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GA20, Me-TMS


Normal alkane RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BPX-5DB-1DB-1DB-5DB-5
Column length (m) 30.15.30.15.15.
Carrier gas He He  
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.25  
Program 60 0C (1 min) 45 0C/min -> 220 0C 4 0C/min -> 300 0C60 0C (0.1 min) 20 0C -> 200 0C 5 0C/min -> 300 0C60C92min) => 30C/min => 210C => 2C/min => 280C(5min) 60 0C (0.5 min) 25 K/min -> 200 0C 20 K/min -> 300 0C
I 2544.2464.2497.2534.2536.
ReferenceLange, Kappler, et al., 2005Chung, Kuo, et al., 2003Yamazaki, Nishijima, et al., 2002Chang, Chen, et al., 2001Chang, Chen, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1HP-1Methyl SiliconeMethyl SiliconeBP-1
Column length (m) 25.25.  25.
Carrier gas HeliumHelium   
Substrate      
Column diameter (mm) 0.200.20  0.2
Phase thickness (mum) 0.330.33  0.25
Program 60 0C (1 min) 20 0C/min -> 240 0C 4 0C/min -> 300 0C60 0C (1 min) 20 0C/min -> 240 0C 4 0C/min -> 300 0Cnot specifiednot specified60C (1min) => 20C/min => 240C => 4C/min => 300C
I 2520.2523.2529.2529.2482.
ReferenceFos, Nuez, et al., 2000Fos, Nuez, et al., 2000Martínez-García, Santes, et al., 2000Martínez-García, Santes, et al., 2000Pérez, Viani, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1HP-1SE-30SE-30HP-5 MS
Column length (m)   25.25.30.
Carrier gas     Helium
Substrate      
Column diameter (mm)   0.250.250.25
Phase thickness (mum)   0.250.250.25
Program  60 0C 30 K/min -> 230 0C 3 K/min -> 265 0C 30 K/min -> 290 0C60 (2min) => 20C/min => 200C => 4C/min => 260C60 (2min) => 20C/min => 200C => 4C/min => 260C50 0C (2 min) 10 0C/min -> 150 0C 3 0C/min -> 300 0C
I 2497.2497.2500.2500.2543.
ReferenceRoss, MacKenzie-Hose, et al., 1999Ross, MacKenzie-Hose, et al., 1999Wang, Little, et al., 1996Wang, Little, et al., 1996van Huizen, Ozga, et al., 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1DB-1DB-1DB-1
Column length (m) 15.15.15.25. 
Carrier gas He  He15
Substrate      
Column diameter (mm) 0.250.250.250.320.257
Phase thickness (mum)  0.250.250.330.25
Program 80C(1min) => 30C/min => 245C => 5C/min => 300Cnot specifiednot specified50C(1min) => 20C/min => 240C => 4C/min => 295Cnot specified
I 2509.2476.2477.2509.2471.
ReferenceKawaide, Sassa, et al., 1995Koshioka, Nishijama, et al., 1995Koshioka, Nishijama, et al., 1995Lange, Hedden, et al., 1993Nishijima, Murakami, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Ultra 2HP-1Methyl SiliconeMethyl SiliconeMethyl Silicone
Column length (m) 22.12.   
Carrier gas HeliumHe   
Substrate      
Column diameter (mm) 0.320.2   
Phase thickness (mum) 0.520.33   
Program not specified60C(1min) => 15C/min => 200C => 5C/min => 270Cnot specifiednot specifiednot specified
I 2468.2493.2509.2509.2511.
ReferenceTalon, Zacarias, et al., 1992Beall, Morgan, et al., 1991Garcia-Martinez, Santes, et al., 1991Garcia-Martinez, Santes, et al., 1991Garcia-Martinez, Santes, et al., 1991
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1Ultra-2DB-1DB-1OV-1
Column length (m) 12.25.15.15.25.
Carrier gas He HeliumHelium 
Substrate      
Column diameter (mm) 0.20.320.2580.2580.20
Phase thickness (mum) 0.330.52  0.25
Program 60C(1min) => 15C/min => 200C => 5C/min => 270C50C => 40C/min => 220C => 8C/min => 280Cnot specifiednot specifiednot specified
I 2485.2468.2482.2482.2477.
ReferenceMatheussen, Morgan, et al., 1991Talon, Zeevaart, et al., 1991Nakayama, Yamane, et al., 1990Nakayama, Yamane, et al., 1990Yamane, Fujioka, et al., 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase OV-1
Column length (m) 25.
Carrier gas  
Substrate  
Column diameter (mm) 0.20
Phase thickness (mum) 0.25
Program not specified
I 2477.
ReferenceYamane, Fujioka, et al., 1988
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Lange, Kappler, et al., 2005
Lange, T.; Kappler, J.; Fischer, A.; Frisse, A.; Padeffke, T.; Schmidtke, S.; Lange, M.J.P., Gibberellin biosynthesis in developing pumpkin seedlings, Plant Physiol., 2005, 139, 1, 213-223, https://doi.org/10.1104/pp.105.064162 . [all data]

