GA14, MeTMS
- Formula: C25H40O5Si
- Molecular weight: 448.6676
- IUPAC Standard InChI: InChI=1S/C25H40O5Si/c1-15-13-25-14-16(15)9-10-17(25)23(2)12-11-18(30-31(6,7)8)24(3,22(27)29-5)20(23)19(25)21(26)28-4/h16-20H,1,9-14H2,2-8H3/t16-,17?,18+,19-,20?,23+,24-,25+/m0/s1
- IUPAC Standard InChIKey: QQEYOHKHRLMQMP-ZGHKCMSCSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Stereoisomers:
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Van Den Dool and Kratz RI, non-polar column, custom temperature program
Go To: Top, References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
| Column type | Capillary | Capillary | Capillary |
|---|---|---|---|
| Active phase | PE-1HT | BPX-5 | DB-1 |
| Column length (m) | 30. | 30. | 15. |
| Carrier gas | He | He | |
| Substrate | |||
| Column diameter (mm) | 0.32 | 0.25 | 0.22 |
| Phase thickness (μm) | 0.1 | 0.25 | 0.25 |
| Program | 60C => 45C/min => 220C => 4C/min => 300C | 60C => 45C/min => 220C => 4C/min => 300C | 60(0.1 min)-200 0C at 20 deg/min; 200-300 0C at 5 deg/min |
| I | 2485. | 2537. | 2496. |
| Reference | Frisse, Pimenta, et al., 2003 | Frisse, Pimenta, et al., 2003 | Pearce, Koshioka, et al., 1994 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI |
References
Go To: Top, Van Den Dool and Kratz RI, non-polar column, custom temperature program, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Frisse, Pimenta, et al., 2003
Frisse, A.; Pimenta, M.J.; Lange, T.,
Expression studies of gibberellin oxidases in developing pumpkin seeds,
Plant Physiol., 2003, 131, 3, 1220-1227, retrieved from http://www.plantphysiol.org, https://doi.org/10.1104/pp.015206
. [all data]
Pearce, Koshioka, et al., 1994
Pearce, D.W.; Koshioka, M.; Pharis, R.P.,
Chromatography of gibberellins,
J. Chromatogr. A, 1994, 658, 1, 91-122, https://doi.org/10.1016/0021-9673(94)85210-3
. [all data]
Notes
Go To: Top, Van Den Dool and Kratz RI, non-polar column, custom temperature program, References
- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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