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15-Methylhentriacontane


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-5MS3132.Steiner, Steidle, et al., 200530. m/0.32 mm/0.25 «mu»m, He, 2. K/min; Tstart: 150. C; Tend: 300. C
CapillaryHT-53133.Goh S.H., Ooi K.E., et al., 199325. m/0.53 mm/0.22 «mu»m, N2, 15. K/min, 320. C @ 20. min; Tstart: 150. C
CapillaryHT-53132.Goh S.H., Ooi K.E., et al., 199325. m/0.53 mm/0.22 «mu»m, N2, 15. K/min, 320. C @ 20. min; Tstart: 150. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryDB-13135.Bernier, Carlson, et al., 199830. m/0.32 mm/0.25 «mu»m; Program: 60C (2min) => 10C/min => 220C => 3C/min => 310C
CapillaryDB-13134.Sutton and Carlson, 1993He; Column length: 30. m; Column diameter: 0.25 mm; Program: 60C => 20C/min => 230C => 5C/min => 330C

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryUltra-13130.Nelson and Charlet, 2003He, 4. K/min; Column length: 12.5 m; Column diameter: 0.2 mm; Tstart: 150. C; Tend: 320. C
CapillaryDB-53130.Juárez, Blomquist, et al., 2001He, 3. K/min; Column length: 30. m; Column diameter: 0.32 mm; Tstart: 200. C; Tend: 280. C
CapillaryCP Sil 5 CB3131.Sinninghe Damsté, Erkes, et al., 19954. K/min; Tstart: 130. C; Tend: 320. C
CapillaryBP-13126.Lockey and Oraha, 199012. m/0.22 mm/0.25 «mu»m, Helium, 2. K/min; Tstart: 100. C; Tend: 300. C
PackedOV-1013127.Nelson, de Renobales, et al., 1989Helium, Gas-Chrom Q (100-120 mesh), 3. K/min, 320. C @ 25. min; Column length: 3. m; Tstart: 150. C
CapillaryDexsil 3003130.Lockey, 19785. K/min; Column length: 15. m; Tstart: 50. C; Tend: 370. C

Normal alkane RI, non-polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryMethyl Silicone3132.Sullivan, 2002Program: not specified
CapillaryDB-13135.Carlson, Geden, et al., 199930. m/0.32 mm/0.25 «mu»m, He; Program: 60C (2min) => 10C/min => 220C => 3C/min => 310C (12 - 42 min)
CapillaryCP Sil 5 CB3131.Kenig, Sinninghe Damsté, et al., 199525. m/0.32 mm/0.2 «mu»m, He; Program: 50C => 20C/min => 130C => 4C/min => 300C (20min)
CapillaryDexsil 3003121.Lockey, 1981Column length: 15. m; Program: 50 0C 5 0C/min -> 200 0C 2 0C/min -> 340 0C
CapillaryDexsil 3003132.Lockey, 1981Column length: 15. m; Program: 50 0C 5 0C/min -> 200 0C 2 0C/min -> 340 0C

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Steiner, Steidle, et al., 2005
Steiner, S.; Steidle, J.L.M.; Ruther, J., Female sex pheromone in immature insect males - a case of pre-emergence chemical mimicry?, Behavioral Ecology and Sociobiology, 2005, 58, 2, 111-120, https://doi.org/10.1007/s00265-005-0930-x . [all data]

Goh S.H., Ooi K.E., et al., 1993
Goh S.H.; Ooi K.E.; Chuah C.H.; Yong H.S.; Khoo S.G.; Ong S.H., Cuticular hydrocarbons from two species of Malaysian Bactrocera fruit flies, Biochem. Syst. Ecol., 1993, 21, 2, 215-226, https://doi.org/10.1016/0305-1978(93)90039-T . [all data]

Bernier, Carlson, et al., 1998
Bernier, U.R.; Carlson, D.A.; Geden, C.J., Gas chromatography/mass spectrometry analysis of the cuticular hydrocarbons from parasitic wasps of the genus Muscidifurax, J. Am. Soc. Mass Spectrom., 1998, 9, 4, 320-332, https://doi.org/10.1016/S1044-0305(97)00288-2 . [all data]

