5β-Pregnane-11,20-dione-3α,21-diol, EO-TMS, # 1


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type Capillary
Active phase SE-52
Column length (m) 19.
Carrier gas Helium
Substrate  
Column diameter (mm) 0.40
Phase thickness (μm)  
Tstart (C) 160.
Tend (C) 260.
Heat rate (K/min) 2.
Initial hold (min)  
Final hold (min)  
I 3058.
ReferenceHonour, Tourniaire, et al., 1978
Comment MSDC-RI

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Honour, Tourniaire, et al., 1978
Honour, J.W.; Tourniaire, J.; Biglieri, E.G.; Shackleton, C.H.L., Urinary steroid excretion in 17alpha-hydroxylase deficiency, J. Steroid Biochem., 1978, 9, 6, 495-505, https://doi.org/10.1016/0022-4731(78)90115-2 . [all data]


Notes

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