3-Methyl-2-butenyl (E)-caffeate, bis-TMS


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryPE-52422.Isidorov and Vinogorova, 2003He, 5. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tstart: 50. C; Tend: 250. C
CapillaryMethyl Silicone2396.Greenaway and Whatley, 199125. m/0.32 mm/0.50 μm, He, 3. K/min; Tstart: 75. C; Tend: 310. C
CapillaryMethyl Silicone2402.Greenaway and Whatley, 199025. m/0.32 mm/0.5 μm, He, 3. K/min; Tstart: 75. C; Tend: 300. C

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Isidorov and Vinogorova, 2003
Isidorov, V.A.; Vinogorova, V.T., GC-MS analysis of compounds extracted from buds of Populus balsamifera and Populus nigra, Z. Naturforsch. C:, 2003, 58, 355-360. [all data]

Greenaway and Whatley, 1991
Greenaway, W.; Whatley, F.R., Synthesis of esters of acetyloxycaffeic acids and their occurrence in poplar bud exudates, J. Chromatogr., 1991, 543, 113-121, https://doi.org/10.1016/S0021-9673(01)95759-0 . [all data]

Greenaway and Whatley, 1990
Greenaway, W.; Whatley, F.R., Resolution of complex mixtures of phenolics in poplar bud exudate by analysis of gas chromatography-mass spectrometry data, J. Chromatogr., 1990, 519, 1, 145-158, https://doi.org/10.1016/0021-9673(90)85143-J . [all data]


Notes

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