Sutton and Carlson, 1993
Sutton, B.D.; Carlson, D.A., Interspecific variation in tephritid fruit fly larvae surface hydrocarbons, Arch. Insect Biochem. Physiol., 1993, 23, 2, 53-65, https://doi.org/10.1002/arch.940230202 . [all data]

Nelson and Charlet, 2003
Nelson, D.R.; Charlet, L.D., Cuticular hydrocarbons of the sunflower beetle,Zygogramma exclamationis, Comp. Biochem. Physiol. B: Comp. Biochem., 2003, 135, 2, 273-284, https://doi.org/10.1016/S1096-4959(03)00080-0 . [all data]

Juárez, Blomquist, et al., 2001
Juárez, P.; Blomquist, G.J.; Schofield, C.J., Hydrocarbons of Rhodnius prolixus, a Chagas disease vector, Comp. Biochem. Physiol. B: Comp. Biochem., 2001, 129, 4, 733-746, https://doi.org/10.1016/S1096-4959(01)00380-3 . [all data]

Sinninghe Damsté, Erkes, et al., 1995
Sinninghe Damsté, J.S.; Erkes, A.-M.W.E.P.; Rijpstra, W.I.C.; de Leeuw, J.W.; Wakeham, S.G., C32-C36 polymethyl alkenes in Black Sea sediments, Geochim. Cosmochim. Acta, 1995, 59, 2, 347-353, https://doi.org/10.1016/0016-7037(95)00281-4 . [all data]

Lockey and Oraha, 1990
Lockey, K.H.; Oraha, V.S., Cuticular lipids of adult Locusta Migratoria Migratoriodes (R and F), Schstocerca Gregaria (Forskal) (Acrididae) and other orthopteran species - II. Hydrocarbons, Comp. Biochem. Physiol., 1990, 95B, 4, 721-744. [all data]

Nelson, de Renobales, et al., 1989
Nelson, D.R.; de Renobales, M.; Dwyer, L.A.; Zamboni, A.C.; Fatland, C.L.; Blomquist, G.J., Novel very long-chain methyl branched alcohols and their esters, and methyl branched alkanes in pupae of the gabbage looper, Trichoplusa ni (Hubner), Insect Biochem., 1989, 19, 2, 197-208, https://doi.org/10.1016/0020-1790(89)90092-9 . [all data]

Lockey, 1978
Lockey, K.H., The adult cuticular hydrocarbons of Tenebrio Molitor L. and Tenebrio Obscurus F. (Coleoptera: Tenebrionidae), Insect Biochem., 1978, 8, 4, 237-250, https://doi.org/10.1016/0020-1790(78)90032-X . [all data]

Sullivan, 2002
Sullivan, B.T., Evidence for a sex pheromone in bark beetle parasitoid Roptrpcerus xylophagorum, J. Chem. Ecology, 2002, 28, 5, 1045-1063, https://doi.org/10.1023/A:1015270003717 . [all data]

Carlson, Geden, et al., 1999
Carlson, D.A.; Geden, C.J.; Bernier, U.R., Identification of pupal exiviae of Nasania vitripennis and Muscidifurax raptorellus parasitoids using cuticular hydrocarbons, Biol. Control, 1999, 15, 2, 97-106, https://doi.org/10.1006/bcon.1999.0708 . [all data]

Kenig, Sinninghe Damsté, et al., 1995
Kenig, F.; Sinninghe Damsté, J.S.; Kock-van Dalen, A.C.; Rijpstra, W.I.C.; Huc, A.Y.; de Leeuw, J.W., Occurrence and origin of mono-, di-, and trimethylalkanes in modern and holocene cyanobacterial mats from Abu Dhabi, United Arab Emirates, Geochim. Cosmochim. Acta, 1995, 59, 14, 2999-3015, https://doi.org/10.1016/0016-7037(95)00190-5 . [all data]

Lockey, 1981
Lockey, K.H., Cuticular hydrocarbons of adult Cylindrinotus laevioctostriatus (Goeze) and Phylan gibbus (Fabricius) (Coleoptera: Tenebrionidae), Insect. Biochem., 1981, 11, 5, 549-561, https://doi.org/10.1016/0020-1790(81)90023-8 . [all data]


Notes

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