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1-nonen-3-one


Normal alkane RI, polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxDB-WaxStabilwaxSupelcowax-10
Column length (m) 30.30.30.30.60.
Carrier gas HeliumHeliumHeliumHeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.250.53
Phase thickness (mum) 0.250.250.250.501.
Tstart (C) 60.60.60.35.40.
Tend (C) 200.200.200.225.240.
Heat rate (K/min) 8.8.8.6.4.
Initial hold (min) 3.3.3.5.2.
Final hold (min) 9.59.59.510.20.
I 1418.1430.1433.1398.1427.
ReferenceRochat, Egger, et al., 2009Rochat, Egger, et al., 2009Rochat, Egger, et al., 2009Watcharananun, Cadwallader, et al., 2009Rochat and Chaintreau, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax-10Supelcowax-10DB-WaxEC-1000HP-FFAP
Column length (m) 60.60.30.30.50.
Carrier gas HeHeH2He 
Substrate      
Column diameter (mm) 0.530.530.320.250.32
Phase thickness (mum) 1.1.0.50.250.5
Tstart (C) 40.40.40.35.35.
Tend (C) 240.240.200.230.230.
Heat rate (K/min) 4.4.4.5.6.
Initial hold (min) 2.2.5.5. 
Final hold (min) 20.20. 15.15.
I 1428.1430.1422.1410.1405.
ReferenceRochat and Chaintreau, 2005Rochat and Chaintreau, 2005Culleré, Escudero, et al., 2004Bendall, 2001Preininger and Ullrich, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase Carbowax 20M
Column length (m) 15.
Carrier gas  
Substrate  
Column diameter (mm) 0.32
Phase thickness (mum)  
Tstart (C) 50.
Tend (C) 225.
Heat rate (K/min) 6.
Initial hold (min) 3.
Final hold (min)  
I 1405.
ReferenceRoberts and Acree, 1996
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Rochat, Egger, et al., 2009
Rochat, S.; Egger, J.; Chaintreau, A., Strategy for the identification of key odorants: application to shrimp aroma, J. Chromatogr. A, 2009, 1216, 36, 6424-6432, https://doi.org/10.1016/j.chroma.2009.07.014 . [all data]

Watcharananun, Cadwallader, et al., 2009
Watcharananun, W.; Cadwallader, K.R.; Huangrak, K.; Kim, H.; Lorjaroenphon, Y., Identification of predominant odorants in Thai desserts flavored by smoking with Tian Op, a traditional Thai scented candle, J. Agric. Food Chem., 2009, 57, 3, 996-1005, https://doi.org/10.1021/jf802674c . [all data]

Rochat and Chaintreau, 2005
Rochat, S.; Chaintreau, A., Carbonyl Odorants Contributing to the In-Oven Roast Beef Top Note, J. Agric. Food Chem., 2005, 53, 24, 9578-9585, https://doi.org/10.1021/jf058089l . [all data]

Culleré, Escudero, et al., 2004
Culleré, L.; Escudero, A.; Cacho, J.; Ferreira, V., Gas chromatography-olfactometry and chemical quantitative study of the aroma of six premium auality Spanish aged red wines, J. Agric. Food Chem., 2004, 52, 6, 1653-1660, https://doi.org/10.1021/jf0350820 . [all data]

Bendall, 2001
Bendall, J.G., Aroma compounds of fresh milk from New Zealand cows fed different diets, J. Agric. Food Chem., 2001, 49, 10, 4825-4832, https://doi.org/10.1021/jf010334n . [all data]

Preininger and Ullrich, 2001
Preininger, M.; Ullrich, F., Trace compound analysis for off-flavor characterization of micromilled milk powder, Am. Chem. Soc. Symp. Ser., 2001, 782, 46-61. [all data]

Roberts and Acree, 1996
Roberts, D.D.; Acree, T.E., Effects of heating and cream addition on fresh raspberry aroma using a retronasal aroma simulator and gas chromatography olfactometry, J. Agric. Food Chem., 1996, 44, 12, 3919-3925, https://doi.org/10.1021/jf950701t . [all data]


Notes

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