3α,16α-dihydroxy-5α-androstan-17-one, MO-TMS, (syn,anti)
- Formula: C28H55NO3Si3
- Molecular weight: 537.9977
- IUPAC Standard InChI: InChI=1S/C28H55NO3Si3/c1-27-16-14-21(30-33(3,4)5)18-20(27)12-13-22-23(27)15-17-28(2)24(22)19-25(31-34(6,7)8)26(28)29-32-35(9,10)11/h20-25H,12-19H2,1-11H3/t20-,21+,22?,23?,24?,25+,27-,28-/m1/s1
- IUPAC Standard InChIKey: GZYUNKFWUXTIDF-VYPMHKRISA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Stereoisomers:
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | OV-1 | 2618. | Bègue, Dumas, et al., 1979 | He, 1. K/min; Tstart: 180. C; Tend: 250. C |
| Capillary | OV-1 | 2624. | Bègue, Dumas, et al., 1979 | He, 1. K/min; Tstart: 180. C; Tend: 250. C |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Bègue, Dumas, et al., 1979
Bègue, R.-J.; Dumas, M.; Morinière, M.; Nivois, C.; Padieu, P.,
Steroids and hypertension. 1-Gas-liquid chromatography and gas chromatography mass spectrometry of 3,15- and 3,16-dihydroxy-17-oxosteroids,
Biomed. Mass Spectrom., 1979, 6, 11, 476-481, https://doi.org/10.1002/bms.1200061104
. [all data]
Notes
Go To: Top, Gas Chromatography, References
- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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