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Bisabolene


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
PackedOV-11461.Carter, Gianfagna, et al., 198915. K/min; Column length: 1.83 m; Tstart: 90. C; Tend: 200. C
CapillaryMethyl Silicone1465.4Rao, Rajanikanth, et al., 19894. K/min, 250. C @ 15. min; Column length: 12. m; Column diameter: 0.5 mm; Tstart: 70. C

Kovats' RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryBP-11500.MacLeod, MacLeod, et al., 1988Column length: 25. m; Column diameter: 0.2 mm; Program: not specified

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-51522.Bell, 200460. m/0.25 mm/0.25 «mu»m, Helium, 7. K/min; Tstart: 40. C; Tend: 250. C
CapillaryDB-51500.Tzakou, Roussis, et al., 1997He, 50. C @ 3. min, 5. K/min; Column length: 60. m; Column diameter: 0.24 mm; Tend: 280. C
CapillaryDB-11509.Stashenko, Prada, et al., 199660. m/0.25 mm/0.25 «mu»m, He, 50. C @ 5. min, 3.5 K/min; Tend: 250. C

Van Den Dool and Kratz RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-Wax1792.Stashenko, Prada, et al., 199660. m/0.25 mm/0.25 «mu»m, He, 50. C @ 5. min, 2.5 K/min; Tend: 180. C

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryOV-1011514.Zollo, Biyiti, et al., 19985. K/min; Column length: 25. m; Column diameter: 0.32 mm; Tstart: 50. C; Tend: 200. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-11540.Delort and Jaquier, 200960. m/0.25 mm/0.25 «mu»m, Helium; Program: 50 0C (5 min) 3 0C/min -> 120 0C 5 0C/min -> 250 0C (3 min) 15 0C/min -> 300 0C (20 min)
CapillaryOV-11487.Li, Liang, et al., 2009Helium; Column length: 30. m; Column diameter: 0.25 mm; Program: 40 0C 2 0C/min -> 120 0C 10 0C/min -> 230 0C (15 min)
CapillaryOV-11488.Li, Liang, et al., 2009Helium; Column length: 30. m; Column diameter: 0.25 mm; Program: 40 0C 2 0C/min -> 120 0C 10 0C/min -> 230 0C (15 min)

Normal alkane RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-Wax1777.Tu, Thanh, et al., 200260. m/0.25 mm/0.25 «mu»m, N2, 2. K/min; Tstart: 70. C; Tend: 230. C
CapillaryDB-Wax1736.Umano, Hagi, et al., 200260. m/0.25 mm/0.25 «mu»m, He, 40. C @ 2. min, 2. K/min; Tend: 200. C

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Carter, Gianfagna, et al., 1989
Carter, C.D.; Gianfagna, T.J.; Sacalis, J.N., Sesquiterpenes in glandular trichomes of a wild tomato species and toxicity to the Colorado potato beetle, J. Agric. Food Chem., 1989, 37, 5, 1425-1428, https://doi.org/10.1021/jf00089a048 . [all data]

Rao, Rajanikanth, et al., 1989
Rao, A.S.; Rajanikanth, B.; Seshadri, R., Volatile aroma components of Curcuma amada Roxb., J. Agric. Food Chem., 1989, 37, 3, 740-743, https://doi.org/10.1021/jf00087a036 . [all data]

MacLeod, MacLeod, et al., 1988
MacLeod, A.J.; MacLeod, G.; Subramanian, G., Volatile aroma constituents of orange, Phytochemistry, 1988, 27, 7, 2185-2188, https://doi.org/10.1016/0031-9422(88)80123-7 . [all data]

Bell, 2004
Bell, W.A.-M., Examination of Aroma Volatiles Formed from Thermal Processing of Florida Reconstituted Grapefruit Juice. A Thesis presented to the graduate school of the university of Florida in partial fulfillment of the requirements for the degree of master of science, 2004. [all data]

Tzakou, Roussis, et al., 1997
Tzakou, O.; Roussis, V.; Loukis, A.; Harvala, C.; Galati, E.M.; Germanò, M.P., Essential oil analysis of Teucrium divaricatum Heldr. ssp. divaricatum growing in Greece, Flavour Fragr. J., 1997, 12, 2, 113-115, https://doi.org/10.1002/(SICI)1099-1026(199703)12:2<113::AID-FFJ633>3.0.CO;2-3 . [all data]

Stashenko, Prada, et al., 1996
Stashenko, E.E.; Prada, N.Q.; Martínez, J.R., HRGC/FID/NP and HRGC/MSD study of Colombian Ylang-Ylang (Cananga odorata) oils obtained by different extraction techniques, J. Hi. Res. Chromatogr., 1996, 19, 6, 353-358, https://doi.org/10.1002/jhrc.1240190609 . [all data]

Zollo, Biyiti, et al., 1998
Zollo, P.H.A.; Biyiti, L.; Tchoumbougnang, F.; Menut, C.; Lamaty, G.; Bouchet, Ph., Aromatic plants of tropical central Africa. Part XXXII. Chemical composition and antifungal activity of thirteen essential oils from aromatic plants of Cameroon, Flavour Fragr. J., 1998, 13, 2, 107-114, https://doi.org/10.1002/(SICI)1099-1026(199803/04)13:2<107::AID-FFJ701>3.0.CO;2-G . [all data]

Delort and Jaquier, 2009
Delort, E.; Jaquier, A., Novel terpenyl esters from Australian finger lime (Citrus australasica) peel extract, Flav. Fragr. J., 2009, 24, 3, 123-132, https://doi.org/10.1002/ffj.1922 . [all data]

Li, Liang, et al., 2009
Li, X.-R.; Liang, Y.-Z.; Zhou, T.; Zhang, L.-X.; Hu, C.-D., Comparative analysis of volatile constituents between recipe jingfangsan and its single herbs by GC-MS combined with alternative moving window factor analysis method, J. Sep. Sci., 2009, 32, 2, 258-266, https://doi.org/10.1002/jssc.200800574 . [all data]

Tu, Thanh, et al., 2002
Tu, N.T.M.; Thanh, L.X.; Une, A.; Ukeda, H.; Sawamura, M., Volatile constituents of Vietnamese pummelo, orange, tangerine and lime peel oils, Flavour Fragr. J., 2002, 17, 3, 169-174, https://doi.org/10.1002/ffj.1076 . [all data]

Umano, Hagi, et al., 2002
Umano, K.; Hagi, Y.; Shibamoto, T., Volatile chemicals identified in extracts from newly hybrid citrus, dekopon (Shiranuhi mandarin Suppl. J.), J. Agric. Food Chem., 2002, 50, 19, 5355-5359, https://doi.org/10.1021/jf0203951 . [all data]


Notes

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