0.5min) => 20C/min => 200C => 5C/min => 300C
CapillaryDB-12660.Hisamatsu, Koshioka, et al., 199815. m/0.25 mm/0.33 «mu»m; Program: 120(2min) => (16C/min) => 216(5min) => (8C/min) => 280C
CapillaryOV-12665.Webb, Appleford, et al., 199825. m/0.2 mm/0.25 «mu»m; Program: 60C(2min) => 10C/min => 150C => 3C/min => 300C
CapillaryBP-12672.Webb, Appleford, et al., 199825. m/0.2 mm/0.1 «mu»m; Program: 60C(2min) => 10C/min => 150C => 3C/min => 300C
CapillaryDB-12666.Grünzweig, Rabinowitch, et al., 1997He; Column length: 30. m; Column diameter: 0.25 mm; Program: 40C (2min) => 10C/min => 150C => 3C/min => 300C
CapillaryDB-12671.Grünzweig, Rabinowitch, et al., 1997He; Column length: 30. m; Column diameter: 0.25 mm; Program: 40C (2min) => 10C/min => 150C => 3C/min => 300C
CapillaryCP Sil 5 CB2675.Kappers, Jordi, et al., 199730. m/0.25 mm/0.4 «mu»m, He; Program: 200C => 25C/min => 250C => 4C/min => 280C(4min)
CapillaryCP Sil 5 CB2675.Kappers, Jordi, et al., 199730. m/0.25 mm/0.4 «mu»m, He; Program: 200C => 25C/min => 250C => 4C/min => 280C(4min)
CapillaryDB-12669.Pearce, Koshioka, et al., 199415. m/0.22 mm/0.25 «mu»m; Program: 60(0.1 min)-200 0C at 20 deg/min; 200-300 0C at 5 deg/min
CapillarySE-522660.Hedden, Hoad, et al., 199325. m/0.22 mm/0.25 «mu»m, He; Program: 50C => 15C/min => 240C => 4C/min => 300C
CapillarySE-522660.Hedden, Hoad, et al., 199325. m/0.22 mm/0.25 «mu»m, He; Program: 50C => 15C/min => 240C => 4C/min => 300C
CapillaryOV-12669.Kobayashi, Gaskin, et al., 199325. m/0.2 mm/0.25 «mu»m; Program: 50C(2min) => 10C/min => 150C => 3C/min => 300C
CapillaryOV-12657.Gaskin, Gilmour, et al., 1984He; Column length: 25. m; Column diameter: 0.2 mm; Program: 60C(2min) => 13C/min => 150C => 3C/min => 280C(10min)

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-52719.Park, Nakajima, et al., 200515. m/0.25 mm/0.25 «mu»m, Helium, 60. C @ 2. min, 15. K/min; Tend: 300. C
CapillaryDB-12653.Oyama, Yamauchi, et al., 1996160. C @ 2. min, 16. K/min; Column length: 15. m; Column diameter: 0.258 mm; Tend: 280. C

Normal alkane RI, non-polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryBPX-52672.Lange, Kappler, et al., 200530. m/0.25 mm/0.25 «mu»m, He; Program: 60 0C (1 min) 45 0C/min -> 220 0C 4 0C/min -> 300 0C
CapillaryOV-12678.Sakamoto, Kobayashi, et al., 2001Program: not specified
CapillaryHP-12690.Fos, Nuez, et al., 200025. m/0.20 mm/0.33 «mu»m, Helium; Program: 60 0C (1 min) 20 0C/min -> 240 0C 4 0C/min -> 300 0C
CapillaryHP-12692.Fos, Nuez, et al., 200025. m/0.20 mm/0.33 «mu»m, Helium; Program: 60 0C (1 min) 20 0C/min -> 240 0C 4 0C/min -> 300 0C
CapillaryUltra-22621.Talon, Zeevaart, et al., 199125. m/0.32 mm/0.52 «mu»m; Program: 50C => 40C/min => 220C => 8C/min => 280C

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Odén, Wang, et al., 1995
Odén, P.C.; Wang, Q.; Högberg, K.-A.; Werner, M., Transport and metabolism of gibberellins in relation to flower bud differentiation in Norway spruce (Picea abies), Tree Physiol., 1995, 15, 7-8, 451-456, https://doi.org/10.1093/treephys/15.7-8.451 . [all data]

Talon, Koornneef, et al., 1990
Talon, M.; Koornneef, M.; Zeevaart, J.A.D., Endogenous gibberellins in Arabidopsis thaliana and possible steps blocked in the biosynthetic pathways of the semidwarf ga4 and ga5 mutants, Proc. Nat. Acad. Sci. U.S.A., 1990, 87, 20, 7983-7987, https://doi.org/10.1073/pnas.87.20.7983 . [all data]

Hedden, Croker, et al., 1989
Hedden, P.; Croker, S.J.; Rademacher, W.; Jung, J., Effects of the triazole plant growth retardant BAS 111..W on gibberellin levels in oilseed rape, Brassica napus, Physiol. Plant., 1989, 75, 4, 445-451, https://doi.org/10.1111/j.1399-3054.1989.tb05607.x . [all data]

Frisse, Pimenta, et al., 2003
Frisse, A.; Pimenta, M.J.; Lange, T., Expression studies of gibberellin oxidases in developing pumpkin seeds, Plant Physiol., 2003, 131, 3, 1220-1227, retrieved from http://www.plantphysiol.org, https://doi.org/10.1104/pp.015206 . [all data]

