Dibenzothiophene, 2,4-dimethyl


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-Petro2050.Lu, Wu, et al., 200450. m/0.20 mm/0.50 μm, He, 35. C @ 5. min, 2. K/min, 300. C @ 5. min
CapillaryPONA2050.Yang, Wang, et al., 200250. m/0.20 mm/0.50 μm, 1.5 K/min, 270. C @ 10. min; Tstart: 120. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-Petro2050.Lu, Wu, et al., 200450. m/0.20 mm/0.50 μm, He; Program: not specified

Lee's RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-5MS329.92Schade and Andersson, 200630. m/0.25 mm/0.25 μm, He, 60. C @ 1. min, 10. K/min; Tend: 300. C
CapillaryHP-5MS330.72Zhou, Wang, et al., 200430. m/0.25 mm/0.25 μm, 65. C @ 5. min, 3. K/min, 290. C @ 20. min

Lee's RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-5MS329.95Zhou, Wang, et al., 200430. m/0.25 mm/0.25 μm; Program: not specified
CapillaryDB-5328.05Mössner, de Alda, et al., 199960. m/0.25 mm/0.25 μm, He; Program: 60C (1 min) => 45 C/min => 150C (2 min) => 2 C/min => 300 C (25 min)

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Lu, Wu, et al., 2004
Lu, X.; Wu, J.; Wu, J.; Kong, H.; Hua, R.; Tao, W.; Gu, J.; Xu, G., Characterization and quantitative determination of diesel fractions by comprehensive two-dimensional gas chromatography/time of flight mass spectrometry, Chin. J. Chromatogr., 2004, 22, 1, 5-11. [all data]

Yang, Wang, et al., 2002
Yang, Y.-T.; Wang, H.-Y.; Lu, W.-Z., Determination od sulfur compounds in catalytic diesel oil by gas chromatography with atomic emission detector and its application, Chin. J. Chromatogr., 2002, 20, 6, 493-497. [all data]

Schade and Andersson, 2006
Schade, T.; Andersson, J.T., Speciation of alkylated dibenzothiophenes through correlation of structure and gas chromatographic retention indexes, J. Chromatogr. A, 2006, 1117, 2, 206-213, https://doi.org/10.1016/j.chroma.2006.03.079 . [all data]

Zhou, Wang, et al., 2004
Zhou, J.; Wang, T.; Shi, Q.; Huang, Y.; Mao, T.; Zhong, N.; Zhang, Y.; Zhang, X., Determination of sulfur and oxygen containing polycyclic aromatic hydrocarbons in inhalable particulate by gas chromatography - mass spectrometry, J. Chin. Mass Spectrom. Soc., 2004, 25, 3, 134-140. [all data]

Mössner, de Alda, et al., 1999
Mössner, S.G.; de Alda, M.J.L.; Sander, L.C.; Lee, M.L.; Wise, S.A., Gas chromatographic retention behavior of polycyclic aromatic sulfur heterocyclic compounds, (dibenzothiophene, naphtho[b]thiophenes, benzo[b]naphthothiophenes and alkyl-substituted derivatives) on stationary phases of different selectivity, J. Chromatogr. A, 1999, 841, 2, 207-228, https://doi.org/10.1016/S0021-9673(99)00363-5 . [all data]


Notes

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