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Flavone, 3,5,7-trihydroxy, tris-TMS


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryMethyl Silicone2745.Greenaway and Whatley, 199025. m/0.32 mm/0.5 «mu»m, He, 3. K/min; Tstart: 75. C; Tend: 300. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryMethyl Silicone2738.Greenaway, May, et al., 1989Program: not specified

Normal alkane RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
PackedOV-1210.2692.Katagi, Horii, et al., 1973Nitrogen; Column length: 2. m

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-52785.Isidorov, Kotowska, et al., 200530. m/0.25 mm/0.25 «mu»m, He, 5. K/min; Tstart: 50. C; Tend: 300. C

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Greenaway and Whatley, 1990
Greenaway, W.; Whatley, F.R., Resolution of complex mixtures of phenolics in poplar bud exudate by analysis of gas chromatography-mass spectrometry data, J. Chromatogr., 1990, 519, 1, 145-158, https://doi.org/10.1016/0021-9673(90)85143-J . [all data]

Greenaway, May, et al., 1989
Greenaway, W.; May, J.; Whatley, F.R., Flavonoid aglycones identified by gas chromatography-mass spectrometry in bud exudate of Populus balsamifera, J. Chromatogr., 1989, 472, 393-400, https://doi.org/10.1016/S0021-9673(00)94139-6 . [all data]

Katagi, Horii, et al., 1973
Katagi, T.; Horii, A.; Oomura, Y.; Miyakawa, H.; Kyu, T.; Ikeda, Y.; Isoi, K., Gas chromatography of flavonoids, J. Chromatogr., 1973, 79, 45-56, https://doi.org/10.1016/S0021-9673(01)85272-9 . [all data]

Isidorov, Kotowska, et al., 2005
Isidorov, V.A.; Kotowska, U.; Vinogorova, V.T., GC Identification of organic compounds based on partition coefficients of their TMS derivatives in a hexane-acetonitrile system and retention indices, Anal. Sci., 2005, 21, 12, 1483-1489, https://doi.org/10.2116/analsci.21.1483 . [all data]


Notes

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