GA29, MeTMSi


Kovats' RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5HP-5Cross-Linked MethylsiliconeCross-Linked Methylsilicone
Column length (m)    25.25.
Carrier gas He  HeHe
Substrate      
Column diameter (mm) 0.25  0.20.2
Phase thickness (μm) 0.25  0.110.11
Program 60C(0.1min) => 20C/min => 200C => 5C/min => 300Cnot specifiednot specified60C(2min) => 30C/min => 210C(1min) => 10C/min => 240C60C(2min) => 30C/min => 210C(1min) => 10C/min => 240C
I 2682.2670.2671.2685.2687.
ReferenceEmery, Pearce, et al., 2001Morvan-Bertrand, Ernstsen, et al., 2001Morvan-Bertrand, Ernstsen, et al., 2001Schneider, Jensen, et al., 1992Schneider, Jensen, et al., 1992
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryPackedPackedCapillary
Active phase Cross-Linked MethylsiliconeCross-Linked MethylsiliconeNonpolarNonpolarSE-52/54
Column length (m) 25.25.  25.
Carrier gas HeHe  He
Substrate      
Column diameter (mm) 0.20.2  0.22
Phase thickness (μm) 0.110.11  0.25
Program 60C(2min) => 30C/min => 210C(1min) => 10C/min => 240C60C(2min) => 30C/min => 210C(1min) => 10C/min => 240Cnot specifiednot specified50C(1min) => 15C/min => 240C => 4C/min => 300C
I 2689.2690.2696.2698.2722.
ReferenceSchneider, Jensen, et al., 1992Schneider, Jensen, et al., 1992Poling, 1991Poling, 1991Croker, Hedden, et al., 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-52/54BP-1BP-1BP-1BP-1
Column length (m) 25.25.25.25.25.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.320.320.320.32
Phase thickness (μm) 0.250.330.330.330.33
Program 50C(1min) => 15C/min => 240C => 4C/min => 300C50C(1min) => 20C/min => 240C => 4C/min => 295C50C(1min) => 20C/min => 240C => 4C/min => 295C50C(1min) => 20C/min => 240C => 4C/min => 295C50C(1min) => 20C/min => 240C => 4C/min => 295C
I 2725.2680.2685.2687.2694.
ReferenceCroker, Hedden, et al., 1990Talón, Hedden, et al., 1990Talón, Hedden, et al., 1990Talón, Hedden, et al., 1990Hedden, Croker, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase BP-1
Column length (m) 25.
Carrier gas He
Substrate  
Column diameter (mm) 0.32
Phase thickness (μm) 0.33
Program 50C(1min) => 20C/min => 240C => 4C/min => 295C
I 2700.
ReferenceHedden, Croker, et al., 1989
Comment MSDC-RI

References

Go To: Top, Kovats' RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Emery, Pearce, et al., 2001
Emery, R.J.N.; Pearce, D.W.; Pharis, R.P.; Reid, D.M.; Chinnappa, C.C., Stem elongation and gibberellins in alpine and prairie ecotypes of Stellaria longipes, Plant Growth Regul., 2001, 35, 1, 17-29, https://doi.org/10.1023/A:1013823517189 . [all data]

Morvan-Bertrand, Ernstsen, et al., 2001
Morvan-Bertrand, A.; Ernstsen, A.; Lindgård, B.; Koshioka, M.; le Saos, J.; Boucaud, J.; Prud'homme, M.-P.; Junttila, O., Endogenous gibberellins in Lolium perenne and influence of defoliation on their contents in elongating leaf bases and in leaf sheaths, Physiol. Plant., 2001, 111, 2, 225-231, https://doi.org/10.1034/j.1399-3054.2001.1110214.x . [all data]

Schneider, Jensen, et al., 1992
Schneider, G.; Jensen, E.; Spray, C.R.; Phinney, B.O., Hydrolysis and reconjugation of gibberellin A20 glucosyl ester by seedlings of Zea mays L., Proc. Nat. Acad. Sci. U.S.A., 1992, 89, 17, 8045-8048, https://doi.org/10.1073/pnas.89.17.8045 . [all data]

Poling, 1991
Poling, S.M., Identification of endogenous gibberellins in immature navel orange fruit, J. Agric. Food Chem., 1991, 39, 4, 677-680, https://doi.org/10.1021/jf00004a010 . [all data]

Croker, Hedden, et al., 1990
Croker, S.J.; Hedden, P.; Lenton, J.R.; Stoddart, J.L., Comparison of gibberellins in normal and slender barley seedlings, Plant Physiol., 1990, 94, 1, 194-200, https://doi.org/10.1104/pp.94.1.194 . [all data]

Talón, Hedden, et al., 1990
Talón, M.; Hedden, P.; Primo-Millo, E., Gibberellins in Citrus sinensis: a comparison between seeded and seedless varieties, J. Plant Growth Regul., 1990, 9, 4, 201-206, https://doi.org/10.1007/BF02041963 . [all data]

Hedden, Croker, et al., 1989
Hedden, P.; Croker, S.J.; Rademacher, W.; Jung, J., Effects of the triazole plant growth retardant BAS 111..W on gibberellin levels in oilseed rape, Brassica napus, Physiol. Plant., 1989, 75, 4, 445-451, https://doi.org/10.1111/j.1399-3054.1989.tb05607.x . [all data]


Notes

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