Chung, Kuo, et al., 2003
Chung, J.-D.; Kuo, S.-R.; Chien, C.-T., Identification and quantification of gibberellin transformation and dosage changes in good and poor flowering clones of Calocedrus formosana grafts, Taiwan J. For. Sci., 2003, 18, 4, 387-400. [all data]

Yamazaki, Nishijima, et al., 2002
Yamazaki, H.; Nishijima, T.; Koshioka, M.; Miura, H., Gibberellins do no act against abscisic acid in the regulation of bulb dormancy of Allium wakegi Araki, Plant Growth Regul., 2002, 36, 3, 223-229, https://doi.org/10.1023/A:1016577529378 . [all data]

Chang, Chen, et al., 2001
Chang, S.-T.; Chen, W.-S.; Koshioka, M.; Mander, L.N.; Huang, K.-L.; Du, B.-S., Gibberellins in relation to flowering in Polianthes tuberosa, Physiol. Plant., 2001, 112, 3, 429-432, https://doi.org/10.1034/j.1399-3054.2001.1120317.x . [all data]

Fos, Nuez, et al., 2000
Fos, M.; Nuez, F.; Garcia-Martinez, J.L., The gene pat-2, which induces natural partenocarpy, alters the gibberellin content in unpollinated tomato ovaries, Plant Physiol., 2000, 122, 2, 471-479, https://doi.org/10.1104/pp.122.2.471 . [all data]

Martínez-García, Santes, et al., 2000
Martínez-García, J.F.; Santes, C.M.; García-Martínez, J.L., The end-of-day far-red irradiation increases gibberellin A1 content in cowpea (Vigna sinensis) epicotyls by reducing its inactivation, Physiol. Plant., 2000, 108, 4, 426-434, https://doi.org/10.1034/j.1399-3054.2000.t01-1-100413.x . [all data]

Pérez, Viani, et al., 2000
Pérez, F.J.; Viani, C.; Retamales, J., Bioactive gibberellins in seeded and seedless grapes: identification and changes in content during berry development, Am. J. Enol. Vitic, 2000, 51, 4, 315-318. [all data]

Ross, MacKenzie-Hose, et al., 1999
Ross, J.J.; MacKenzie-Hose, A.K.; Davies, P.J.; Lester, D.R.; Twitchin, B.; Reid, J.B., Further evidence for feedback regulation of gibberellin biosynthesis in pea, Physiol. Plant., 1999, 105, 3, 532-538, https://doi.org/10.1034/j.1399-3054.1999.105319.x . [all data]

Wang, Little, et al., 1996
Wang, Q.; Little, C.H.A.; Moritz, T.; Odén, P.C., Identification of endogenous gibberellins, and metabolism of tritiated and deuterated GA4, GA9, and GA20, in Scots pine (Pinus sylvestris) shoots, Physiol. Plant., 1996, 97, 4, 764-771, https://doi.org/10.1111/j.1399-3054.1996.tb00542.x . [all data]

van Huizen, Ozga, et al., 1995
van Huizen, R.; Ozga, J.A.; Reinecke, D.M.; Twitchin, B.; Mander, L.N., Seed and 4-chloroindole-3-acetic acid regulation of gibberellin metabolism in pea pericarp, Plant Physiol., 1995, 109, 4, 1213-1217, https://doi.org/10.1104/pp.109.4.1213 . [all data]