Pearce, Hutt, et al., 2002
Pearce, D.W.; Hutt, O.E.; Rood, S.B.; Mander, L.N., Gibberellins in shoots and developing capsules of Populus species, Phytochemistry, 2002, 59, 6, 679-687, https://doi.org/10.1016/S0031-9422(02)00009-2 . [all data]

Hisamatsu, Koshioka, et al., 1998
Hisamatsu, T.; Koshioka, M.; Kubota, S.; Nishijima, T.; Yamane, H.; King, R.W.; Mander, L.N., Isolation and identification of GA112 (12«beta»-hydroxy-GA12) in Matthiola incana, Phytochemistry, 1998, 47, 1, 3-6, https://doi.org/10.1016/S0031-9422(97)00543-8 . [all data]

Webb, Appleford, et al., 1998
Webb, S.E.; Appleford, N.E.J.; Gaskin, P.; Lenton, J.R., Gibberellins in internodes and ears of wheat containing different dwarfing alleles, Phytochemistry, 1998, 47, 5, 671-677, https://doi.org/10.1016/S0031-9422(97)00684-5 . [all data]

Grünzweig, Rabinowitch, et al., 1997
Grünzweig, J.M.; Rabinowitch, H.D.; Katan, J.; Wodner, M.; Ben-Tal, Y., Endogenous gibberellins in foliage of tomato (Lycopersicon esculentum), Phytochemistry, 1997, 46, 5, 811-815, https://doi.org/10.1016/S0031-9422(97)00383-X . [all data]

Kappers, Jordi, et al., 1997
Kappers, I.F.; Jordi, W.; Maas, F.M.; van der Plas, L.H.W., Gibberellins in leaves of Alstroemeria hybrida: identification and quantification in relation to leaf age, J. Plant Growth Regul., 1997, 16, 4, 219-225, https://doi.org/10.1007/PL00007000 . [all data]

Pearce, Koshioka, et al., 1994
Pearce, D.W.; Koshioka, M.; Pharis, R.P., Chromatography of gibberellins, J. Chromatogr. A, 1994, 658, 1, 91-122, https://doi.org/10.1016/0021-9673(94)85210-3 . [all data]

Hedden, Hoad, et al., 1993
Hedden, P.; Hoad, G.V.; Gaskin, P.; Lewis, M.J.; Green, J.R.; Furber, M.; Mander, L.N., Kaurenoids and gibberellins, including the newly characterized gibberellin A88, in developing apple seeds, Phytochemistry, 1993, 32, 2, 231-237, https://doi.org/10.1016/S0031-9422(00)94973-2 . [all data]

Kobayashi, Gaskin, et al., 1993
Kobayashi, M.; Gaskin, P.; Spray, C.R.; Suzuki, Y.; Phinney, B.O.; MacMillan, J., Metabolism and biological activity of Gibberellin A4 in vegetative shoots of Zea mays, Oryza sativa, and Arabidopsis thaliana, Plant Physiol., 1993, 102, 379-386. [all data]

Gaskin, Gilmour, et al., 1984
Gaskin, P.; Gilmour, S.J.; Lenton, J.R.; MacMillan, J.; Sponsel, V.M., Endogenous gibberellins and kauranoids identified from developing and germinating barley grain, J. Plant Growth Regul., 1984, 2, 1-4, 229-242, https://doi.org/10.1007/BF02042252 . [all data]

Park, Nakajima, et al., 2005
Park, S.-H.; Nakajima, M.; Sakane, M.; Xu, Z.-J.; Tomioka, K.; Yamaguchi, I., Gibberellin 2-oxidases from seedings of Adzuki bean (Vigna angularis) show high gibberellin-binding activity in the presence os 2-oxoglutarate and Co2+, Biosci. Biotechnol. Biochem., 2005, 69, 8, 1498-1507, https://doi.org/10.1271/bbb.69.1498 . [all data]

Oyama, Yamauchi, et al., 1996
Oyama, N.; Yamauchi, T.; Yamane, H.; Murofushi, N.; Agatsuma, M.; Pour, M.; Mander, L.N., Identification of gibberellins and 9,15-cyclogibberellins in developing apple seeds, Biosci. Biotechnol. Biochem., 1996, 60, 2, 305-308, https://doi.org/10.1271/bbb.60.305 . [all data]

Lange, Kappler, et al., 2005
Lange, T.; Kappler, J.; Fischer, A.; Frisse, A.; Padeffke, T.; Schmidtke, S.; Lange, M.J.P., Gibberellin biosynthesis in developing pumpkin seedlings, Plant Physiol., 2005, 139, 1, 213-223, https://doi.org/10.1104/pp.105.064162 . [all data]

Sakamoto, Kobayashi, et al., 2001
Sakamoto, T.; Kobayashi, M.; Itoh, H.; Tahiri, A.; Kayano, T.; Tanaka, H.; Iwahori, S.; Matsuoka, M., Expression of a gibberellin 2-oxidase gene around the shoot apex is related to phase transition in rice, Plant Physiology, 2001, 125, 3, 1508-1516, https://doi.org/10.1104/pp.125.3.1508 . [all data]

Fos, Nuez, et al., 2000
Fos, M.; Nuez, F.; Garcia-Martinez, J.L., The gene pat-2, which induces natural partenocarpy, alters the gibberellin content in unpollinated tomato ovaries, Plant Physiol., 2000, 122, 2, 471-479, https://doi.org/10.1104/pp.122.2.471 . [all data]

Talon, Zeevaart, et al., 1991
Talon, M.; Zeevaart, J.A.D.; Gage, D.A., Identification of gibberellins in spinach and effects of light and darkness on their levels, Plant Physiol., 1991, 97, 4, 1521-1526, https://doi.org/10.1104/pp.97.4.1521 . [all data]


Notes

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