20-hydroxy-methylprednisolone, MO-tetraTMS (3)


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type Capillary
Active phase Cross-Linked Methylsilicone
Column length (m) 25.
Carrier gas He
Substrate  
Column diameter (mm) 0.2
Phase thickness (μm) 0.11
Tstart (C) 220.
Tend (C) 270.
Heat rate (K/min) 2.
Initial hold (min)  
Final hold (min)  
I 3337.
ReferenceRodchenkov, Uralets, et al., 1987
Comment MSDC-RI

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Rodchenkov, Uralets, et al., 1987
Rodchenkov, G.M.; Uralets, V.P.; Semenov, V.A., Determination of methylprednisolone metabolites in human urine by gas chromatography-mass spectrometry, J. Chromatogr., 1987, 423, 15-22, https://doi.org/10.1016/0378-4347(87)80323-7 . [all data]


Notes

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