Kawaide, Sassa, et al., 1995
Kawaide, H.; Sassa, T.; Kamiya, Y., Plant-like biosynthesis of gibberellin A1 in the fungus Phaeosphaeria Sp. L487, Phytochemistry, 1995, 39, 2, 305-310, https://doi.org/10.1016/0031-9422(95)00006-S . [all data]

Koshioka, Nishijama, et al., 1995
Koshioka, M.; Nishijama, T.; Mander, L.N., Gibberellin metabolism in suspension cultured cells of Raphanus Sativus, Phytochemistry, 1995, 38, 2, 359-363, https://doi.org/10.1016/0031-9422(94)00624-3 . [all data]

Lange, Hedden, et al., 1993
Lange, T.; Hedden, P.; Graebe, J.E., Biosynthesis of 12«alpha»- and 13-hydroxylated gibberellins in a cell-free system from Cucurbita maxima endosperm and the identification of new endogenous gibberellins, Planta, 1993, 189, 3, 340-349, https://doi.org/10.1007/BF00194430 . [all data]

Nishijima, Murakami, et al., 1993
Nishijima, T.; Murakami, F.; Koshioka, M.; Yamazaki, H., Endogenous gibberellins in Aralia cordata, Japan Society for Biosci. Biotechnol. Agrochem., 1993, 57, 1, 1953-1954, https://doi.org/10.1271/bbb.57.1953 . [all data]

Talon, Zacarias, et al., 1992
Talon, M.; Zacarias, L.; PRimo-Millo, E., Gibberellins and Partenocarpic ability in developing ovaries of seedless mandarins, Plant Physiol., 1992, 99, 4, 1575-1581, https://doi.org/10.1104/pp.99.4.1575 . [all data]

Beall, Morgan, et al., 1991
Beall, F.D.; Morgan, P.W.; Mander, L.N.; Miller, F.R.; Babb, K.H., Genetic regulation of development in Sorghum bicolor. V. The ma3R allele results in gibberellin enrichment, Plant Physiol., 1991, 95, 1, 116-125, https://doi.org/10.1104/pp.95.1.116 . [all data]

Garcia-Martinez, Santes, et al., 1991
Garcia-Martinez, J.L.; Santes, C.; Croker, S.J.; Hedden, P., Identification, quantitation and distribution of gibberellins in fruits of Pisum sativum L. cv. Alaska during pod development, Planta, 1991, 184, 1, 53-60, https://doi.org/10.1007/BF00208236 . [all data]

Matheussen, Morgan, et al., 1991
Matheussen, A.-M.; Morgan, P.W.; Frederiksen, R.A., Implication of gibberellins in head smut (Sporisorium reilianum) of Sorghum bicolor, Plant Physiol., 1991, 96, 2, 537-544, https://doi.org/10.1104/pp.96.2.537 . [all data]

Talon, Zeevaart, et al., 1991
Talon, M.; Zeevaart, J.A.D.; Gage, D.A., Identification of gibberellins in spinach and effects of light and darkness on their levels, Plant Physiol., 1991, 97, 4, 1521-1526, https://doi.org/10.1104/pp.97.4.1521 . [all data]

Nakayama, Yamane, et al., 1990
Nakayama, M.; Yamane, H.; Yokota, T.; Yamaguchi, I.; Murofushi, N.; Takahashi, N.; Nishijima, T.; Katsura, N.; Nonaka, M.; Gaskin, P.; MacMillan, J.; Mander, L.N.; Chu, A., Endogenous gibberellins in mature seed of Raphanus sativus L. cv. Taibyo-sobutori, Agric. Biol. Chem., 1990, 54, 3, 837-840, https://doi.org/10.1271/bbb1961.54.837 . [all data]

Yamane, Fujioka, et al., 1988
Yamane, H.; Fujioka, S.; Spray, C.R.; Phinney, B.O.; MacMillan, J.; Gaskin, P.; Takahashi, N., Endogenous Gibberellines from Sporophytes of Two Tree Ferns, Cibotium glaucum and Dicksonia antarctica, Plant Phisiol., 1988, 86, 3, 857-862, https://doi.org/10.1104/pp.86.3.857 . [all data]


Notes

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