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3«alpha»-hydroxy-pregn-4-en-20-one, MO-TMS


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryZB-12746.Ebner, Corol, et al., 200630. m/0.25 mm/0.25 «mu»m, He; Program: 70C(5min) => 20C/min => 220C(0.33min) => 5C/min => 315C (4min)

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-5MS2737.Eechaute, Dhooge, et al., 199930. m/0.25 mm/0.25 «mu»m, He, 4. K/min; Tstart: 150. C; Tend: 290. C

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Ebner, Corol, et al., 2006
Ebner, M.J.; Corol, D.I.; Havlíková, H.; Honour, J.W.; Fry, J.P., Identification of neuroactive steroids and their precursors and metabolites in adult male rat brain, Endocrinology, 2006, 147, 1, 179-190, https://doi.org/10.1210/en.2005-1065 . [all data]

Eechaute, Dhooge, et al., 1999
Eechaute, W.P.; Dhooge, W.S.; Gao, C.Q.; Calders, P.; Rubens, R.; Weyne, J.; Kaufman, J.M., Progesterone-transforming enzyme activity in the hypothalamus of the male rat, J. Steroid Biochem. Mol. Biol., 1999, 70, 4-6, 159-167, https://doi.org/10.1016/S0960-0760(99)00106-5 . [all data]


Notes

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