GA17, MeTMS


Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBCP Sil 5 CBOV-1OV-1BP-1
Column length (m) 25.25.25.25.25.
Carrier gas HeHeHe  
Substrate      
Column diameter (mm) 0.250.250.20.20.2
Phase thickness (μm)   0.250.250.1
Program 60C(0.7min) => 20C/min => 220C => 4C/min => 300C60C(0.7min) => 20C/min => 220C => 4C/min => 300C60C(2min) => 10C/min => 150C => 3C/min => 300C(10min)60C(2min) => 10C/min => 150C => 3C/min => 300C60C(2min) => 10C/min => 150C => 3C/min => 300C
I 2629.2629.2575.2575.2582.
ReferenceTaylor, Blake, et al., 2000Taylor, Blake, et al., 2000Davis, Kobayashi, et al., 1999Webb, Appleford, et al., 1998Webb, Appleford, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1OV-1OV-1OV-1OV-1
Column length (m) 25.25.25.25.25.
Carrier gas    HeHe
Substrate      
Column diameter (mm) 0.20.20.20.20.2
Phase thickness (μm) 0.10.250.25  
Program 60C(2min) => 10C/min => 150C => 3C/min => 300C60C(2min) => 10C/min => 150C => 3C/min => 300C60C(2min) => 10C/min => 150C => 3C/min => 300C60C(2min) => 13C/min => 150C => 3C/min => 280C(10min)60C(2min) => 13C/min => 150C => 3C/min => 280C(10min)
I 2583.2575.2579.2583.2584.
ReferenceWebb, Appleford, et al., 1998Santes, Hedden, et al., 1995Santes, Hedden, et al., 1995Talo, Spray, et al., 1995Talo, Spray, et al., 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1CP Sil 5 CBSE-52SE-52SPB-1
Column length (m) 15.25.25.25.30.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.220.250.220.220.25
Phase thickness (μm) 0.25 0.250.250.25
Program 60(0.1 min)-200 0C at 20 deg/min; 200-300 0C at 5 deg/min60C(0.3min) => 20C/min => 220C => 4C/min => 300C50C => 15C/min => 240C => 4C/min => 300C50C => 15C/min => 240C => 4C/min => 300C60C(2min) => 20C/min => 160C => 5C/min => 290C
I 2585.2605.2568.2571.2590.
ReferencePearce, Koshioka, et al., 1994Taylor, Blake, et al., 1994Hedden, Hoad, et al., 1993Hedden, Hoad, et al., 1993Poling and Maier, 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase SPB-1OV-1OV-1
Column length (m) 30. 25.
Carrier gas HeHeHe
Substrate    
Column diameter (mm) 0.25 0.2
Phase thickness (μm) 0.25  
Program 60C(2min) => 20C/min => 160C => 5C/min => 290C50C(1min) => 15C/min => 200C => 4C/min => 260C60C(2min) => 13C/min => 150C => 3C/min => 280C(10min)
I 2594.2569.2567.
ReferencePoling and Maier, 1988Heupel R.C., Phinney B.O., et al., 1985Gaskin, Gilmour, et al., 1984
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Taylor, Blake, et al., 2000
Taylor, D.R.; Blake, P.S.; Crisp, C.M., Identification of gibberellins in leaf tissues of day-neutral strawberry (Fragaria × ananassa Duch.) cultivars, Plant Growth Regul., 2000, 30, 1, 5-7, https://doi.org/10.1023/A:1006275024517 . [all data]

Davis, Kobayashi, et al., 1999
Davis, G.; Kobayashi, M.; Phinney, B.O.; Lange, T.; Croker, S.J.; Gaskin, P.; MacMillan, J., Gibberellin biosynthesis in maize. Metabolic studies with GA15, GA24, GA25, GA7, and 2,3-dehydro-GA9, Plant Physiol., 1999, 121, 3, 1037-1045, https://doi.org/10.1104/pp.121.3.1037 . [all data]

Webb, Appleford, et al., 1998
Webb, S.E.; Appleford, N.E.J.; Gaskin, P.; Lenton, J.R., Gibberellins in internodes and ears of wheat containing different dwarfing alleles, Phytochemistry, 1998, 47, 5, 671-677, https://doi.org/10.1016/S0031-9422(97)00684-5 . [all data]

Santes, Hedden, et al., 1995
Santes, C.M.; Hedden, P.; Gaskin, P.; Garcia-Martinez, J.L., Gibberellins and related compounds in young fruits of pea and their relationship to fruit-set, Phytochemistry, 1995, 40, 5, 1347-1355, https://doi.org/10.1016/0031-9422(95)00489-T . [all data]

Talo, Spray, et al., 1995
Talo, A.; Spray, C.R.; Somers, D.A.; Donovan, C.M.; Gaskin, P.; Macmillian, J.; Phinney, B.O., Endogenous gibberellins from callus cultures of maize, Phytochemistry, 1995, 40, 1, 11-15, https://doi.org/10.1016/0031-9422(95)00000-W . [all data]

Pearce, Koshioka, et al., 1994
Pearce, D.W.; Koshioka, M.; Pharis, R.P., Chromatography of gibberellins, J. Chromatogr. A, 1994, 658, 1, 91-122, https://doi.org/10.1016/0021-9673(94)85210-3 . [all data]

Taylor, Blake, et al., 1994
Taylor, D.R.; Blake, P.S.; Browning, G., Identification of gibberellins in leaf tissues of strawberry (Fragaria × ananassa Duch.) grown under different photoperiods, Plant Growth Regul., 1994, 15, 3, 235-240, https://doi.org/10.1007/BF00029896 . [all data]

Hedden, Hoad, et al., 1993
Hedden, P.; Hoad, G.V.; Gaskin, P.; Lewis, M.J.; Green, J.R.; Furber, M.; Mander, L.N., Kaurenoids and gibberellins, including the newly characterized gibberellin A88, in developing apple seeds, Phytochemistry, 1993, 32, 2, 231-237, https://doi.org/10.1016/S0031-9422(00)94973-2 . [all data]

Poling and Maier, 1988
Poling, S.M.; Maier, V.P., Identification of endogenous gibberellins in navel orange shoots, Plant Physiol., 1988, 88, 3, 639-642, https://doi.org/10.1104/pp.88.3.639 . [all data]

Heupel R.C., Phinney B.O., et al., 1985
Heupel R.C.; Phinney B.O.; Spray C.R.; Gaskin P.; MacMillan J.; Hedden P.; Graebe J.E., Native gibberellins and the metabolism of [14C] gibberellin A53 and of [17-C-13,17-3H)] gibberellin A-20 in tassels of Zea-mays, Phytochemistry, 1985, 24, 1, 47-53, https://doi.org/10.1016/S0031-9422(00)80805-5 . [all data]

Gaskin, Gilmour, et al., 1984
Gaskin, P.; Gilmour, S.J.; Lenton, J.R.; MacMillan, J.; Sponsel, V.M., Endogenous gibberellins and kauranoids identified from developing and germinating barley grain, J. Plant Growth Regul., 1984, 2, 1-4, 229-242, https://doi.org/10.1007/BF02042252 . [all data]


Notes

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